TWI370133B - Process for preparing acylphosphanes and derivatives thereof - Google Patents
Process for preparing acylphosphanes and derivatives thereofInfo
- Publication number
- TWI370133B TWI370133B TW095101582A TW95101582A TWI370133B TW I370133 B TWI370133 B TW I370133B TW 095101582 A TW095101582 A TW 095101582A TW 95101582 A TW95101582 A TW 95101582A TW I370133 B TWI370133 B TW I370133B
- Authority
- TW
- Taiwan
- Prior art keywords
- phenyl
- c4alkyl
- halogen
- alkyl
- formula
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 abstract 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 4
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 abstract 4
- 229910052739 hydrogen Inorganic materials 0.000 abstract 4
- 239000001257 hydrogen Substances 0.000 abstract 4
- 238000005984 hydrogenation reaction Methods 0.000 abstract 4
- 229910052736 halogen Inorganic materials 0.000 abstract 3
- 150000002367 halogens Chemical class 0.000 abstract 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 3
- 125000006702 (C1-C18) alkyl group Chemical group 0.000 abstract 2
- 150000004982 aromatic amines Chemical class 0.000 abstract 2
- 235000010290 biphenyl Nutrition 0.000 abstract 2
- 239000004305 biphenyl Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 abstract 2
- 125000000623 heterocyclic group Chemical group 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000001624 naphthyl group Chemical group 0.000 abstract 2
- 239000003586 protic polar solvent Substances 0.000 abstract 2
- 125000004209 (C1-C8) alkyl group Chemical group 0.000 abstract 1
- 101150047265 COR2 gene Proteins 0.000 abstract 1
- 101100467189 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) QCR2 gene Proteins 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- -1 cyclic phenylphosphanes Chemical class 0.000 abstract 1
- IMDXZWRLUZPMDH-UHFFFAOYSA-N dichlorophenylphosphine Chemical class ClP(Cl)C1=CC=CC=C1 IMDXZWRLUZPMDH-UHFFFAOYSA-N 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/505—Preparation; Separation; Purification; Stabilisation
- C07F9/5063—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
- C07F9/5068—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure >P-Hal
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP05100253 | 2005-01-17 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW200631958A TW200631958A (en) | 2006-09-16 |
| TWI370133B true TWI370133B (en) | 2012-08-11 |
Family
ID=34979152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW095101582A TWI370133B (en) | 2005-01-17 | 2006-01-16 | Process for preparing acylphosphanes and derivatives thereof |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7470819B2 (OSRAM) |
| EP (1) | EP1838721B1 (OSRAM) |
| JP (1) | JP5234912B2 (OSRAM) |
| AT (1) | ATE538126T1 (OSRAM) |
| TW (1) | TWI370133B (OSRAM) |
| WO (1) | WO2006074983A1 (OSRAM) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5727135B2 (ja) * | 2006-06-09 | 2015-06-03 | デンツプライ インターナショナル インコーポレーテッド | 光重合性組成物 |
| EP2190903B1 (en) | 2007-09-04 | 2012-04-04 | Basf Se | Cyclic phosphines as flame retardants |
| CN102405239B (zh) | 2009-04-20 | 2014-10-15 | 瑞士联邦苏黎世技术大学 | 聚合物纳米颗粒 |
| WO2012052147A1 (en) | 2010-10-19 | 2012-04-26 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Process for the modification of polymers, in particular polymer nanoparticles |
| WO2012052148A1 (en) | 2010-10-19 | 2012-04-26 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Ultra fast process for the preparation of polymer nanoparticles |
| WO2014053455A1 (en) | 2012-10-01 | 2014-04-10 | ETH Zürich | A process for the preparation of acylphosphanes |
| EP3296301A1 (en) | 2016-09-19 | 2018-03-21 | ETH Zürich | A versatile process for the preparation of acylphosphines |
| EP3539924A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel vinyl phosphines and photo-initiators obtainable therefrom |
| US20220411447A1 (en) * | 2020-01-14 | 2022-12-29 | The University Of Vermont And State Agricultural College | Methods of Preparing Primary Phosphine Products Using Lewis Acid Catalysts |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3443221A1 (de) * | 1984-11-27 | 1986-06-05 | ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld | Bisacylphosphinoxide, ihre herstellung und verwendung |
| CH691970A5 (de) * | 1996-03-04 | 2001-12-14 | Ciba Sc Holding Ag | Alkylphenylbisacylphosphinoxide und Photoinitiatormischungen. |
| JP3975307B2 (ja) * | 1998-06-18 | 2007-09-12 | チッソ株式会社 | ホスフィン類の製造法 |
| SK286152B6 (sk) | 1998-11-30 | 2008-04-07 | Ciba Specialty Chemicals Holding Inc. | Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov |
| JP4225898B2 (ja) | 2001-08-21 | 2009-02-18 | チバ ホールディング インコーポレーテッド | 深色モノ−及びビス−アシルホスフィンオキシド及びスルフィド並びに光開始剤としてのこれらの使用 |
| WO2004050668A1 (en) * | 2002-12-04 | 2004-06-17 | Ciba Specialty Chemicals Holding Inc. | Process for the synthesis of cycloorganylphosphanes and di(alkali metal/alkaline earth metal) oligophosphanediides |
| CA2531318A1 (en) * | 2003-07-18 | 2005-02-17 | Ciba Specialty Chemicals Holding Inc. | Process for preparing acylphosphanes and derivatives thereof |
| TW200523265A (en) * | 2003-07-31 | 2005-07-16 | Basf Ag | A process for the preparation of acylphosphines |
| JP5148283B2 (ja) | 2004-11-23 | 2013-02-20 | チバ ホールディング インコーポレーテッド | アシルホスファン及びその誘導体の製造方法 |
-
2006
- 2006-01-09 US US11/795,059 patent/US7470819B2/en active Active
- 2006-01-09 JP JP2007550781A patent/JP5234912B2/ja active Active
- 2006-01-09 AT AT06701700T patent/ATE538126T1/de active
- 2006-01-09 WO PCT/EP2006/050081 patent/WO2006074983A1/en not_active Ceased
- 2006-01-09 EP EP06701700A patent/EP1838721B1/en active Active
- 2006-01-16 TW TW095101582A patent/TWI370133B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| WO2006074983A1 (en) | 2006-07-20 |
| ATE538126T1 (de) | 2012-01-15 |
| JP2008526918A (ja) | 2008-07-24 |
| EP1838721A1 (en) | 2007-10-03 |
| US20080071115A1 (en) | 2008-03-20 |
| TW200631958A (en) | 2006-09-16 |
| JP5234912B2 (ja) | 2013-07-10 |
| US7470819B2 (en) | 2008-12-30 |
| EP1838721B1 (en) | 2011-12-21 |
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