TWI370133B - Process for preparing acylphosphanes and derivatives thereof - Google Patents

Process for preparing acylphosphanes and derivatives thereof

Info

Publication number
TWI370133B
TWI370133B TW095101582A TW95101582A TWI370133B TW I370133 B TWI370133 B TW I370133B TW 095101582 A TW095101582 A TW 095101582A TW 95101582 A TW95101582 A TW 95101582A TW I370133 B TWI370133 B TW I370133B
Authority
TW
Taiwan
Prior art keywords
phenyl
c4alkyl
halogen
alkyl
formula
Prior art date
Application number
TW095101582A
Other languages
English (en)
Chinese (zh)
Other versions
TW200631958A (en
Inventor
Reinhard H Sommerlade
Katharina Fritzsche
Walter Fischer
Original Assignee
Ciba Sc Holding Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Sc Holding Ag filed Critical Ciba Sc Holding Ag
Publication of TW200631958A publication Critical patent/TW200631958A/zh
Application granted granted Critical
Publication of TWI370133B publication Critical patent/TWI370133B/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/505—Preparation; Separation; Purification; Stabilisation
    • C07F9/5063—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
    • C07F9/5068—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure >P-Hal
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW095101582A 2005-01-17 2006-01-16 Process for preparing acylphosphanes and derivatives thereof TWI370133B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP05100253 2005-01-17

Publications (2)

Publication Number Publication Date
TW200631958A TW200631958A (en) 2006-09-16
TWI370133B true TWI370133B (en) 2012-08-11

Family

ID=34979152

Family Applications (1)

Application Number Title Priority Date Filing Date
TW095101582A TWI370133B (en) 2005-01-17 2006-01-16 Process for preparing acylphosphanes and derivatives thereof

Country Status (6)

Country Link
US (1) US7470819B2 (enExample)
EP (1) EP1838721B1 (enExample)
JP (1) JP5234912B2 (enExample)
AT (1) ATE538126T1 (enExample)
TW (1) TWI370133B (enExample)
WO (1) WO2006074983A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2029639B1 (en) * 2006-06-09 2012-02-29 DENTSPLY International Inc. Photopolymerizable compositions featuring novel amine accelerator for improved color stability and reduced polymerization stress thereby
EP2190903B1 (en) 2007-09-04 2012-04-04 Basf Se Cyclic phosphines as flame retardants
WO2010121387A1 (en) * 2009-04-20 2010-10-28 ETH Zürich Polymer nanoparticles
WO2012052147A1 (en) 2010-10-19 2012-04-26 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Process for the modification of polymers, in particular polymer nanoparticles
CN103282388B (zh) 2010-10-19 2017-02-15 马克斯·普朗克科学促进学会 用于制备聚合物纳米颗粒的超快速方法
ES2881686T3 (es) 2012-10-01 2021-11-30 Eth Zuerich Un procedimiento para la preparación de acilofosfanos
EP3296301A1 (en) 2016-09-19 2018-03-21 ETH Zürich A versatile process for the preparation of acylphosphines
EP3539924A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel vinyl phosphines and photo-initiators obtainable therefrom
WO2021146093A1 (en) * 2020-01-14 2021-07-22 University Of Vermont And State Agricultural College Methods of preparing primary phosphine products using lewis acid catalysts

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3443221A1 (de) * 1984-11-27 1986-06-05 ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld Bisacylphosphinoxide, ihre herstellung und verwendung
SE520727C2 (sv) * 1996-03-04 2003-08-19 Ciba Sc Holding Ag Alkylfenylbisacylfosfinoxid och fotoinitiatorblandningar
JP3975307B2 (ja) * 1998-06-18 2007-09-12 チッソ株式会社 ホスフィン類の製造法
SK286152B6 (sk) * 1998-11-30 2008-04-07 Ciba Specialty Chemicals Holding Inc. Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov
CA2454914A1 (en) 2001-08-21 2003-03-06 Ciba Specialty Chemicals Holding Inc. Bathochromic mono- and bis-acylphosphine oxides and sulfides and their use as photoinitiators
ATE435230T1 (de) 2002-12-04 2009-07-15 Ciba Holding Inc Verfahren zur synthese von cycloorganylphosphanen und von di(alkali/erdalkalimetall)oligophosphandiiden
CA2531318A1 (en) * 2003-07-18 2005-02-17 Ciba Specialty Chemicals Holding Inc. Process for preparing acylphosphanes and derivatives thereof
TW200523265A (en) * 2003-07-31 2005-07-16 Basf Ag A process for the preparation of acylphosphines
CN101065388B (zh) 2004-11-23 2011-12-21 西巴特殊化学品控股有限公司 制备酰基磷烷及其衍生物的方法

Also Published As

Publication number Publication date
TW200631958A (en) 2006-09-16
EP1838721B1 (en) 2011-12-21
JP5234912B2 (ja) 2013-07-10
JP2008526918A (ja) 2008-07-24
WO2006074983A1 (en) 2006-07-20
ATE538126T1 (de) 2012-01-15
US20080071115A1 (en) 2008-03-20
EP1838721A1 (en) 2007-10-03
US7470819B2 (en) 2008-12-30

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