TWI490193B - 用於二氯丙醇的共沸回收之方法與設備 - Google Patents

用於二氯丙醇的共沸回收之方法與設備 Download PDF

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Publication number
TWI490193B
TWI490193B TW097113155A TW97113155A TWI490193B TW I490193 B TWI490193 B TW I490193B TW 097113155 A TW097113155 A TW 097113155A TW 97113155 A TW97113155 A TW 97113155A TW I490193 B TWI490193 B TW I490193B
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TW
Taiwan
Prior art keywords
liquid
mixture
ester
hydrochlorination
phase
Prior art date
Application number
TW097113155A
Other languages
English (en)
Chinese (zh)
Other versions
TW200906779A (en
Inventor
Danil Tirtowidjojo
Andrei S Merenov
Christian D Kneupper
Bruce D Hook
Anil J Mehta
Original Assignee
Dow Global Technologies Llc
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Publication date
Application filed by Dow Global Technologies Llc filed Critical Dow Global Technologies Llc
Publication of TW200906779A publication Critical patent/TW200906779A/zh
Application granted granted Critical
Publication of TWI490193B publication Critical patent/TWI490193B/zh

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/34—Halogenated alcohols
    • C07C31/42—Polyhydroxylic acyclic alcohols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
TW097113155A 2007-04-12 2008-04-11 用於二氯丙醇的共沸回收之方法與設備 TWI490193B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US92302007P 2007-04-12 2007-04-12

Publications (2)

Publication Number Publication Date
TW200906779A TW200906779A (en) 2009-02-16
TWI490193B true TWI490193B (zh) 2015-07-01

Family

ID=39643205

Family Applications (2)

Application Number Title Priority Date Filing Date
TW097113155A TWI490193B (zh) 2007-04-12 2008-04-11 用於二氯丙醇的共沸回收之方法與設備
TW104101060A TW201518267A (zh) 2007-04-12 2008-04-11 用於二氯丙醇的共沸回收之方法與設備

Family Applications After (1)

Application Number Title Priority Date Filing Date
TW104101060A TW201518267A (zh) 2007-04-12 2008-04-11 用於二氯丙醇的共沸回收之方法與設備

Country Status (7)

Country Link
US (1) US8629305B2 (enExample)
EP (1) EP2137124A1 (enExample)
JP (1) JP2010523703A (enExample)
KR (1) KR20090130123A (enExample)
CN (1) CN101657405A (enExample)
TW (2) TWI490193B (enExample)
WO (1) WO2008128013A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2137124A1 (en) 2007-04-12 2009-12-30 Dow Global Technologies Inc. Process and apparatus for azeotropic recovery of dichlorohydrins
US8420870B2 (en) * 2007-04-12 2013-04-16 Dow Global Technologies Llc Process and apparatus for recovery of dichlorohydrins via codistillation
JP2011516552A (ja) 2008-04-09 2011-05-26 ダウ グローバル テクノロジーズ リミティド ライアビリティ カンパニー ジクロロヒドリン類の効率的回収のための方法及び装置
WO2011000896A1 (en) 2009-07-03 2011-01-06 Akzo Nobel Chemicals International B.V. Process for preparing dichlorohydrin
EP2576489A1 (en) * 2010-05-26 2013-04-10 Dow Global Technologies LLC Process for hydrochlorination of multihydroxylated aliphatic hydrocarbons
TWI547470B (zh) * 2015-12-18 2016-09-01 長春人造樹脂廠股份有限公司 製造二氯丙醇之方法
BR112019002563B1 (pt) * 2016-08-11 2022-07-12 Versalis S.P.A. Processo para a purificação do solvente derivado da produção de misturas elastoméricas
CN109107207B (zh) * 2018-07-18 2021-07-23 万华化学集团股份有限公司 一种带有外循环系统的反应精馏装置及其应用
CN111875477A (zh) * 2020-08-03 2020-11-03 岳阳隆兴实业公司 一种邻氯醇共沸提纯方法
CN111943805A (zh) * 2020-09-16 2020-11-17 安徽工业大学 一种(r)-3-氯-1,2-丙二醇的制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200602999A (en) * 2004-02-27 2006-01-16 Imation Corp Multi-connector memory card with retractable sheath to protect the connectors
TW200904786A (en) * 2007-04-12 2009-02-01 Dow Global Technologies Inc Multi-stage process and apparatus for recovering dichlorohydrins
TW200906778A (en) * 2007-04-12 2009-02-16 Dow Global Technologies Inc Process and appratus for recovery of dichlorohydrins via codistillation

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE197308C (enExample)
JPS60258171A (ja) * 1984-06-04 1985-12-20 Showa Denko Kk エピクロルヒドリンの製造方法
CZ20032346A3 (cs) 2003-09-01 2005-04-13 Spolek Pro Chemickou A Hutní Výrobu,A.S. Způsob přípravy dichlorpropanolů z glycerinu
EP1770081A1 (en) * 2003-11-20 2007-04-04 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol , the glycerol coming eventualy from the conversion of animal fats in the manufacture of biodiesel
KR101225402B1 (ko) * 2004-07-21 2013-01-23 다우 글로벌 테크놀로지스 엘엘씨 다중히드록시화-지방족 탄화수소 또는 그의 에스테르의클로로히드린으로의 전환
EP1762556A1 (en) * 2005-05-20 2007-03-14 SOLVAY (Société Anonyme) Process for producing dichloropropanol from glycerol
US8344185B2 (en) * 2005-05-20 2013-01-01 SOLVAY (Société Anonyme Method for making a chlorhydrine by reaction between a polyhydroxylated aliphatic hydrocarbon and a chlorinating agent
CN100509726C (zh) 2007-01-26 2009-07-08 江苏工业学院 一种从甘油制备二氯丙醇的方法
EP2137124A1 (en) 2007-04-12 2009-12-30 Dow Global Technologies Inc. Process and apparatus for azeotropic recovery of dichlorohydrins

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200602999A (en) * 2004-02-27 2006-01-16 Imation Corp Multi-connector memory card with retractable sheath to protect the connectors
TW200904786A (en) * 2007-04-12 2009-02-01 Dow Global Technologies Inc Multi-stage process and apparatus for recovering dichlorohydrins
TW200906778A (en) * 2007-04-12 2009-02-16 Dow Global Technologies Inc Process and appratus for recovery of dichlorohydrins via codistillation

Also Published As

Publication number Publication date
KR20090130123A (ko) 2009-12-17
EP2137124A1 (en) 2009-12-30
TW200906779A (en) 2009-02-16
TW201518267A (zh) 2015-05-16
US20100105965A1 (en) 2010-04-29
CN101657405A (zh) 2010-02-24
WO2008128013A1 (en) 2008-10-23
JP2010523703A (ja) 2010-07-15
US8629305B2 (en) 2014-01-14

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