TWI563090B - The preparation of caprolactam from 6-amino caproic acid obtained in a fermentation process - Google Patents
The preparation of caprolactam from 6-amino caproic acid obtained in a fermentation processInfo
- Publication number
- TWI563090B TWI563090B TW104123268A TW104123268A TWI563090B TW I563090 B TWI563090 B TW I563090B TW 104123268 A TW104123268 A TW 104123268A TW 104123268 A TW104123268 A TW 104123268A TW I563090 B TWI563090 B TW I563090B
- Authority
- TW
- Taiwan
- Prior art keywords
- caprolactam
- preparation
- fermentation process
- caproic acid
- acid obtained
- Prior art date
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title 2
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 title 1
- 229960002684 aminocaproic acid Drugs 0.000 title 1
- 238000000855 fermentation Methods 0.000 title 1
- 230000004151 fermentation Effects 0.000 title 1
- 238000002360 preparation method Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D223/08—Oxygen atoms
- C07D223/10—Oxygen atoms attached in position 2
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Micro-Organisms Or Cultivation Processes Thereof (AREA)
- Polyamides (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09180383 | 2009-12-22 |
Publications (2)
Publication Number | Publication Date |
---|---|
TW201615838A TW201615838A (zh) | 2016-05-01 |
TWI563090B true TWI563090B (en) | 2016-12-21 |
Family
ID=41818720
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TW104123268A TWI563090B (en) | 2009-12-22 | 2010-12-21 | The preparation of caprolactam from 6-amino caproic acid obtained in a fermentation process |
TW099144938A TWI537386B (zh) | 2009-12-22 | 2010-12-21 | 由發酵法獲得的6-胺己酸製備己內醯胺 |
TW105130335A TWI624546B (zh) | 2009-12-22 | 2010-12-21 | 由發酵法獲得的6-胺己酸製備己內醯胺(三) |
Family Applications After (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TW099144938A TWI537386B (zh) | 2009-12-22 | 2010-12-21 | 由發酵法獲得的6-胺己酸製備己內醯胺 |
TW105130335A TWI624546B (zh) | 2009-12-22 | 2010-12-21 | 由發酵法獲得的6-胺己酸製備己內醯胺(三) |
Country Status (9)
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI563090B (en) * | 2009-12-22 | 2016-12-21 | Dsm Ip Assets Bv | The preparation of caprolactam from 6-amino caproic acid obtained in a fermentation process |
WO2014182016A1 (ko) * | 2013-05-06 | 2014-11-13 | 한국생명공학연구원 | 6-아미노카프로산의 생물학적 합성 및 이를 위한 형질전환 미생물 |
US10087472B2 (en) | 2013-05-06 | 2018-10-02 | Korea Research Institute Of Bioscience And Biotechnology | Biological synthesis of 6-aminocaproic acid and transgenic microorganism therefor |
WO2016048048A1 (ko) * | 2014-09-23 | 2016-03-31 | 한국생명공학연구원 | 신규 카프로락탐 전환 효소를 이용한 ε-카프로락탐의 제조 방법 |
US20160297747A1 (en) * | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange |
RU2640657C1 (ru) * | 2017-02-15 | 2018-01-11 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Ивановский государственный химико-технологический университет" (ИГХТУ) | Способ выделения капролактама из содержащих капролактам и его олигомеры полимеров |
WO2020060970A1 (en) | 2018-09-18 | 2020-03-26 | Invista North America S.A.R.L. | Systems and methods for recovering amines and their derivates from aqueous mixtures |
JP7205275B2 (ja) * | 2018-09-21 | 2023-01-17 | 日立金属株式会社 | ガリウムの回収方法 |
CN109280023B (zh) * | 2018-12-04 | 2020-06-12 | 河北美邦工程科技股份有限公司 | 一种己内酰胺连续结晶纯化方法 |
IT201800021409A1 (it) * | 2018-12-28 | 2020-06-28 | Aquafil S P A | Processo per la produzione di epsilon caprolattame dallacido 6-aminocaproico. |
JP7196669B2 (ja) * | 2019-02-14 | 2022-12-27 | 日立金属株式会社 | ガリウムの回収方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060127975A1 (en) * | 2002-11-27 | 2006-06-15 | Thomas Link | Method for culturing cells in order to produce substances |
US20070254341A1 (en) * | 2004-01-19 | 2007-11-01 | Raemakers-Franken Petronella C | Biochemical Synthesis of 6-Amino Caproic Acid |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1268869A (en) | 1968-09-04 | 1972-03-29 | Teijin Ltd | PROCESS FOR THE PREPARATION OF epsilon-CAPROLACTAM |
EP0860431A1 (en) * | 1997-02-19 | 1998-08-26 | Dsm N.V. | Process to prepare e-caprolactam |
KR100516986B1 (ko) * | 1997-02-19 | 2005-09-26 | 코닌클리즈케 디에스엠 엔.브이. | 6-아미노카프론산 유도체를 과열 수증기와 접촉시킴으로써 촉매 없이 카프로락탐을 제조하는 방법 |
US5990306A (en) * | 1997-09-03 | 1999-11-23 | Alliedsignal Inc. | Process for the purification of caprolactam obtained from the depolymerization of polyamide-containing carpet |
EP0943608A1 (en) * | 1998-03-20 | 1999-09-22 | Dsm N.V. | Process for the continuous purification of crude epsilon--caprolactam |
EP1761487B1 (en) * | 2004-06-10 | 2013-08-07 | Board of Trustees of Michigan State University | Synthesis of caprolactam from lysine |
US7145713B2 (en) * | 2004-07-13 | 2006-12-05 | Montana State University | Techniques for recovering optical spectral features using a chirped optical field |
US7947483B2 (en) * | 2007-08-10 | 2011-05-24 | Genomatica, Inc. | Methods and organisms for the growth-coupled production of 1,4-butanediol |
CN109055450A (zh) | 2008-03-11 | 2018-12-21 | 基因组股份公司 | 从5-甲酰缬草酸制备6-氨基己酸 |
TWI563090B (en) * | 2009-12-22 | 2016-12-21 | Dsm Ip Assets Bv | The preparation of caprolactam from 6-amino caproic acid obtained in a fermentation process |
-
2010
- 2010-12-21 TW TW104123268A patent/TWI563090B/zh active
- 2010-12-21 TW TW099144938A patent/TWI537386B/zh active
- 2010-12-21 TW TW105130335A patent/TWI624546B/zh active
- 2010-12-22 BR BR112012015506A patent/BR112012015506A2/pt not_active Application Discontinuation
- 2010-12-22 JP JP2012545882A patent/JP5777067B2/ja active Active
- 2010-12-22 WO PCT/NL2010/050878 patent/WO2011078668A1/en active Application Filing
- 2010-12-22 EA EA201200931A patent/EA029354B1/ru unknown
- 2010-12-22 EA EA201792404A patent/EA201792404A1/ru unknown
- 2010-12-22 US US13/518,647 patent/US20130030146A1/en not_active Abandoned
- 2010-12-22 UA UAA201208949A patent/UA105409C2/uk unknown
- 2010-12-22 CN CN201080059413.7A patent/CN102686562B/zh active Active
- 2010-12-22 CN CN201410284066.8A patent/CN104177282B/zh active Active
- 2010-12-22 MY MYPI2020004950A patent/MY196967A/en unknown
- 2010-12-22 MY MYPI2016703173A patent/MY177957A/en unknown
- 2010-12-22 MY MYPI2012700394A patent/MY161889A/en unknown
- 2010-12-22 BR BR122017013721A patent/BR122017013721A8/pt not_active Application Discontinuation
-
2015
- 2015-04-28 JP JP2015091816A patent/JP2015180635A/ja active Pending
- 2015-12-08 US US14/963,114 patent/US20160200677A1/en not_active Abandoned
-
2017
- 2017-05-08 JP JP2017092480A patent/JP6499225B2/ja active Active
-
2019
- 2019-03-14 JP JP2019046791A patent/JP2019115352A/ja active Pending
-
2020
- 2020-07-17 US US16/932,405 patent/US20210171459A1/en not_active Abandoned
-
2021
- 2021-03-04 JP JP2021034513A patent/JP2021098720A/ja active Pending
-
2023
- 2023-05-02 JP JP2023075986A patent/JP2023099166A/ja active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060127975A1 (en) * | 2002-11-27 | 2006-06-15 | Thomas Link | Method for culturing cells in order to produce substances |
US20070254341A1 (en) * | 2004-01-19 | 2007-11-01 | Raemakers-Franken Petronella C | Biochemical Synthesis of 6-Amino Caproic Acid |
Also Published As
Publication number | Publication date |
---|---|
MY196967A (en) | 2023-05-15 |
BR122017013721A2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 2011-06-30 |
EA201200931A1 (ru) | 2013-01-30 |
MY177957A (en) | 2020-09-28 |
EA201792404A1 (ru) | 2018-03-30 |
JP2017214358A (ja) | 2017-12-07 |
BR112012015506A2 (pt) | 2015-09-22 |
WO2011078668A1 (en) | 2011-06-30 |
MY161889A (en) | 2017-05-15 |
JP5777067B2 (ja) | 2015-09-09 |
CN102686562B (zh) | 2014-07-16 |
TW201726922A (zh) | 2017-08-01 |
TW201129699A (en) | 2011-09-01 |
BR122017013721A8 (pt) | 2018-01-02 |
CN104177282B (zh) | 2017-06-27 |
JP6499225B2 (ja) | 2019-04-10 |
CN102686562A (zh) | 2012-09-19 |
JP2013515050A (ja) | 2013-05-02 |
JP2015180635A (ja) | 2015-10-15 |
TWI537386B (zh) | 2016-06-11 |
EA029354B1 (ru) | 2018-03-30 |
JP2023099166A (ja) | 2023-07-11 |
JP2021098720A (ja) | 2021-07-01 |
TW201615838A (zh) | 2016-05-01 |
US20160200677A1 (en) | 2016-07-14 |
TWI624546B (zh) | 2018-05-21 |
US20210171459A1 (en) | 2021-06-10 |
CN104177282A (zh) | 2014-12-03 |
JP2019115352A (ja) | 2019-07-18 |
UA105409C2 (uk) | 2014-05-12 |
US20130030146A1 (en) | 2013-01-31 |
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