TWI604061B - Alloy manufacturing method and an alloy manufacturing equipment - Google Patents

Alloy manufacturing method and an alloy manufacturing equipment Download PDF

Info

Publication number
TWI604061B
TWI604061B TW105124087A TW105124087A TWI604061B TW I604061 B TWI604061 B TW I604061B TW 105124087 A TW105124087 A TW 105124087A TW 105124087 A TW105124087 A TW 105124087A TW I604061 B TWI604061 B TW I604061B
Authority
TW
Taiwan
Prior art keywords
alloy
crucible
raw material
manufacturing apparatus
preheater
Prior art date
Application number
TW105124087A
Other languages
Chinese (zh)
Other versions
TW201803998A (en
Inventor
Jin-Chin Guan
K Chow Hubert
Original Assignee
Hsu-Yang Technologies Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hsu-Yang Technologies Co Ltd filed Critical Hsu-Yang Technologies Co Ltd
Priority to TW105124087A priority Critical patent/TWI604061B/en
Application granted granted Critical
Publication of TWI604061B publication Critical patent/TWI604061B/en
Publication of TW201803998A publication Critical patent/TW201803998A/en

Links

Landscapes

  • Powder Metallurgy (AREA)

Description

合金製造設備 Alloy manufacturing equipment

一種合金製造設備,尤指利用原料與原料之間發生化學反應所產生的熱能,激發整體的固態反應(Solid Reaction),因而合成新的合金之設備。 An alloy manufacturing equipment, in particular, a device that synthesizes a new alloy by utilizing thermal energy generated by a chemical reaction between a raw material and a raw material to excite an overall solid reaction (Solid Reaction).

按,一般使用於合金製造之自然反應熔煉法(Spontaneous Reaction Synthesis SRS),是利用物體之間發生化學反應所產生的熱能,激發整體的固態反應(Solid Reaction),因而合成新的合金,現有的自然反應熔煉法,是將多種不同合金原料(粉末),混合壓成胚體,在放進真空爐中進行加熱,使其產生自然反應製成合金,然而合金原料必須事先混合加工成胚體,造成製程複雜、成本增加等問題。 According to the Spontaneous Reaction Synthesis (SRS), which is generally used in the manufacture of alloys, it uses the thermal energy generated by chemical reactions between objects to excite the entire solid reaction, thus synthesizing new alloys. The natural reaction melting method is to mix a plurality of different alloy raw materials (powders) into an embryo body, and heat them in a vacuum furnace to produce a natural reaction to form an alloy. However, the alloy raw materials must be mixed and processed into an embryo body in advance. This causes problems such as complicated processes and increased costs.

再者,真空爐進行加熱所製成之合金,須經由冷卻裝置進行冷卻,一般作法係直接將真空爐連接冷卻裝置,此種作法冷卻裝置大部份時間會處於等待狀態,無法有效的提高產能。 Furthermore, the alloy produced by heating in a vacuum furnace must be cooled by a cooling device. Generally, the vacuum furnace is directly connected to the cooling device, and the cooling device of this method is in a waiting state for most of the time, and the productivity cannot be effectively improved. .

是以,要如何解決上述習知之問題與缺失,即為相關業者所亟欲研發之課題所在。 Therefore, how to solve the above-mentioned problems and shortcomings is the subject of research and development that the relevant industry is eager to develop.

本發明之主要目的乃在於,利用製造合金之複數種原料於製造設備內,依據原料之熔點由低至高形成複數層原料層,俾使複數原料層由下至上依序反應製成合金,進而省略習知技術中須事先將原料混合加工成胚體之工 序,以節省生產時間,提高生產效率。 The main object of the present invention is to form a plurality of raw material layers from low to high in accordance with the melting point of the raw materials by using a plurality of raw materials for manufacturing the alloy, and to form an alloy by sequentially reacting the plurality of raw material layers from bottom to top, thereby omitting In the prior art, the raw materials must be mixed and processed into the body of the embryo. Order to save production time and increase production efficiency.

本創作之次要目的在於,利用複數個加熱裝置以循環方式進行抽真空、預熱以及加熱流程,俾使複數個加熱裝置依序將反應形成的合金送入冷卻裝置進行冷卻,提高設備之利用率以及降低生產成本。 The secondary purpose of this creation is to use a plurality of heating devices to perform vacuuming, preheating and heating processes in a cyclic manner, so that a plurality of heating devices sequentially send the alloy formed by the reaction into a cooling device for cooling, thereby improving the utilization of the device. Rate and reduce production costs.

為達上述目的,本發明合金製造設備係設置有加熱裝置,以及連接於加熱裝置之冷卻裝置,加熱裝置具有坩鍋、預熱器以及加熱器,當製造設備進行製造合金時,係將製造合金之複數種原料(粉末狀),依據原料之熔點由低至高依序置入製造設備之坩鍋內,使合金之原料於坩鍋內,形成複數層原料層,且上方原料層之熔點高於下方原料層之熔點,續利用預熱器對坩鍋進行預熱,以及加熱器對原料層之原料進行加熱,讓複數原料層由下至上產生反應過程,再將反應形成的合金送入冷卻裝置進行冷卻。 To achieve the above object, the alloy manufacturing apparatus of the present invention is provided with a heating device, and a cooling device connected to the heating device, the heating device having a crucible, a preheater, and a heater, which are alloyed when the manufacturing equipment manufactures the alloy. The plurality of raw materials (powder) are placed in the crucible of the manufacturing equipment according to the melting point of the raw materials from low to high, so that the raw materials of the alloy are formed in the crucible to form a plurality of raw material layers, and the melting point of the upper raw material layer is higher than The melting point of the raw material layer is continued, and the crucible is preheated by the preheater, and the raw material of the raw material layer is heated by the heater, the reaction process is generated from the bottom to the top of the plurality of raw material layers, and the alloy formed by the reaction is sent to the cooling device. Cool down.

前述合金製造設備,其中該製造設備之預熱器進行預熱以及加熱器進行加熱前,係先使坩鍋內形成真空狀態或是將惰性氣體填充於坩鍋內。 In the foregoing alloy manufacturing apparatus, before the preheater of the manufacturing apparatus performs preheating and the heater is heated, the vacuum is formed in the crucible or the inert gas is filled in the crucible.

前述合金製造設備,其中該製造設備之坩鍋具有鍋體以及鍋蓋,預熱器係設置於鍋體外側,加熱器係設置於鍋蓋,且坩鍋連接有氣管以及排料管。 In the above alloy manufacturing apparatus, the crucible of the manufacturing apparatus has a pot body and a lid, the preheater is disposed outside the pot body, the heater is disposed on the pot lid, and the crucible is connected with the gas pipe and the discharge tube.

前述合金製造設備,其中該製造設備之加熱裝置為複數設置,且各製造設備之預熱器進行預熱以及加熱器進行加熱前,係先以抽真空方式使坩鍋內形成真空狀態或是將惰性氣體填充於坩鍋內,且複數個加熱裝置係以循環方式進行抽真空、預熱以及加熱流程,俾使複數個加熱裝置依序將反應形成的合金送入冷卻裝置進行冷卻。 The above-mentioned alloy manufacturing equipment, wherein the heating device of the manufacturing device is provided in plural, and before the preheater of each manufacturing device is preheated and the heater is heated, the vacuum state is formed in the crucible by vacuuming or The inert gas is filled in the crucible, and a plurality of heating devices perform a vacuuming, preheating, and heating process in a circulating manner, and the plurality of heating devices sequentially feed the alloy formed by the reaction into a cooling device for cooling.

10‧‧‧製造設備 10‧‧‧Manufacture equipment

1‧‧‧加熱裝置 1‧‧‧heating device

11‧‧‧坩鍋 11‧‧‧ Shabu Shabu

111‧‧‧鍋體 111‧‧‧ pot body

112‧‧‧鍋蓋 112‧‧‧ pot lid

12‧‧‧預熱器 12‧‧‧Preheater

13‧‧‧加熱器 13‧‧‧heater

14‧‧‧氣管 14‧‧‧ trachea

15‧‧‧排料管 15‧‧‧Drainage tube

2‧‧‧冷卻裝置 2‧‧‧Cooling device

21‧‧‧冷卻槽 21‧‧‧Cooling trough

22‧‧‧進氣管 22‧‧‧Air intake pipe

23‧‧‧出氣管 23‧‧‧Exhaust pipe

24‧‧‧進料口 24‧‧‧ Feed inlet

25‧‧‧出料口 25‧‧‧Outlet

A‧‧‧原料層 A‧‧‧Material layer

B‧‧‧合金 B‧‧‧ alloy

第一圖係為本發明之示意圖(一)。 The first figure is a schematic diagram (1) of the present invention.

第二圖係為本發明之示意圖(二)。 The second figure is a schematic diagram (2) of the present invention.

第三圖係為本發明第一種製造合金方式之流程圖。 The third figure is a flow chart of the first method of manufacturing an alloy according to the present invention.

第四圖係為本發明第二種製造合金方式之流程圖。 The fourth figure is a flow chart of the second method of manufacturing an alloy of the present invention.

請參閱第一圖與第二圖所示,由圖中可清楚看出,本發明合金之製造設備10係設置有複數個加熱裝置1,以及連接於加熱裝置1之冷卻裝置2,其中:該加熱裝置1具有坩鍋11、預熱器12以及加熱器13,坩鍋11具有鍋體111以及鍋蓋112,預熱器12係設置於鍋體111外側,加熱器13係設置於鍋蓋112,且坩鍋11連接有氣管14以及排料管15。 Referring to the first and second figures, it can be clearly seen from the figure that the manufacturing apparatus 10 of the alloy of the present invention is provided with a plurality of heating devices 1 and a cooling device 2 connected to the heating device 1, wherein: The heating device 1 has a crucible 11, a preheater 12, and a heater 13. The crucible 11 has a pot body 111 and a lid 112. The preheater 12 is disposed outside the pot body 111, and the heater 13 is disposed on the lid 112. And the crucible 11 is connected with the gas pipe 14 and the discharge pipe 15.

該冷卻裝置2具有冷卻槽21,以及連通於冷卻槽21之進氣管22與出氣管23,冷卻槽21上下二側分別設置有進料口24與出料口25,且進料口24連通於各加熱裝置1之排料管15。 The cooling device 2 has a cooling tank 21, and an air inlet pipe 22 and an air outlet pipe 23 that communicate with the cooling tank 21. The upper and lower sides of the cooling tank 21 are respectively provided with a feed port 24 and a discharge port 25, and the feed port 24 is connected. The discharge pipe 15 of each heating device 1 is used.

請參閱第一圖至第三圖所示,當本發明於進行合金製造時,係先將製造合金之複數種原料,依據原料之熔點由低至高依序置入坩鍋11內,形成複數層原料層A,使上方原料層A之熔點高於下方原料層A之熔點,續利用氣管14對坩鍋11內進行抽氣,使坩鍋11內形成真空狀態,再利用預熱器12對坩鍋11進行預熱,以及加熱器13對原料層A之原料進行加熱,讓複數原料層A由下至上產生反應過程,再將反應形成的合金B經由排料管15送入冷卻裝置2之冷卻槽21進行冷卻,此時冷卻裝置2之進氣管22會將冷卻氣體送入冷卻槽21內,讓冷卻氣體與合金B進行熱交換後,再由出氣管23排出,俾使由進料口24進入冷卻槽21之合金B於送出出料口25時,可大幅降其溫度。 Referring to the first to third figures, when the invention is used in the manufacture of an alloy, a plurality of raw materials for manufacturing the alloy are first placed in the crucible 11 according to the melting point of the raw material, to form a plurality of layers. In the raw material layer A, the melting point of the upper raw material layer A is higher than the melting point of the lower raw material layer A, and the inside of the crucible 11 is continuously evacuated by the gas pipe 14, so that the crucible 11 is in a vacuum state, and the preheater 12 is used to face the crucible. The pot 11 is preheated, and the heater 13 heats the raw material of the raw material layer A, the reaction process is generated from the bottom to the top of the plurality of raw material layers A, and the alloy B formed by the reaction is sent to the cooling device 2 through the discharge pipe 15 for cooling. The tank 21 is cooled. At this time, the intake pipe 22 of the cooling device 2 sends the cooling gas into the cooling tank 21, and the cooling gas is heat-exchanged with the alloy B, and then discharged from the gas outlet pipe 23, so that the feed port is made. When the alloy B entering the cooling tank 21 is sent out of the discharge port 25, the temperature thereof can be drastically lowered.

請參閱第一圖、第二圖與第四圖所示,本發明另一製造合金之程序,係先將製造合金之複數種原料,依據原料之熔點由低至高依序置入坩鍋11內,形成複數層原料層A,使上方原料層A之熔點高於下方原料層A之熔點,續利用氣管14對坩鍋11內填充惰性氣體,再利用預熱器12對坩鍋11進行預熱,以及加熱器13對原料層A之原料進行加熱,讓複數原料層A由下至上產生反應過程,再將反應形成的合金B,經由排料管15送入冷卻裝置2之冷卻槽21進行冷卻程序。 Referring to the first, second and fourth figures, another procedure for manufacturing an alloy according to the present invention is to firstly process a plurality of raw materials for the alloy, and sequentially place the raw materials according to the melting point of the raw materials into the crucible 11 from low to high. a plurality of raw material layers A are formed such that the melting point of the upper raw material layer A is higher than the melting point of the lower raw material layer A, and the inert gas is filled in the crucible 11 by the gas pipe 14, and the crucible 11 is preheated by the preheater 12. And the heater 13 heats the raw material of the raw material layer A, causes the plural raw material layer A to generate a reaction process from bottom to top, and then transfers the alloy B formed by the reaction to the cooling tank 21 of the cooling device 2 through the discharge pipe 15 for cooling. program.

再者,由於本發明製造設備10之加熱裝置1為複數設置,因此複數個加熱裝置1可以循環方式進行抽真空(填充惰性氣體)、預熱以及加熱流程,俾使複數個加熱裝置1依序將反應形成的合金B送入冷卻裝置2進行冷卻,提高冷卻裝置2之使用率,避免設備閒置。 Furthermore, since the heating device 1 of the manufacturing apparatus 10 of the present invention is provided in plural, a plurality of heating devices 1 can perform vacuuming (filling of inert gas), preheating, and heating processes in a cyclic manner, so that a plurality of heating devices 1 are sequentially arranged. The alloy B formed by the reaction is sent to the cooling device 2 for cooling, thereby increasing the utilization rate of the cooling device 2 and preventing the device from being idle.

Claims (5)

一種合金製造設備,其中:該製造設備係設置有加熱裝置,以及連接於加熱裝置之冷卻裝置,加熱裝置具有坩鍋、預熱器以及加熱器;將製造合金之複數種原料,依據原料之熔點由低至高依序置入製造設備之坩鍋內,使合金之原料於坩鍋內,形成複數層原料層,且上方原料層之熔點高於下方原料層之熔點,續利用預熱器對坩鍋進行預熱,以及加熱器對原料層之原料進行加熱,讓複數原料層由下至上產生反應過程,再將反應形成的合金送入冷卻裝置進行冷卻;前述之加熱裝置為複數設置,且各加熱裝置之預熱器進行預熱以及加熱器進行加熱前,係先以抽真空方式使坩鍋內形成真空狀態,且複數個加熱裝置係以循環方式進行抽真空、預熱以及加熱流程,俾使複數個加熱裝置依序將反應形成的合金送入冷卻裝置進行冷卻。 An alloy manufacturing apparatus, wherein: the manufacturing apparatus is provided with a heating device, and a cooling device connected to the heating device, the heating device has a crucible, a preheater and a heater; a plurality of materials for manufacturing the alloy, according to the melting point of the raw material The low-to-high order is placed in the crucible of the manufacturing equipment, and the raw material of the alloy is placed in the crucible to form a plurality of raw material layers, and the melting point of the upper raw material layer is higher than the melting point of the lower raw material layer, and the preheater is used for the crucible. The pot is preheated, and the heater heats the raw material of the raw material layer, the reaction process is generated from the bottom to the top of the plurality of raw material layers, and the alloy formed by the reaction is sent to a cooling device for cooling; the aforementioned heating device is provided in plural, and each Before the preheater of the heating device is preheated and the heater is heated, the vacuum state is formed in the crucible by vacuuming, and the plurality of heating devices are vacuumed, preheated and heated in a circulating manner. The plurality of heating means sequentially feeds the alloy formed by the reaction into a cooling device for cooling. 如請求項1所述之合金製造設備,其中該製造設備之預熱器進行預熱以及加熱器進行加熱前,係先使坩鍋內形成真空狀態。 The alloy manufacturing apparatus according to claim 1, wherein the preheater of the manufacturing apparatus is preheated and the heater is heated to form a vacuum state in the crucible. 如請求項1所述之合金製造設備,其中該製造設備之預熱器進行預熱以及加熱器進行加熱前,係先於坩鍋內填充惰性氣體。 The alloy manufacturing apparatus according to claim 1, wherein the preheater of the manufacturing apparatus is preheated and the heater is heated before the inert gas is filled in the crucible. 如請求項1所述之合金製造設備,其中該製造設備之坩鍋具有鍋體以及鍋蓋,預熱器係設置於鍋體外側,加熱器係設置於鍋蓋,且坩鍋連接有氣管以及排料管。 The alloy manufacturing apparatus according to claim 1, wherein the crucible of the manufacturing apparatus has a pot body and a lid, the preheater is disposed outside the pot body, the heater is disposed on the lid, and the crucible is connected with the trachea and Discharge tube. 如請求項1所述之合金製造設備,其中該製造設備之加熱裝置為複數設置,且各製造設備之預熱器進行預熱以及加熱器進行加熱前,係先將惰性氣體填充於坩鍋內,且複數個加熱裝置係以循環方式進行抽真空、預熱以及加熱流程,俾使複數個加熱裝置依序將反應形成的合金送入冷卻裝置進行冷 卻。 The alloy manufacturing apparatus according to claim 1, wherein the heating device of the manufacturing device is provided in plural, and before the preheater of each manufacturing device is preheated and the heater is heated, the inert gas is first filled in the crucible. And a plurality of heating devices perform a vacuuming, preheating, and heating process in a cyclic manner, and the plurality of heating devices sequentially send the alloy formed by the reaction into the cooling device for cooling. but.
TW105124087A 2016-07-29 2016-07-29 Alloy manufacturing method and an alloy manufacturing equipment TWI604061B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
TW105124087A TWI604061B (en) 2016-07-29 2016-07-29 Alloy manufacturing method and an alloy manufacturing equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
TW105124087A TWI604061B (en) 2016-07-29 2016-07-29 Alloy manufacturing method and an alloy manufacturing equipment

Publications (2)

Publication Number Publication Date
TWI604061B true TWI604061B (en) 2017-11-01
TW201803998A TW201803998A (en) 2018-02-01

Family

ID=61023024

Family Applications (1)

Application Number Title Priority Date Filing Date
TW105124087A TWI604061B (en) 2016-07-29 2016-07-29 Alloy manufacturing method and an alloy manufacturing equipment

Country Status (1)

Country Link
TW (1) TWI604061B (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWM512452U (en) * 2015-06-11 2015-11-21 Her Chang Technology Co Ltd Cast molding device
CN105648243A (en) * 2014-11-27 2016-06-08 Ald真空技术股份有限公司 Melting method for alloys

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105648243A (en) * 2014-11-27 2016-06-08 Ald真空技术股份有限公司 Melting method for alloys
TWM512452U (en) * 2015-06-11 2015-11-21 Her Chang Technology Co Ltd Cast molding device

Also Published As

Publication number Publication date
TW201803998A (en) 2018-02-01

Similar Documents

Publication Publication Date Title
CN106041025A (en) Inert gas shielding immersion type heating difunctional low-pressure casting furnace
CN206721301U (en) A kind of microwave radiation technology leaching device
TWI604061B (en) Alloy manufacturing method and an alloy manufacturing equipment
CN106521202B (en) A kind of preparation method of molybdenum hafnium alloy plate
CN100551832C (en) A kind of preparation high temperature nuclear reactor fuel element UO 2The method of nuclear core
JP2016532629A5 (en)
CN207276500U (en) A kind of cooled-preheated circulator of light calcined magnesia shaft furnace
CN101845559B (en) Device and method for preparing lithium metal by using vacuum metal heat reduction
CN203855414U (en) Tubular graphitization furnace
CN103072960B (en) Production method of nano silicon nitride powder
CN205329110U (en) Annealing furnace
CN102795620B (en) A kind of hot pressure sintering stove for producing high purity graphite
CN103290237A (en) Arsenic lead alloy synthesis and sublimation integral furnace used for producing high-purity arsenic
CN102674359A (en) Device and method for cooing tail gas recovery liquid of polysilicon reduction furnace with inner tank
CN106044749A (en) Novel copper and copper-alloy coated graphite powder and graphene material and preparation method thereof
JP2005225690A (en) METHOD AND APPARATUS FOR MANUFACTURING SiO
CN201280434Y (en) High-purity graphitization apparatus
CN202350506U (en) Recycling device for heat energy of intermediate-frequency induction roasting furnace
CN105648534A (en) Process for synthesizing gallium arsenide polycrystalline material
JP2020001999A (en) Semiconductor synthesis device and synthesis method
JP2008115068A (en) Process for producing aluminum nitride containing material
CN104388688A (en) Device and method for smelting lithium through vacuum thermal reduction of metal
CN105758176A (en) Device for preparing high-purity nano molybdenum trioxide
CN207501654U (en) A kind of heat-treatment furnace
CN207828393U (en) A kind of residual heat insulation is brought down a fever stove