TWI474929B - Joined type sputtering target assembly and manufacturing method thereof - Google Patents

Joined type sputtering target assembly and manufacturing method thereof Download PDF

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TWI474929B
TWI474929B TW101104032A TW101104032A TWI474929B TW I474929 B TWI474929 B TW I474929B TW 101104032 A TW101104032 A TW 101104032A TW 101104032 A TW101104032 A TW 101104032A TW I474929 B TWI474929 B TW I474929B
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back tube
target
layer
sputtering target
preliminary
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TW101104032A
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Chinese (zh)
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TW201332777A (en
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Shih Hsun Chen
Chien Yao Huang
Chun Chieh Chang
Kent Jiann Der Wu
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Thintech Materials Technology Co Ltd
Han Tai Technology Co Ltd
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Description

接合式管狀濺鍍靶材及其製作方法Joint tubular sputtering target and manufacturing method thereof

本發明係關於一種接合式管狀靶材及其製作方法,特別是一種接合式管狀靶材與背管間具有結合穩定性之接合式管狀濺鍍靶材及其製作方法。The present invention relates to a joined tubular target and a method for fabricating the same, and more particularly to a bonded tubular sputtering target having a bonding stability between a bonded tubular target and a back tube, and a method of fabricating the same.

濺鍍,是將平面靶材或管狀靶材之標靶材料沉積到一預定基板上而形成薄膜之技術,典型的標靶材料包括有金、銀、鈦、鎢、鉬、鋁、銅、銅鋁合金、鋁鈮合金、鈦鎢合金、銦銅合金、銦鋅合金、錫鋅合金、二氧化矽或氮化鈦等,依照應用產業需求及成本考量,可將上述標靶材料製成平面靶材或管狀靶材以進行濺鍍作業。Sputtering is a technique of depositing a target material of a planar target or a tubular target onto a predetermined substrate to form a thin film. Typical target materials include gold, silver, titanium, tungsten, molybdenum, aluminum, copper, copper. Aluminum alloy, aluminum-bismuth alloy, titanium-tungsten alloy, indium-copper alloy, indium-zinc alloy, tin-zinc alloy, cerium oxide or titanium nitride, etc., according to the application industry needs and cost considerations, the above target materials can be made into planar targets Material or tubular target for sputtering.

請參照第1圖所示,習用平面靶材8包含一平面背板81、一接合層82及一標靶材料83,根據所欲選用的標靶材料83,選擇濕潤性佳的接合層82,將該標靶材料83穩定地結合於該平面背板81上。由於習用平面靶材8在磁控濺射製程中,其轟擊位置通常集中在切線磁場較強的區域,無法均勻地侵蝕該標靶材料83而造成濺鍍薄膜品質不穩定,因此,習用平面靶材8的使用率只能達到35~50%左右。Referring to FIG. 1 , the conventional planar target 8 includes a planar back plate 81 , a bonding layer 82 and a target material 83 . According to the target material 83 to be selected, the bonding layer 82 with good wettability is selected. The target material 83 is stably bonded to the planar back plate 81. Since the conventional planar target 8 is in the magnetron sputtering process, its bombardment position is usually concentrated in a region where the tangential magnetic field is strong, and the target material 83 cannot be uniformly eroded, resulting in unstable quality of the sputtering film. Therefore, the conventional planar target is used. The use rate of material 8 can only reach about 35~50%.

為改善習用平面靶材8之濺鍍品質不穩定及使用率低的問題,遂發展出管狀靶材,藉由該管狀靶材旋轉標靶材料進行濺鍍,使該管狀靶材之表面均勻侵蝕,而提高其濺鍍品質,又可均勻轟擊該標靶材料,進而提高該靶材使用率達70~85%以上。In order to improve the problem of unstable sputtering quality and low usage rate of the conventional planar target material 8, a tubular target material is developed, and the tubular target material is sputtered to cause uniform erosion of the surface of the tubular target material. By improving the sputtering quality, the target material can be uniformly bombarded, thereby increasing the utilization rate of the target by 70-85%.

請參照第2及3圖,係中華民國第I317763號「很長圓筒形濺鍍標靶及其製造方法」專利案所揭示之管狀靶材,該習用管狀靶材9包含一支持管91、一接合層92及一濺鍍標靶93,該支持管91係為不鏽鋼管或鈦管,以提供較佳之機械強度來支持該濺鍍標靶93,該接合層92係以銦作為黏附材料,增加該濺鍍標靶93與該支持管91之間的結合穩定度,避免習用管狀靶材9在使用過程中,該濺鍍標靶93與該支持管91之間相互脫離。Please refer to Figures 2 and 3, which are tubular targets disclosed in the Patent No. I317763 of the Republic of China, "The Very Long Cylindrical Sputtering Target and Its Manufacturing Method", the conventional tubular target 9 comprising a support tube 91, a a bonding layer 92 and a sputtering target 93. The support tube 91 is a stainless steel tube or a titanium tube to provide better mechanical strength to support the sputtering target 93. The bonding layer 92 is made of indium as an adhesion material. The bonding stability between the sputtering target 93 and the support tube 91 prevents the conventional tubular target 9 from being detached from each other during use.

然而,該支持管91或該濺鍍標靶93分別與該接合層92之間的濕潤性差,該專利前案係僅以超音波能量處理該接合層92,以增加該接合層92之濕潤性。惟,僅以超音波能量處理該接合層92,仍無法有效提高該接合層92與該濺鍍標靶93或與該支持管21之間的結合穩定性,在濺鍍所必需的升溫及降溫作業中,仍會發生該支持管91與該濺鍍標靶93相互脫離的問題。However, the support tube 91 or the sputter target 93 has poor wettability with the bonding layer 92, respectively. The prior patent only treats the bonding layer 92 with ultrasonic energy to increase the wettability of the bonding layer 92. . However, if the bonding layer 92 is treated only with ultrasonic energy, the bonding stability between the bonding layer 92 and the sputtering target 93 or the supporting tube 21 cannot be effectively improved, and the temperature rise and temperature required for sputtering are not required. During the operation, the problem that the support tube 91 and the sputtering target 93 are separated from each other still occurs.

本發明之主要目的係提供一種接合式管狀濺鍍靶材,其濺鍍靶材與背管間之結合穩定性佳者。SUMMARY OF THE INVENTION A primary object of the present invention is to provide a bonded tubular sputter target having excellent adhesion stability between the sputter target and the back tube.

本發明之次一目的係提供一種接合式管狀濺鍍靶材之製作方法,其係能夠提高濺鍍靶材與背管之結合穩定性者。A second object of the present invention is to provide a method of fabricating a bonded tubular sputtering target which is capable of improving the bonding stability of a sputtering target and a back tube.

為達到前述發明目的,本發明所運用之技術內容包含有:In order to achieve the foregoing object, the technical content of the present invention includes:

一種接合式管狀濺鍍靶材,係包含:一背管;一濺鍍靶胚,具有一內腔,該內腔係供容置該背管;及一輔助黏合層,係包含至少一硬焊銅層與一軟焊銦層,該輔助黏合層係結合於該背管與該濺鍍靶胚之間;其中該背管係由不鏽鋼、鈦、鈦合金、鉬或鉬合金製成的背管。A joint tubular sputtering target comprises: a back tube; a sputter target having an inner cavity for receiving the back tube; and an auxiliary adhesive layer comprising at least one brazing a copper layer and a soldered indium layer, the auxiliary adhesive layer is bonded between the back tube and the sputter target; wherein the back tube is a back tube made of stainless steel, titanium, titanium alloy, molybdenum or molybdenum alloy .

本發明之接合式管狀濺鍍靶材中,該硬焊銅層係一個,該硬焊銅層係結合於該背管之外表面或該濺鍍靶胚之內表面。In the jointed tubular sputtering target of the present invention, the brazing copper layer is one, and the brazing copper layer is bonded to the outer surface of the back tube or the inner surface of the sputter target.

本發明之接合式管狀濺鍍靶材中,該硬焊銅層係二個,該硬焊銅層係結合於該背管之外表面及該濺鍍靶胚之內表面。In the jointed tubular sputtering target of the present invention, the brazing copper layer is two, and the brazing copper layer is bonded to the outer surface of the backing tube and the inner surface of the sputter target.

本發明之接合式管狀濺鍍靶材中,該硬焊銅層之厚度為0.1~1.0微米。In the bonded tubular sputtering target of the present invention, the brazing copper layer has a thickness of 0.1 to 1.0 μm.

本發明之接合式管狀濺鍍靶材中,該輔助黏合層之厚度為0.3~0.5毫米。In the jointed tubular sputtering target of the present invention, the auxiliary adhesive layer has a thickness of 0.3 to 0.5 mm.

一種接合式管狀濺鍍靶材之製作方法,係包含:一前處理步驟,提供一背管及至少一濺鍍靶胚,對該背管之外表面及/或該濺鍍靶胚之內表面進行噴砂處理,使該背管之外表面及/或該濺鍍靶胚之內表面粗糙度為1.5~2.5微米;一硬焊步驟,係於該背管之外表面及/或該濺鍍靶胚之內表面,形成硬焊銅層;一濕潤步驟,於該背管、該濺鍍靶胚或該硬焊銅層上,分別形成一濕潤層,分別得到一預備背管及一預備靶胚;一總成步驟,將該至少一預備靶胚套設於該預備背管上,該至少一預備靶胚與該預備背管之間形 成至少一間隙;及一軟焊結合步驟,將熔融態銦填充至該預備背管及該預備靶胚之間隙中,形成一輔助黏合層,使該預備背管及該預備靶胚結合。A method for fabricating a bonded tubular sputtering target, comprising: a pre-processing step of providing a back tube and at least one sputter target, the outer surface of the back tube and/or the inner surface of the sputter target Sandblasting to make the outer surface of the back tube and/or the inner surface roughness of the sputter target 1.5 to 2.5 micrometers; a brazing step on the outer surface of the back tube and/or the sputtering target Forming a brazing copper layer on the inner surface of the embryo; forming a wetting layer on the back tube, the sputter target or the brazing copper layer to obtain a preliminary back tube and a preliminary target embryo respectively And an assembly step of arranging the at least one preliminary target embryo on the preparatory back tube, and forming a shape between the at least one preliminary target embryo and the preliminary back tube Forming at least one gap; and a soldering bonding step, filling molten indium into the gap between the preliminary back tube and the preliminary target embryo to form an auxiliary adhesive layer, and combining the preliminary back tube and the preliminary target embryo.

本發明之接合式管狀濺鍍靶材之製作方法中,該硬焊銅層可以選擇係以熱噴焊方式、電鍍或非電鍍方式形成。In the method of fabricating the junction-type tubular sputtering target of the present invention, the brazing copper layer may be selectively formed by thermal spray welding, electroplating or electroless plating.

本發明之接合式管狀濺鍍靶材之製作方法中,該濕潤層係以塗覆、電鍍或非電鍍方式形成,較佳係另以超音波能量與電刷處理該濕潤層,該濕潤層之厚度較佳為0.2~0.8微米。In the method for fabricating the junction-type tubular sputtering target of the present invention, the wet layer is formed by coating, electroplating or electroless plating, and preferably the wet layer is treated by ultrasonic energy and a brush. The thickness is preferably from 0.2 to 0.8 μm.

本發明之接合式管狀濺鍍靶材之製作方法中,該總成步驟中,該預備背管外表面間隔放置至少三條區隔線,該區隔線之直徑較佳為0.3~0.5毫米。In the manufacturing method of the jointed tubular sputtering target of the present invention, in the assembly step, the outer surface of the preliminary back tube is spaced apart by at least three partition lines, and the diameter of the partition line is preferably 0.3 to 0.5 mm.

本發明之接合式管狀濺鍍靶材之製作方法中,該總成步驟中,該預備靶胚之間放置一環狀墊片。In the method for producing a jointed tubular sputtering target of the present invention, in the assembly step, an annular gasket is placed between the preliminary target embryos.

本發明之接合式管狀濺鍍靶材之製作方法中,該前處理步驟中,該硬焊步驟及該濕潤步驟後,較佳係另進行一拋光步驟,將該硬焊銅層或該濕潤層之粗糙度處理至小於2.5微米。In the method for fabricating the bonded tubular sputtering target of the present invention, in the pre-treatment step, after the brazing step and the wetting step, preferably, a polishing step is performed to bond the brazing copper layer or the wetting layer. The roughness is treated to less than 2.5 microns.

為讓本發明之上述及其他目的、特徵及優點能更明顯易懂,下文特舉本發明之較佳實施例,並配合所附圖式,作詳細說明如下:The above and other objects, features and advantages of the present invention will become more <RTIgt;

請參照第4圖所示,本發明之接合式管狀濺鍍靶材,包含有一背管1、至少一濺鍍靶胚2及一輔助黏合層3,該濺鍍靶胚2係套設於該背管1之外周壁,且該背管1與該濺鍍靶胚2之間係以該輔助黏合層3結合。Referring to FIG. 4, the jointed tubular sputtering target of the present invention comprises a back tube 1, at least one sputter target 2 and an auxiliary adhesive layer 3. The sputter target 2 is sleeved on the The outer peripheral wall of the back tube 1 and the back tube 1 and the sputter target 2 are joined by the auxiliary adhesive layer 3.

該背管1具有一內腔11及一外表面12,該內腔11係供容置加熱裝置或總成架,以便本發明接合式管狀濺鍍靶材之製作,該外表面12係結合該輔助黏合層3。舉例而言,該背管1可以選擇為不鏽鋼、鈦、鈦合金、鉬或鉬合金等材料製成,但不以此為限;本實施例係選擇為機械強度較高之不鏽鋼,以供支持該濺鍍靶胚2。The back tube 1 has an inner cavity 11 and an outer surface 12 for receiving a heating device or an assembly frame for fabricating the bonded tubular sputtering target of the present invention. Auxiliary bonding layer 3. For example, the back pipe 1 may be selected from materials such as stainless steel, titanium, titanium alloy, molybdenum or molybdenum alloy, but not limited thereto; this embodiment is selected as stainless steel with high mechanical strength for support. The sputter target 2 is sputtered.

該濺鍍靶胚2具有一內腔21及一內表面22,該內腔21係供容置該背管1,該內表面22係與該輔助黏合層3結合。舉例而言,本實施例之濺鍍靶胚2可以係任何濺鍍靶材,如金、銀、鈦、鎢、鉬、鋁、銅、銅鋁合金、鋁鈮合金、鈦鎢合金、銦銅合金、銦鋅合金、錫鋅合金、二氧化矽或氮化鈦等濺鍍材料。本實施例之背管1具有一外徑h1,該濺鍍靶胚2具有一內徑h2,該背管1之外徑h1係小於該濺鍍靶胚2之內徑h2,且該背管1之外徑h1與該濺鍍靶胚2之內徑h2差為0.3~0.5毫米(mm),使該背管1容置於該濺鍍靶胚2之內腔21時,該背管1及該濺鍍靶胚2之間具有一間隙。The sputter target 2 has an inner cavity 21 and an inner surface 22 for receiving the back tube 1, and the inner surface 22 is coupled to the auxiliary adhesive layer 3. For example, the sputter target 2 of the embodiment may be any sputter target such as gold, silver, titanium, tungsten, molybdenum, aluminum, copper, copper aluminum alloy, aluminum tantalum alloy, titanium tungsten alloy, indium copper. Sputtering materials such as alloys, indium-zinc alloys, tin-zinc alloys, cerium oxide or titanium nitride. The back tube 1 of the embodiment has an outer diameter h1, the sputter target 2 has an inner diameter h2, and the outer diameter h1 of the back tube 1 is smaller than the inner diameter h2 of the sputter target 2, and the back tube The difference between the outer diameter h1 of 1 and the inner diameter h2 of the sputter target 2 is 0.3-0.5 mm (mm), so that the back tube 1 is accommodated in the inner cavity 21 of the sputter target 2, the back tube 1 There is a gap between the sputter target 2 and the sputter target 2.

該輔助黏合層3,係包含至少一硬焊銅層31與一軟焊銦層32,該輔助黏合層3係結合於該背管1與該濺鍍靶胚2之間。更詳言之,該輔助黏合層3之硬焊銅層31可以選擇結合於該背管1之外表面12及/或該濺鍍靶胚2之內表面22,且該軟焊銦層32之位置係根據該硬焊銅層31所結合的位置設置;請參照第4圖所示,該硬焊銅層31係結合於該背管1之外表面12,則該軟焊銦層32結合於該硬焊銅層31與該濺鍍靶胚2之間;或者,如第5圖所示,該硬焊銅層31係結合於該濺鍍靶胚2之內表面22,則該軟焊銦層32結合於該硬焊銅層31與該背管1之間;又,如第6圖所示,該硬焊銅層31係分別結合於該背管1之外表面12或該濺鍍靶胚2之內表面22,則該軟焊銦層32係結合於該背管1及該濺鍍靶胚2上之二硬焊銅層31之間。藉由該硬焊銅層31,增加該軟焊銦層32與該背管1或該濺鍍靶胚2之間的濕潤性,係具有增加該背管1與該濺鍍靶胚2之結合穩定性之功效。The auxiliary bonding layer 3 comprises at least one brazing copper layer 31 and a solder indium layer 32. The auxiliary bonding layer 3 is bonded between the backing tube 1 and the sputter target 2 . More specifically, the brazing copper layer 31 of the auxiliary bonding layer 3 may be selectively bonded to the outer surface 12 of the backing tube 1 and/or the inner surface 22 of the sputter target 2, and the solder indium layer 32 is The position is set according to the position at which the brazing copper layer 31 is bonded; as shown in FIG. 4, the brazing copper layer 31 is bonded to the outer surface 12 of the back tube 1, and the solder indium layer 32 is bonded to The brazing copper layer 31 is interposed between the sputter target 2; or, as shown in FIG. 5, the brazing copper layer 31 is bonded to the inner surface 22 of the sputter target 2, and the soldered indium is The layer 32 is bonded between the brazing copper layer 31 and the back tube 1; further, as shown in FIG. 6, the brazing copper layer 31 is bonded to the outer surface 12 of the back tube 1 or the sputtering target, respectively. The inner surface 22 of the embryo 2 is bonded between the back tube 1 and the two brazing copper layers 31 on the sputter target 2 . Increasing the wettability between the solder indium layer 32 and the back tube 1 or the sputter target 2 by the brazing copper layer 31, thereby increasing the combination of the back tube 1 and the sputter target 2 The effect of stability.

請參照第7圖,本發明之接合式管狀濺鍍靶材係由下列步驟所製成:一前處理步驟S1、一硬焊步驟S2、一濕潤步驟S3、一總成步驟S4及一軟焊結合步驟S5。Referring to FIG. 7, the jointed tubular sputtering target of the present invention is produced by the following steps: a pre-processing step S1, a brazing step S2, a wetting step S3, an assembly step S4, and a soldering process. Combined with step S5.

該前處理步驟S1,係提供一背管1及至少一濺鍍靶胚2,對該背管1之外表面12及/或該濺鍍靶胚2之內表面22進行噴砂處理,使該背管1之外表面12及/或該濺鍍靶胚2之內表面22粗糙度為1.5~2.5微米(μm)。更詳言之,該背管1之外表面12及/或該濺鍍靶胚2之內表面22的粗糙度(Ra)為1.5~2.5 μm,若粗糙度小於1.5 μm,則該背管1或該濺鍍靶胚2之表面物理附著力不足,而無法提供該硬焊銅層31或該軟焊銦層32足夠的結合表面積,若粗糙度大於2.5 μm,則該背管1或該濺鍍靶胚2之表面凹凸差異過大,不利該硬焊銅層31或該軟焊銦層32之結合;本實施例係取粒徑為60 μm之氧化鋁粉,以噴砂方式處理該背管1外表面12,使該背管1外表面12之粗糙度為2.0 μm。The pre-processing step S1 provides a back tube 1 and at least one sputter target 2, and the outer surface 12 of the back tube 1 and/or the inner surface 22 of the sputter target 2 are sandblasted to make the back The outer surface 12 of the tube 1 and/or the inner surface 22 of the sputter target 2 has a roughness of 1.5 to 2.5 micrometers (μm). More specifically, the outer surface 12 of the back tube 1 and/or the inner surface 22 of the sputter target 2 have a roughness (Ra) of 1.5 to 2.5 μm, and if the roughness is less than 1.5 μm, the back tube 1 Or the surface of the sputter target 2 has insufficient physical adhesion, and the brazing copper layer 31 or the solder indium layer 32 cannot be provided with a sufficient bonding surface area. If the roughness is greater than 2.5 μm, the back tube 1 or the splash The surface unevenness of the target metal 2 is too large, which is disadvantageous to the combination of the brazing copper layer 31 or the solder indium layer 32. In this embodiment, the alumina powder having a particle size of 60 μm is taken, and the back tube 1 is treated by sand blasting. The outer surface 12 has a roughness of the outer surface 12 of the back tube 1 of 2.0 μm.

本實施例之背管1係選擇為結構強度足以支持該濺鍍靶胚2之SUS304或SUS316不鏽鋼材,但不以此為限。本發明之濺鍍靶胚2可以係任何作為濺鍍用之靶材,如金、銀、鈦、鎢、鉬、鋁、銅、錫、鋅、銅鋁合金、鋁鈮合金、鈦鎢合金、銦銅合金、銦鋅合金、錫鋅合金、二氧化矽或氮化鈦。The back pipe 1 of the present embodiment is selected as a SUS304 or SUS316 stainless steel material having a structural strength sufficient to support the sputter target 2, but is not limited thereto. The sputtering target 2 of the present invention may be any target for sputtering, such as gold, silver, titanium, tungsten, molybdenum, aluminum, copper, tin, zinc, copper aluminum alloy, aluminum-bismuth alloy, titanium tungsten alloy, Indium copper alloy, indium zinc alloy, tin zinc alloy, ceria or titanium nitride.

該硬焊步驟S2,係於該背管1之外表面12及/或該濺鍍靶胚2之內表面22,形成硬焊銅層31。舉例而言,該硬焊銅層31可以選擇以熱噴焊方式、電鍍或非電鍍(熱浸)等方式形成,本實施例較佳係以熱噴焊方式將一銅粉噴塗於該背管1外表面12,形成該硬焊銅層31,其中,該銅粉之粒徑較佳為可通過篩目為400#之大小,即可以熱噴焊方式附著於該背管1之外表面12。The brazing step S2 is performed on the outer surface 12 of the back tube 1 and/or the inner surface 22 of the sputter target 2 to form a brazing copper layer 31. For example, the brazing copper layer 31 may be formed by thermal spraying, electroplating or electroless plating (hot dip). In this embodiment, a copper powder is sprayed on the back tube by thermal spray welding. The outer surface 12 is formed with the brazing copper layer 31. The copper powder preferably has a particle size of 400#, that is, it can be thermally spray-bonded to the outer surface of the back tube 1. .

本實施例之硬焊銅層31厚度較佳為0.1~1.0 μm,該硬焊銅層31之厚度若不及0.1 μm,則緻密度不足且無法完全被覆於該背管1或該濺鍍靶胚2之表面,而無法有效提高該硬焊銅層31與該背管1或與該濺鍍靶胚2之結合強度,若其厚度大於1.0 μm,則增加該接合式管狀濺鍍靶材之製作成本。The thickness of the brazing copper layer 31 of the present embodiment is preferably 0.1 to 1.0 μm. If the thickness of the brazing copper layer 31 is less than 0.1 μm, the density is insufficient and cannot be completely covered by the back tube 1 or the sputtering target. The surface of the second surface cannot effectively increase the bonding strength between the brazing copper layer 31 and the backing tube 1 or the sputtering target 2. If the thickness is greater than 1.0 μm, the bonding tubular sputtering target is increased. cost.

該濕潤步驟S3,於該背管1、該濺鍍靶胚2或該硬焊銅層31上,分別形成一濕潤層321,分別得到一預備背管及一預備靶胚。更詳言之,該濕潤層321之材料係與該軟焊銦層32相同,該濕潤層321係為提高該軟焊銦層32與該硬焊銅層31之濕潤性(又稱金屬化作用),以增加該硬焊銅層31與該軟焊銦層32之結合強度。本實施例之該濕潤層321可以選擇以塗覆、電鍍或非電鍍(熱浸)等方式形成,本實施例係將該背管1及該濺鍍靶胚2加熱至170~190℃,並以一銦塊材直接接觸所欲濕潤之表面,如該硬焊銅層31及該濺鍍靶胚2之內表面,即可將銦塊材熔融並塗覆至該背管1之外表面12、該濺鍍靶胚2之內表面22或該硬焊銅層31上。另外,該濕潤層321較佳係以超音波能量與電刷處理,能更進一步增加該濕潤層321分別與該背管1、該濺鍍靶胚2或該硬焊銅層31的濕潤性,促進該濕潤層321與該背管1外表面12,及該濕潤層321與該濺鍍靶胚2內表面22之結合穩定性。完成塗覆作業並待該濕潤層321冷卻後,得到該預備背管及該預備靶胚,即可進行後續步驟。In the wetting step S3, a wet layer 321 is formed on the back tube 1, the sputter target 2 or the brazing copper layer 31, respectively, to obtain a preliminary back tube and a preliminary target embryo. More specifically, the wet layer 321 is made of the same material as the solder indium layer 32. The wet layer 321 is used to improve the wettability of the solder indium layer 32 and the brazing copper layer 31 (also referred to as metallization). ) to increase the bonding strength between the brazing copper layer 31 and the solder indium layer 32. The wet layer 321 of the embodiment may be selectively formed by coating, electroplating or electroless plating (hot dip). In this embodiment, the back tube 1 and the sputter target 2 are heated to 170 to 190 ° C, and The indium block can be melted and applied to the outer surface of the back tube 1 by directly contacting an indium block with the surface to be wetted, such as the brazing copper layer 31 and the inner surface of the sputter target 2. The inner surface 22 of the target 2 or the brazing copper layer 31 is sputtered. In addition, the wet layer 321 is preferably treated by ultrasonic energy and brush, and the wettability of the wet layer 321 with the back tube 1, the sputtering target 2 or the brazing copper layer 31 can be further increased. The bonding stability between the wet layer 321 and the outer surface 12 of the back tube 1 and the wet layer 321 and the inner surface 22 of the sputter target 2 are promoted. After the coating operation is completed and the wet layer 321 is cooled, the preliminary back tube and the preliminary target embryo are obtained, and the subsequent steps can be performed.

該濕潤層321之厚度較佳係0.2~0.8 μm,該濕潤層321之厚度若不及0.2 μm,則無法有效提高該背管1與該濺鍍靶胚2之結合強度,且無法承受不同濺鍍靶材對於銦的膨脹係數差異所產生的變形量,若其厚度大於0.8 μm,則增加該接合式管狀濺鍍靶材之製作成本。The thickness of the wet layer 321 is preferably 0.2-0.8 μm. If the thickness of the wet layer 321 is less than 0.2 μm, the bonding strength between the back tube 1 and the sputter target 2 cannot be effectively improved, and the sputtering cannot be withstood. The amount of deformation of the target for the difference in the expansion coefficient of indium, if the thickness is greater than 0.8 μm, increases the manufacturing cost of the bonded tubular sputtering target.

請參照第8圖所示,該硬焊步驟S2及該濕潤步驟S3後,較佳另進行一拋光步驟S31,係將該硬焊銅層31及/或該濕潤層321之粗糙度拋光至小於2.5 μm以下。更詳言之,該拋光步驟S31係以編號小於#325之砂紙拋光,但不限定於此,藉由該拋光步驟S31,將該硬焊銅層31及/或該濕潤層321之粗糙度處理至小於2.5 μm以下,可以提供該背管1與該濺鍍靶胚2之間足夠的機械接合面,又不影響超音波與電刷處理時的接觸性,並使結合強度增加。Referring to FIG. 8, after the brazing step S2 and the wetting step S3, a polishing step S31 is preferably performed to polish the roughness of the brazing copper layer 31 and/or the wetting layer 321 to less than 2.5 μm or less. More specifically, the polishing step S31 is performed by sandpaper with a number less than #325, but is not limited thereto, and the roughness of the brazing copper layer 31 and/or the wet layer 321 is treated by the polishing step S31. To less than 2.5 μm, a sufficient mechanical joint between the back tube 1 and the sputter target 2 can be provided without affecting the contact between the ultrasonic wave and the brush treatment, and the bonding strength is increased.

該總成步驟S4,將該至少一預備靶胚套設於該預備背管上,該至少一預備靶胚與該預備背管之間形成至少一間隙。更詳言之,沿該預備背管之軸向上,於該預備背管外表面11間隔放置至少三條直徑為0.3~0.5 mm之區隔線,該區隔線可以選擇為鎢線或銅線,以供固定該預備靶胚於該預備背管上,並用以提供該預備背管及該預備靶胚之間的間隙距離;本實施例之間隔線3係銅線。In the assembly step S4, the at least one preliminary target embryo is sleeved on the preparatory back tube, and at least one gap is formed between the at least one preliminary target embryo and the preliminary back tube. More specifically, at least three partitions having a diameter of 0.3 to 0.5 mm are spaced apart from the outer surface 11 of the preliminary back tube in the axial direction of the preliminary back tube, and the partition line may be selected as a tungsten wire or a copper wire. For fixing the preliminary target embryo on the preparatory back tube, and for providing a gap distance between the preliminary back tube and the preliminary target embryo; the spacer line 3 of the embodiment is a copper wire.

各預備靶胚之間放置一環形墊片(係可由聚四氟乙烯、聚亞胺、聚酮、聚醚碸、聚乙烯對苯二甲酸酯、氟乙烯丙烯共聚物、撓性環氧樹脂或橡膠等材質製成),該環形墊片之厚度較佳為0.5 mm,該環形墊片之外徑係略大於該預備靶胚之外徑,以便使用者在該接合式管狀濺鍍靶材完成後,將該環形墊片拆除;本實施例係選擇厚度為0.5 mm之聚四氟乙烯環形墊片。本實施例之總成步驟S4可以選擇將數個預備靶胚及數個環形墊片對齊,以一夾持具固定成一長筒狀,或者可以將該數個預備靶胚及該環形墊片各別套入該預備背管上,並將之對齊形成一長筒狀;本實施例係選擇以該夾持具將數個預備靶胚及環形墊片固定後,以便將該數個預備靶胚預先加熱備用。A ring gasket is placed between each of the prepared target embryos (which may be made of polytetrafluoroethylene, polyimine, polyketone, polyether oxime, polyethylene terephthalate, fluoroethylene propylene copolymer, flexible epoxy resin). Or a material such as rubber, the thickness of the annular gasket is preferably 0.5 mm, and the outer diameter of the annular gasket is slightly larger than the outer diameter of the preliminary target for the user to engage in the tubular sputtering target. After completion, the annular gasket is removed; in this embodiment, a polytetrafluoroethylene annular gasket having a thickness of 0.5 mm is selected. In the assembly step S4 of the embodiment, a plurality of preliminary target embryos and a plurality of annular spacers may be aligned, and a clamp is fixed into a long cylindrical shape, or the plurality of preliminary target embryos and the annular spacers may be respectively Do not fit into the preparatory back tube and align it to form a long cylindrical shape; in this embodiment, the plurality of preliminary target embryos and the annular spacer are selected by the clamping device to fix the plurality of preliminary target embryos. Preheated for use.

該軟焊結合步驟S5,將熔融態銦填充至該預備背管及該預備靶胚之間隙中,形成一輔助黏合層32,以供該預備背管及該預備靶胚結合。本實施例係將該預備背管固定於一總成架上,並加熱該預備背管至170~190℃,以維持該熔融態銦的流動性,使熔融態銦順利填充至該預備背管與該預備靶胚之間隙中,形成該輔助黏合層32,待該熔融態銦填充完成,並於室溫下靜置冷卻形成該輔助黏合層32。由於銦與銅之間的濕潤度佳,本發明係藉由該背管1及/或該濺鍍靶胚2上的硬焊銅層31,增加該背管1及該濺鍍靶胚2與該輔助黏合層3之結合強度,係能夠達到提升該接合式管狀濺鍍靶材之整體結合穩定性功效。The soldering is combined with the step S5 to fill the molten indium into the gap between the preliminary backing tube and the preliminary target embryo to form an auxiliary adhesive layer 32 for the preparation of the preliminary back tube and the preliminary target embryo. In this embodiment, the preparatory back pipe is fixed on an assembly frame, and the preliminary back pipe is heated to 170 to 190 ° C to maintain the fluidity of the molten indium, so that the molten indium is smoothly filled to the preliminary back pipe. In the gap with the preliminary target, the auxiliary adhesive layer 32 is formed, and the molten indium is filled, and the auxiliary adhesive layer 32 is formed by standing and cooling at room temperature. Due to the good wettability between indium and copper, the present invention increases the back tube 1 and the sputter target 2 by the back tube 1 and/or the brazing copper layer 31 on the sputter target 2 The bonding strength of the auxiliary bonding layer 3 can improve the overall bonding stability of the bonded tubular sputtering target.

下列為本發明接合式管狀濺鍍靶材之製作方法之較佳實施例詳細操作步驟:The following is a detailed operation of the preferred embodiment of the method for fabricating the bonded tubular sputtering target of the present invention:

1. 先提供一SUS304不鏽鋼背管及一鋁濺鍍靶胚,將該SUS304不鏽鋼背管之內表面及該鋁濺鍍靶胚之外表面,以揮發性溶劑(如酒精)擦拭,再以高壓空氣吹拂該等表面,去除殘留粉塵。1. First provide a SUS304 stainless steel back tube and an aluminum sputter target, the inner surface of the SUS304 stainless steel back tube and the outer surface of the aluminum sputter target, wipe with a volatile solvent (such as alcohol), and then with high pressure The air blows the surfaces to remove residual dust.

2. 以粒徑為80 μm之氧化鋁粉,對該SUS304不鏽鋼背管之外表面進行噴砂處理,其噴砂壓力設定為7 kgf/cm2 ,該SUS304不鏽鋼背管之粗糙度係2.0 μm,再以揮發性溶劑及高壓空氣去除該SUS304不鏽鋼背管外表面之殘留粉塵。2. The outer surface of the SUS304 stainless steel back pipe is sandblasted with alumina powder having a particle size of 80 μm. The blasting pressure is set to 7 kgf/cm 2 , and the roughness of the SUS304 stainless steel back pipe is 2.0 μm. The residual dust on the outer surface of the SUS304 stainless steel back pipe was removed with a volatile solvent and high pressure air.

3. 以粒徑為30 μm之銅粉對該SUS304不鏽鋼背管之外表面進行高速火焰熔射之熱噴塗,形成一硬焊銅層於該SUS304不鏽鋼背管外表面,且該硬焊銅層之粗糙度係2.5 μm,再以揮發性溶劑及高壓空氣去除該SUS304不鏽鋼背管外表面之殘留粉塵。3. The outer surface of the SUS304 stainless steel back tube is thermally sprayed by high-speed flame spraying with a copper powder having a particle size of 30 μm to form a brazing copper layer on the outer surface of the SUS304 stainless steel back tube, and the brazing copper layer The roughness is 2.5 μm, and the residual dust on the outer surface of the SUS304 stainless steel back pipe is removed by a volatile solvent and high-pressure air.

4. 以粒徑為60 μm之氧化鋁粉對該鋁濺鍍靶胚進行噴砂處理,其噴砂壓力設定為7 kgf/cm2 ,使該鋁濺鍍靶胚之粗糙度係2.5 μm,再以揮發性溶劑及高壓空氣去除該鋁濺鍍靶胚內表面之殘留粉塵。4. The aluminum sputter target is blasted with alumina powder with a particle size of 60 μm. The blasting pressure is set to 7 kgf/cm 2 , and the roughness of the aluminum sputter target is 2.5 μm. Volatile solvent and high pressure air remove residual dust from the inner surface of the aluminum sputter target.

5.以加熱線圈纏繞該鋁濺鍍靶胚,並以隔熱毯包覆該鋁濺鍍靶胚,將該鋁濺鍍靶胚加熱至180℃,再以塗覆方式將銦塗覆於該鋁濺鍍靶胚之內表面,形成一濕潤層,並以超音波處理使該濕潤層之濕潤性增加,且維持該鋁濺鍍靶胚於180℃之溫度下,以供後續操作。5. winding the aluminum sputter target with a heating coil, coating the aluminum sputter target with a heat insulation blanket, heating the aluminum sputter target to 180 ° C, and applying indium to the coating The aluminum sputters the inner surface of the target to form a wetting layer, and the wettability of the wet layer is increased by ultrasonic treatment, and the aluminum sputter target is maintained at a temperature of 180 ° C for subsequent operation.

6.將一IR加熱器之數支加熱棒置入該SUS304不鏽鋼背管之內腔,並將該數支加熱棒貼合於該SUS304不鏽鋼背管之內表面,將該SUS304不鏽鋼背管加熱至溫度180℃,再以塗覆方式將銦塗覆於該SUS304不鏽鋼背管之外表面,形成另一濕潤層,並以超音波處理使該濕潤層之濕潤性增加,該SUS304不鏽鋼背管靜置於室溫冷卻,以供後續操作。6. Place a plurality of IR heater heater rods into the inner cavity of the SUS304 stainless steel back tube, and attach the plurality of heating rods to the inner surface of the SUS304 stainless steel back tube, and heat the SUS304 stainless steel back tube to At a temperature of 180 ° C, indium was applied to the outer surface of the SUS304 stainless steel back tube by coating to form another wetting layer, and the wettability of the wet layer was increased by ultrasonic treatment, and the SUS304 stainless steel back tube was allowed to stand. Cool at room temperature for subsequent operations.

7.沿該SUS304不鏽鋼背管之軸向,將四條銅線貼合於該SUS304不鏽鋼背管之外表面,且各四條銅線之間具有相等間距,並該SUS304不鏽鋼背管固定於一總成架,將一環形墊片套入該SUS304不鏽鋼背管作為底層之防漏墊片,並以該IR加熱器對該SUS304不鏽鋼背管之內表面加熱至180℃。7. Along the axial direction of the SUS304 stainless steel back pipe, four copper wires are attached to the outer surface of the SUS304 stainless steel back pipe, and the four copper wires are equally spaced, and the SUS304 stainless steel back pipe is fixed to an assembly. A ring gasket was placed in the SUS304 stainless steel back pipe as a bottom leakage preventing gasket, and the inner surface of the SUS304 stainless steel back pipe was heated to 180 ° C by the IR heater.

8.將該鋁濺鍍靶胚套合於該SUS304不鏽鋼背管之外,該鋁濺鍍靶胚與該SUS304不鏽鋼背管之間形成一間隙,以加熱線圈纏繞該鋁濺鍍靶胚,並以隔熱毯包覆該鋁濺鍍靶胚,將該鋁濺鍍靶胚加熱至180℃,再將一熔融態銦緩緩填充至該間隙,填充過程中以震動或拍打方式,將填入該間隙內的熔融態銦之氣泡趕出,待完成填充作業後,停止加熱作業並靜置冷卻,獲得一接合式鋁管狀濺鍍 靶材。8. The aluminum sputter target embryo is sleeved outside the SUS304 stainless steel back tube, and a gap is formed between the aluminum sputter target and the SUS304 stainless steel back tube to wrap the aluminum sputter target embryo with a heating coil, and The aluminum sputter target is coated with a heat insulation blanket, the aluminum sputter target is heated to 180 ° C, and a molten indium is slowly filled into the gap, and the filling process is filled by vibration or tapping. The bubbles of molten indium in the gap are ejected, and after the filling operation is completed, the heating operation is stopped and the cooling is allowed to stand to obtain a joint aluminum tubular sputtering. Target.

請參照附件一之(a)至(e),係以如第1表所示之條件操作,以酒精棉紙擦拭後觀察,該硬焊銅層或該不鏽鋼背管之表面分別與該濕潤層的金屬化效果。Please refer to (a) to (e) of Annex 1 for the conditions shown in Table 1. After wiping with alcohol paper, observe the surface of the brazing copper layer or the stainless steel back tube and the wetting layer. Metallization effect.

由附件一可知,(a)及(c)係未經擦拭前之金屬化表面,而(b)及(d)係經酒精棉紙擦拭後的結果,比較(b)及(d)可以發現形成於該硬焊銅層之濕潤層的結合強度較高,不會因酒精擦拭而脫落,並且將(b)與(a)相較,亦能夠維持其金屬化的效果,(a)及(b)並無明顯差異;反觀,直接於該不鏽鋼板表面形成該銦的濕潤層者,經過擦拭後,該銦的濕潤層便脫落,而裸露出該不鏽鋼板之外表面,無法維持較佳的結合強度。As can be seen from Annex I, (a) and (c) are the metallized surfaces before wiping, and (b) and (d) are the results of wiping with alcohol paper. Comparing (b) and (d) can be found. The wetted layer formed on the brazing copper layer has a high bonding strength, does not fall off due to alcohol wiping, and can maintain the metallization effect of (b) compared with (a), (a) and ( b) there is no significant difference; on the other hand, if the wet layer of the indium is formed directly on the surface of the stainless steel plate, after the wiping, the wet layer of the indium is peeled off, and the outer surface of the stainless steel plate is exposed, and the better is not maintained. Bond strength.

為明顯比較該硬焊銅層所增進該不鏽鋼板表面與該濕潤層之間的結合效果,附件一之(e)係分別以不同操作步驟,處理同一塊不鏽鋼板,依圖面所示,其左方區域之處理步驟同(a),而右方區域之處理步驟同(c),同時對左、右二區域之不鏽鋼板表面擦拭後,可明顯看出由箭頭所指左、右二區域之交界。In order to significantly compare the bonding effect between the surface of the stainless steel plate and the wet layer by the brazing copper layer, the first stainless steel plate is treated by different steps in the first step (e) of the accessory, as shown in the figure. The processing steps in the left region are the same as (a), and the processing steps in the right region are the same as (c). After wiping the surface of the stainless steel plates in the left and right regions, the left and right regions indicated by the arrows are clearly visible. The junction.

由此可知,本發明之接合式管狀濺鍍靶材,係能夠藉由該硬焊銅層分別與該背管、該濺鍍靶胚與該輔助黏合層之較佳結合強度,而更進一步強化該等濺鍍靶材與該不鏽鋼背管之穩定結合之功效,避免在進行濺鍍作業過程發生脫落的情形。It can be seen that the junction-type tubular sputter target of the present invention can be further strengthened by the better bonding strength between the brazing copper layer and the back tube, the sputter target and the auxiliary adhesive layer. The effect of the stable combination of the sputter target and the stainless steel back tube avoids the occurrence of falling off during the sputtering operation.

本發明之接合式管狀濺鍍靶材,其濺鍍靶材與背管間係藉由一硬焊銅層而達到較佳結合穩定性,具有提高該濺鍍靶材與該背管之結合強度功效。The jointed tubular sputtering target of the present invention has a better bonding stability between the sputtering target and the back tube by a brazing copper layer, and has improved bonding strength between the sputtering target and the back tube. efficacy.

本發明之接合式管狀濺鍍靶材之製作方法,其係能夠藉由一道硬焊步驟,具有提高該等濺鍍靶材與該背管之結合穩定性功效。The method for fabricating the jointed tubular sputtering target of the present invention is capable of improving the binding stability of the sputtering target and the back tube by a brazing step.

雖然本發明已利用上述較佳實施例揭示,然其並非用以限定本發明,任何熟習此技藝者在不脫離本發明之精神和範圍之內,相對上述實施例進行各種更動與修改仍屬本發明所保護之技術範疇,因此本發明之保護範圍當視後附之申請專利範圍所界定者為準。While the invention has been described in connection with the preferred embodiments described above, it is not intended to limit the scope of the invention. The technical scope of the invention is protected, and therefore the scope of the invention is defined by the scope of the appended claims.

〔本發明〕〔this invention〕

1‧‧‧背管1‧‧‧ Back tube

11‧‧‧內腔11‧‧‧ lumen

12‧‧‧外表面12‧‧‧ outer surface

2‧‧‧濺鍍靶胚2‧‧‧Splatter target

21‧‧‧內腔21‧‧‧ lumen

22‧‧‧內表面22‧‧‧ inner surface

3‧‧‧輔助黏合層3‧‧‧Auxiliary bonding layer

31‧‧‧硬焊銅層31‧‧‧ brazing copper layer

32‧‧‧軟焊銦層32‧‧‧Soft soldered indium layer

321‧‧‧濕潤層321‧‧‧ Wet layer

h1‧‧‧背管之外徑H1‧‧‧ outer diameter of the back tube

h2‧‧‧濺鍍靶胚之內徑H2‧‧‧Insert diameter of sputter target

S1‧‧‧前處理步驟S1‧‧‧Pre-processing steps

S2‧‧‧硬焊步驟S2‧‧‧ Hard soldering step

S3‧‧‧濕潤步驟S3‧‧‧ Wet step

S31‧‧‧拋光步驟S31‧‧‧ polishing step

S4‧‧‧總成步驟S4‧‧‧ assembly steps

S5‧‧‧軟焊結合步驟S5‧‧‧Soft soldering bonding step

〔習用〕[Use]

8‧‧‧習用平面靶材8‧‧‧Used flat targets

81‧‧‧平面背板81‧‧‧Flat backplane

82‧‧‧接合層82‧‧‧ joint layer

83‧‧‧標靶材料83‧‧‧ Target materials

9‧‧‧習用管狀靶材9‧‧‧Used tubular target

91‧‧‧支持管91‧‧‧Support tube

92‧‧‧接合層92‧‧‧ joint layer

93‧‧‧濺鍍標靶93‧‧‧Sputter target

第1圖:習用平面靶材8之側剖圖。Figure 1: A side cross-sectional view of a conventional planar target 8.

第2圖:習用管狀靶材9之側視圖。Figure 2: Side view of a conventional tubular target 9.

第3圖:習用管狀靶材9之側剖圖。Figure 3: A side cross-sectional view of a conventional tubular target 9.

第4圖:本發明之接合式管狀濺鍍靶材側剖圖(一)。Figure 4 is a side cross-sectional view (I) of the joined tubular sputtering target of the present invention.

第5圖:本發明之接合式管狀濺鍍靶材側剖圖(二)。Figure 5 is a side cross-sectional view (2) of the joined tubular sputtering target of the present invention.

第6圖:本發明之接合式管狀濺鍍靶材側剖圖(三)。Figure 6 is a side cross-sectional view (3) of the joined tubular sputtering target of the present invention.

第7圖:本發明接合式管狀濺鍍靶材之製作方法的步驟方塊圖(一)。Figure 7 is a block diagram (I) of the method for fabricating the bonded tubular sputtering target of the present invention.

第8圖:本發明接合式管狀濺鍍靶材之製作方法的步驟方塊圖(二)。Figure 8 is a block diagram (2) of the method for fabricating the bonded tubular sputtering target of the present invention.

附件一:以如第1表所示之不同處理條件之不鏽鋼板表面金屬化效果照片。Annex I: Photograph of the surface metallization effect of stainless steel plates with different processing conditions as shown in Table 1.

1...背管1. . . Back tube

11...內腔11. . . Inner cavity

12...外表面12. . . The outer surface

2...濺鍍靶胚2. . . Sputter target

21...內腔twenty one. . . Inner cavity

22...內表面twenty two. . . The inner surface

3...輔助黏合層3. . . Auxiliary adhesive layer

31...硬焊銅層31. . . Brazed copper layer

32...軟焊銦層32. . . Soft soldered indium layer

321...濕潤層321. . . Wet layer

h1...背管之外徑H1. . . Outer diameter of the back tube

h2...濺鍍靶胚之內徑H2. . . Splash target inner diameter

Claims (15)

一種接合式管狀濺鍍靶材,係包含:一背管;一濺鍍靶胚,具有一內腔,該內腔係供容置該背管;及一輔助黏合層,係包含至少一硬焊銅層與一軟焊銦層,該輔助黏合層係結合於該背管與該濺鍍靶胚之間;其中該背管係由不鏽鋼、鈦、鈦合金、鉬或鉬合金製成的背管。 A joint tubular sputtering target comprises: a back tube; a sputter target having an inner cavity for receiving the back tube; and an auxiliary adhesive layer comprising at least one brazing a copper layer and a soldered indium layer, the auxiliary adhesive layer is bonded between the back tube and the sputter target; wherein the back tube is a back tube made of stainless steel, titanium, titanium alloy, molybdenum or molybdenum alloy . 如申請專利範圍第1項所述之接合式管狀濺鍍靶材,其中該硬焊銅層係一個,該硬焊銅層係結合於該背管之外表面或該濺鍍靶胚之內表面。 The jointed tubular sputtering target according to claim 1, wherein the brazing copper layer is one, and the brazing copper layer is bonded to the outer surface of the back pipe or the inner surface of the sputter target . 如申請專利範圍第1項所述之接合式管狀濺鍍靶材,其中該硬焊銅層係二個,該硬焊銅層係結合於該背管之外表面及該濺鍍靶胚之內表面。 The jointed tubular sputtering target according to claim 1, wherein the brazing copper layer is two, and the brazing copper layer is bonded to the outer surface of the back tube and the sputter target surface. 如申請專利範圍第1項所述之接合式管狀濺鍍靶材,其中該硬焊銅層之厚度為0.1~1.0微米。 The joined tubular sputtering target according to claim 1, wherein the brazing copper layer has a thickness of 0.1 to 1.0 μm. 如申請專利範圍第1項所述之接合式管狀濺鍍靶材,其中該輔助黏合層之厚度為0.3~0.5毫米。 The jointed tubular sputtering target according to claim 1, wherein the auxiliary adhesive layer has a thickness of 0.3 to 0.5 mm. 一種接合式管狀濺鍍靶材之製作方法,係包含:一前處理步驟,提供一背管及至少一濺鍍靶胚,對該背管之外表面及/或該濺鍍靶胚之內表面進行噴砂處理,使該背管之外表面及/或該濺鍍靶胚之內表面粗糙度為1.5~2.5微米;一硬焊步驟,係於該背管之外表面及/或該濺鍍靶胚之 內表面,形成硬焊銅層;一濕潤步驟,於該背管、該濺鍍靶胚或該硬焊銅層上,分別形成一濕潤層,分別得到一預備背管及一預備靶胚;一總成步驟,將該至少一預備靶胚套設於該預備背管上,該至少一預備靶胚與該預備背管之間形成至少一間隙;及一軟焊結合步驟,將熔融態銦填充至該預備背管及該預備靶胚之間隙中,形成一輔助黏合層,使該預備背管及該預備靶胚結合。 A method for fabricating a bonded tubular sputtering target, comprising: a pre-processing step of providing a back tube and at least one sputter target, the outer surface of the back tube and/or the inner surface of the sputter target Sandblasting to make the outer surface of the back tube and/or the inner surface roughness of the sputter target 1.5 to 2.5 micrometers; a brazing step on the outer surface of the back tube and/or the sputtering target Embryo The inner surface forms a brazing copper layer; a wetting step, respectively forming a wetting layer on the back tube, the sputter target or the brazing copper layer to obtain a preliminary back tube and a preliminary target embryo; In the assembly step, the at least one preliminary target embryo is sleeved on the preliminary back tube, at least one gap is formed between the at least one preliminary target embryo and the preliminary back tube; and a solder bonding step is performed to fill the molten indium An auxiliary adhesive layer is formed in the gap between the preliminary back tube and the preliminary target embryo, and the preliminary back tube and the preliminary target embryo are combined. 如申請專利範圍第6項所述之接合式管狀濺鍍靶材之製作方法,該硬焊步驟及該濕潤步驟後,另進行一拋光步驟,將該硬焊銅層或該濕潤層之粗糙度處理至小於2.5微米。 The method for fabricating a bonded tubular sputtering target according to claim 6, wherein after the brazing step and the wetting step, a polishing step is performed to roughen the brazing copper layer or the wet layer. Processed to less than 2.5 microns. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,其中該硬焊銅層係以熱噴焊方式、電鍍或非電鍍方式形成。 The method of fabricating a bonded tubular sputtering target according to claim 6 or 7, wherein the brazing copper layer is formed by thermal spray welding, electroplating or electroless plating. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之結合方法,其中該濕潤層係銦。 The method of bonding a joined tubular sputtering target according to claim 6 or 7, wherein the wet layer is indium. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,其中該濕潤層係以塗覆、電鍍或非電鍍方式形成。 The method of fabricating a joined tubular sputtering target according to claim 6 or 7, wherein the wetted layer is formed by coating, electroplating or electroless plating. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,其中該濕潤層係另以超音波能量與電刷處理。 The method of fabricating a bonded tubular sputtering target according to claim 6 or 7, wherein the wetted layer is additionally treated with ultrasonic energy and a brush. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,其中該濕潤層之厚度為0.2~0.8微米。 The method for producing a joined tubular sputtering target according to claim 6 or 7, wherein the wet layer has a thickness of 0.2 to 0.8 μm. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,該總成步驟中,該預備背管外表面間隔放置至少三條區隔線。 The method of fabricating a joined tubular sputtering target according to claim 6 or 7, wherein in the assembly step, the outer surface of the preliminary back tube is spaced apart by at least three partition lines. 如申請專利範圍第13項所述之接合式管狀濺鍍靶材之製作方法,該區隔線之直徑為0.3~0.5毫米。 The method for manufacturing a jointed tubular sputtering target according to claim 13 is characterized in that the partition line has a diameter of 0.3 to 0.5 mm. 如申請專利範圍第6或7項所述之接合式管狀濺鍍靶材之製作方法,該總成步驟中,該預備靶胚之間放置一環狀墊片。The method of fabricating a joined tubular sputtering target according to claim 6 or 7, wherein in the assembly step, an annular spacer is placed between the preliminary target embryos.
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