TWI260970B - Preparation of Chinese herbal composite recipe used in horticulture - Google Patents

Preparation of Chinese herbal composite recipe used in horticulture Download PDF

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TWI260970B
TWI260970B TW93121528A TW93121528A TWI260970B TW I260970 B TWI260970 B TW I260970B TW 93121528 A TW93121528 A TW 93121528A TW 93121528 A TW93121528 A TW 93121528A TW I260970 B TWI260970 B TW I260970B
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insecticidal preparation
preparation according
horticultural insecticidal
immersion liquid
mixed
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TW93121528A
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Chinese (zh)
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TW200539813A (en
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Chien-Yung Lee
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Chien-Yung Lee
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Abstract

A recipe of Chinese herbal composite used in horticulture to kill pests. The practical applications of this recipe include pest killing, germ and virus eradication of vegetables, fruit trees, flowers and economical plants. This recipe is composed of Gleditisia Sinensis, Sophora flavescens, Aloe uere, Stermona tuberose, Brucea jauamica and Dioscorea collettis vice versa. We prepare it with modem principles and scientific methods to emulsion spray. Those so called modem and scientific are the emulsion processes, micronization, permeability and the multiply potency it possessed. Several laboratory and field test proved that this invention had definite effect on the past killing, germ eradiation and virus inhibition. This invention is belongs to non toxic Chinese herbal preparation. The spray does not harm or cause toxic effect as it touch human skin, eyes, nasal mucosa, lip, mouth and tongue. It does not accumulate in human body and pollute environment.

Description

1260970 九、發明說明: 【發明所屬之技術領域】 本發明係有關一種園藝殺蟲用的中藥複方及其製備方 法。 5【先前技術】 近二、三世紀以來,物質文明的進步,給人類帶來了 不少正面的價值,同時,亦在生態、環境方面,出現了嚴 重的負面影響,世界人口增加,人類飲食的園、農蓺作物籲 亦必增產,但是,在生態環境負面變化、影響下,二等作 10物卻面臨了病、毒、蟲害的無情侵襲,導致生產的困難。 化學農藥於是應運而生,因為它的殺滅效能確鑿,而 y吏用方便,使之成為農友增產的法寶,—直成為市場的 ,銷貨。及至廿世紀中葉,測試、檢驗的科技挺進,人類 %保、污染等意識抬頭,逐漸證實了此類化學毒劑殘留毒 15 、^染等,於人體健康及自然環境的貽害。目前發達國家 已嚴禁它在本國製造;2004年i月i日起,歐盟將正式禁籲 止320種農藥的銷售,以及沾染有此類殘毒的農副產品進 實際上西洋辰藥企業家早已知此趨勢,且致力於低 辰藥的研發與產銷,所投人研發的資本頗矩;只是此 2〇低毒產品的效用實遠不如劇毒農藥,且容易形成了病毒蟲 類的抗藥性。 —在中華醫藥典籍裡,有關農用殺蟲、滅菌、抑制毒素 =物記載甚多’就殺蟲方面,如醉魚藤、藜蘆、茵芋、狼 毋一患子煙草、除蟲菊、膽矾、百部、皂英、菩楝樹 -3- 1260970 =等:,然而劇毒中藥同樣已不符環保、衛生條件,若用無 =中藥’依據實際實驗,在6倍量縮之製劑中,亦僅能在5 °稀釋下殺滅告蟲’對於經濟效益與應用利便方面,呈現1260970 IX. Description of the invention: [Technical field to which the invention pertains] The present invention relates to a traditional Chinese medicine compound for horticultural insecticidal use and a preparation method thereof. 5 [Prior Art] Since the second and third centuries, the progress of material civilization has brought many positive values to mankind. At the same time, it has also had serious negative effects on the ecological and environmental aspects. The world population has increased and human diet. The gardens and farmland crops will also increase production. However, under the negative changes and influences of the ecological environment, the second-class products are faced with the ruthless invasion of diseases, poisons and insects, which leads to difficulties in production. Chemical pesticides came into being, because its killing effect is conclusive, and y吏 is convenient to use, making it a magic weapon for farmers to increase production, and it has become a market and sells goods. In the middle of the century, the technology of testing and testing advanced, and human consciousness, pollution, and other awareness rose, gradually confirming the poisoning of such chemical poisons, such as dyeing, in human health and the natural environment. At present, developed countries have banned it from manufacturing in the country; since the i-day of 2004, the EU will formally ban the sale of 320 kinds of pesticides, as well as agricultural and sideline products contaminated with such residual drugs. In fact, entrepreneurs of Western medicine have long known this. Trends, and committed to the development, production and marketing of low-Chen medicine, the capital invested by the people invested is quite awkward; only the effectiveness of this low-toxic product is far less than that of highly toxic pesticides, and it is easy to form the resistance of virus insects. - In the Chinese Medicine Classics, there are many records about pesticide killing, sterilization, and inhibition of toxins. In terms of insecticide, such as drunken vine, gourd, oyster, wolfberry, tobacco, pyrethrum, gall bladder矾, Hundred, Soap, Bodhi -3- 1260970 =etc., However, the highly toxic Chinese medicine is also inconsistent with environmental protection and sanitary conditions. Can only kill the worm at 5 ° dilution' for economic benefits and application benefits, presented

Jt!、力’因此’ IX巾藥研製無毒農藥的正確理念,仍 5新的突破。 「發明目的」 #本發明的目的,在於提供—種用於園藝作物殺蟲、滅 囷、抑制毒素的中藥複方,以及新穎、科學的泮取、製備 10 ^法,使增進6倍以上的原藥效。開創中華醫藥新的利用 二價值’雛取代有毒化成錢,維護農翻益、人類健 康,避免環境污染與毒害。 【發明内容】 I5 、緣為達成本發明的上述目的,特為提供藥物主成份的 轉化機理」、「藥物組配」、「冑物製備方法」、「藥理說明 r「使用範圍與方法」、「注意事項」、「轉化及室内實驗」 以及初步的「田間實驗」等。 轉化機理 20 本發明所謂的轉化機理,是指促使藥物達標效能,完 =:::的機要道理;它包括了中醫藥固有的論據、乳 化過私舁透入力度、微細化的處理等等。 在排除有毒帽的絲理念下,錢的t草藥所調製 的殺滅效能,當然難與化成農藥及純化藥品相比擬。然而 -4- 1260970 匕的應用原理並不同於化成錢及純化藥品 =,而是中醫藥固有的論據,即在滅菌、制= ^始、'縧'夠、線諸蟲之目的外,乃可不傷及身體的原 為了在原論點上增進藥效’發明人特別分析了藥物中 ’在組配、製備上使其形成相乘效益,採取合 ”辰^卒取’避免生物碱或必要成份的遺失;尤其是採 =二原中藥製法紐、科學的硃磨機、膠質磨等微細 化過程,以及特殊的乳化過程。 麵虫:ίί权蟲、滅菌、制毒的效能’首先在於促使藥物 、=囷的表皮、黏膜而進人其體内,使其體内、組織間產 15 ^適?的環境驟變’欲達成此目的,則除了藥物組配、 目“效外’最緊要的是促使藥物的微細化以及透入力度 ^此、本發採用的乳化過程,製為水溶性乳化劑;緣為 水洛性的乳化劑更易經由皮膚、黏膜而被吸收。 〜液體和氣體之間的張力,稱為「表面張力」,而兩不相< 體’如本製劑的華詩油(主用成分為百里香盼、 目:、對聚傘花素)、松節油’與浸出藥液間的張力, ' 界面張力」。黃明膠、西黃芪膠、阿拉伯膠等乳化 別,屬于界面活性劑,它可降低油與藥液間的表面張力, 使^降至>1G dyne/em以下。乳化的目標,是要將油質有效 成分’經乳化劑及膠質磨1 _〇id mill)等外界提供的能量 促使折欠成小球滴,使之微細化,使藥物更易渗入蟲菌 體内’增進蟲菌皮膚及枯膜的吸收速率,驟變蟲菌體内環 -5_ 20 1260970 7.華薺葶:以蒸餾法淬取含有香荊芥酚、百里香酚,對 聚傘花素等殺蟲滅菌作用的揮發油,使本製劑更為精 緻。且以之作為乳化油劑,更能使微細化物完成預期 效果。 5 8.松節油:抗菌,驅蟲;乳化油。 9. 黃明膠:乳化劑,保護植物。 10. 朴消:與他種藥物内成分產生輔助、相乘效能,增進 穿透力,以達殺蟲、滅菌的目的。 (詳細内容請閱藥物說明) 10 「使用範圍及方法」 1. 本發明喷霧劑,適用於經濟作物、果樹、花卉、蔬菜 瓜豆,以及一般農作物之蟲、菌、病毒之農害。 2. 取本發明喷霧劑,稀釋以一定倍數之清水中,藉機動 15 或手動喷霧器,均勻喷灑於作物莖葉或害蟲體上。 3. 視蟲、菌、病毒之目、科,為害作物之輕重而決定加 入清水稀釋之倍數。 15〜30倍稀釋,可即殺各種害蟲、病菌、毒素。 30〜60倍稀釋,須經24〜48小時始能殺滅,或驅離。 2〇 60〜150倍稀釋,即有防治效果。 4. 本製劑為接觸性殺蟲劑,對於幼蟲、成蟲、卵皆有殺 滅效能。病蟲毒害對本製劑不能產生抗藥性。不會阻 斷環境生物鏈。稀釋倍數不必逐漸加強,防治週期可 逐漸延伸,對作物、人畜無毒害。 -8- 1260970 「注意事項」 是外时雜麵_,嚴⑼服,紐後能 症狀;可到藥房講買生綠豆粉、生甘草粉、 冷水調服6gm,使之輕麟可,或尋 1發製劑的稀釋賴人畜無害,㈣皮膚、眼睛、眼 冗、口舌均不致產生傷害。 3.本發賴触貯存在陰練賴,郎高溫變質。 厂 附加說明事項」 1.==藝二中藥複方喷灑劑’是以濃縮淬取的量化 里 $㈢如不添加,亦可產生相當之# 「草方的淬取,皆以具有殺蟲菌效能的 收取賤“。取_藥’但亦可採用其他藥材為 20 3·=之再泮取浸液’其— 5 if水6〇〜8〇%、乙醇15〜25%、甘油8〜12%。 拉備乳化過程’ W黃明膠或阿 一香:=(c特別是二含有百里㈣( 介酚(Carvacrol)、對〜聚傘花素( -9- 1260970 P-cymene)為主的中藥揮私 為乳化劍。 〜,但亦可採用其他藥材 6。本發明製_另1徵’是在麵 添加入朴消(硫酸鈉)3〇〜12〇 扪原梁液中 入本發明複方及製備特徵,伴,二 亦即本發賴錢魏射㈣的權利’ ,用於保持環境衛生 ·用於居家環境中 '10- 1260970 「藥物說明資料表」 NO: 1 中草藥名稱 皂荚 Zaolia 學名 Gleditsia Sinensis Lam 依 據 中華本草第4冊第480頁(中國上海科學技 術出版社) 產地、採收 季節、部位 產於東北、華北、華南以及四川、貴州等 地;秋季果實成熟變黑時採摘晒乾。 炮製、萃取 過程、方法 ⑴皂莢12kg,水浸6小時,分二次煎集藥 液;蒸發去水分5使剩5公升流浸膏, 入萆蘚粉末2kg攪勻;45t:乾燥,粉碎 過120目篩為細末,收貯備用。 有效成分 莢果含三菇皂甙:皂莢甙(gledinin),其甙 元為皂莢甙元,皂莢皂甙,尚含蜡醇、二 十九烷、正二十七烷、豆留醇、谷留醇、 鞣質等。 原記載藥理 作 用 抗菌作用,皂莢浸劑在試管内對堇色毛癬 菌和星形奴卡菌和某些皮膚真菌有抑制作 用。豬牙皂在體外有殺死絲蟲幼蟲和溶血 作用,主要表現為局部黏膜刺激作用。在 中樞神經系統,可致先痙攣後麻痒,最後 呼吸衰竭死亡。 藥理應用、 目 的 以皂莢含有的皂武、烧、醇等成分,達到 殺蟲滅菌的目標;並與他藥促進穿透作用。 ^〇U97〇 NO; 4 --- 依 ^--- 據 *^ 產地、 採收 季節、 部位 炮製、 萃取 過程、 方法 原記載藥理 作 用 部 Baibu 學 中菜 ^^^^3 Stemona tuberosa Lour 卓第8冊第189頁(中國上海科 ^產’移裁3年採挖,於冬季地上部枯 :、或春季萌芽前,挖出塊根,除去細 隼i')2 kg切片’水浸3小時’分二次煎 =液’祕水分制5公升流浸膏,入 牛末2 kg授勻;6〇。匸乾燥,粉碎過 =葉,根含百部碱、對葉百部碱、異對 葉=部碱等13種碱類;還含糖、脂類、蛋 二以及草酸等 [•抗病原微生物。 2.抗寄士蟲;經專家體外試驗表明,5〇%濃 度,藥液,可使蟯蟲在2〇小時内全死。 對葉百部碱能麻痺蛔蟲的活動。 十又滅叱触,百部水浸液和醇浸液對體虱、 陰虱均有殺滅作用,並使虱卵難以孵化。 對绳姐m、蟲、財、填、地老虎等 殺蟲、減菌、消病毐。 -14- ⑽0970Jt!, force 'so' IX towel developed the correct concept of non-toxic pesticides, still a new breakthrough. "Object of the Invention" The purpose of the present invention is to provide a traditional Chinese medicine compound for horticultural crops for killing insects, killing mites, and inhibiting toxins, as well as novel and scientific methods for extracting and preparing 10^, so as to increase the originality by 6 times or more. Drug effect. Create a new use of Chinese medicine, the second value of the 'five to replace the toxic into money, to maintain agricultural benefits, human health, to avoid environmental pollution and poison. SUMMARY OF THE INVENTION I5 and the purpose of achieving the above object of the present invention are to provide a conversion mechanism for a drug main component, a "drug combination", a "preparation method for a drug", and a "pharmacological description r" range and method for use. "Precautions", "Conversion and Indoor Experiments" and preliminary "Field Experiments". Transformation mechanism 20 The so-called transformation mechanism of the present invention refers to the principle of promoting the compliance of the drug, and the completion of the =:::; it includes the inherent arguments of traditional Chinese medicine, the emulsification of the penetration of the private, the processing of micro-refinement, etc. . Under the concept of removing the toxic cap, the killing efficacy of the t-medicine of the money is of course difficult to compare with the chemical and purified drugs. However, the application principle of -4- 1260970 匕 is different from the conversion of money and purified medicines, but the inherent arguments of traditional Chinese medicine, that is, in the sterilization, system = ^ beginning, '绦' enough, the purpose of the line insects, or not Injury to the body in order to improve the efficacy of the original arguments. 'The inventor specifically analyzed the drug in the composition, preparation to form a multiplicative benefit, take the combination of "Chen ^ stroke" to avoid the loss of alkaloids or essential ingredients In particular, the production process of the second Chinese traditional medicine, the scientific Zhu mill, the colloid mill, and the special emulsification process. The surface worm: ίί, the sterilization, the effectiveness of the production of drugs, the first is to promote drugs, = The epidermis and mucous membrane of the cockroach enter the body, causing the environment to change within the body and between the tissues. In order to achieve this goal, in addition to the drug combination, the most important thing is to promote The micronization and penetration of the drug, the emulsification process used in the present invention, is made into a water-soluble emulsifier; the water-soluble emulsifier is more easily absorbed through the skin and mucous membrane. ~ The tension between liquid and gas is called "surface tension", and the two are not the same as the body's Huashi oil (the main ingredient is thyme hope, mesh: cymene), turpentine 'The tension between the leaching solution, 'interfacial tension'. Emulsification of yellow gelatin, western gum, gum arabic, etc., is a surfactant, which can reduce the surface tension between oil and liquid, so that it falls below >1G dyne/em. The goal of emulsification is to make the oil-based active ingredient 'emulsifier and gel mill 1 _〇 id mill) and other external energy to reduce the deficiencies into small balls, make it fine, and make the drug more easily penetrate into the bacteria. 'Improve the absorption rate of the skin and the film of the worm, the ring of the worms in the body -5_ 20 1260970 7. Hua Tuo: Distilling the method containing the sucrose, thyme, cymene and other insecticides by distillation The volatile oil of sterilization makes the preparation more delicate. And as an emulsified oil agent, the finer compound can achieve the desired effect. 5 8. Turpentine oil: antibacterial, deworming; emulsified oil. 9. Yellow gelatin: an emulsifier that protects plants. 10. Park Yong: Produce auxiliary and multiplying effects with other ingredients in the drug, and improve penetrating power for the purpose of insecticide and sterilization. (Please refer to the drug description for details) 10 "Scope of use and method" 1. The spray of the present invention is suitable for agricultural crops, fruit trees, flowers, vegetables, melon beans, and pests of common crops, bacteria, and viruses. 2. Take the spray of the present invention, dilute it in a certain number of clean water, and spray it evenly on the stems or leaves of the crop by means of a motorized 15 or a hand sprayer. 3. The order of the insects, bacteria, viruses, and families, and the weight of the crops, is determined to be added to the dilution of water. 15~30 times dilution, can kill all kinds of pests, germs and toxins. 30 to 60 times dilution, can be killed by 24 to 48 hours, or driven away. 2〇 60~150 times dilution, that is, there is control effect. 4. The preparation is a contact insecticide and has a killing effect on larvae, adults and eggs. The pests and diseases are not resistant to the preparation. It does not block the environmental biological chain. The dilution factor does not have to be gradually strengthened, and the control cycle can be extended gradually, and it is not harmful to crops, humans and animals. -8- 1260970 "Precautions" is the external miscellaneous noodles _, strict (9) service, can be symptoms after the New Zealand; can go to the pharmacy to buy raw mung bean powder, raw licorice powder, cold water transfer 6gm, make it light, or find The dilution of the hair preparation is harmless to humans and animals, and (4) the skin, eyes, eyes are redundant, and the tongue is not harmful. 3. This hair is stored in the Yin Lai, Lang high temperature deterioration. Additional explanations for the factory" 1.==Yi Er Chinese Medicine Compound Sprayer is a quantitative quenching of the amount of money (3), if not added, can also produce equivalent # "grass extraction, all with insecticidal bacteria The performance of the charge 贱 ". Take _drugs, but you can also use other medicinal materials to re-soak the immersion liquid _ _ 5 if water 6 〇 ~ 8 〇 %, ethanol 15 ~ 25%, glycerol 8 ~ 12%. Pulling the emulsification process 'W yellow gelatin or Ayixiang:=(c especially two containing Chinese phenol (4) (Carvacrol), ~ cymene (-9-1260970 P-cymene)-based Chinese medicine Privately emulsified sword. ~, but other medicinal materials can also be used. 6. The invention of the invention _ another 1 levy is added to the complex (Sodium sulphate) 3 〇 ~ 12 〇扪 梁 梁 中 入 into the compound of the invention and preparation Characteristics, companionship, and second, the right to send money to Wei Wei (4), for maintaining environmental sanitation · used in the home environment '10-1260970 "Drug Description Data Sheet" NO: 1 Chinese herbal medicine name Zaolia scientific name Gleditsia Sinensis Lam According to Chinese Materia Medica Volume 4, page 480 (China Shanghai Science and Technology Press) Origin, harvest season, parts are produced in Northeast, North China, South China, Sichuan, Guizhou and other places; autumn fruit ripening and blackening when harvested and dried. Extraction process, method (1) 12kg of acacia, water immersion for 6 hours, sub-freshing liquid; evaporation of water 5 to make 5 liters of flow extract, 2kg of mash powder; 45t: dry, crushed 120 mesh For the fine, the storage is ready for use. The active ingredient pod contains three mushroom saponins: gledinin, the scorpion is acacia saponin, acacia saponin, still contains wax alcohol, octadecane, n-heptadecane, bean sterol, tropolol, hydrazine Quality, etc. Originally recorded pharmacological action antibacterial effect, acacia infusion in the test tube against Trichophyton rubrum and Star Nocardia and some skin fungi. Pig tooth soap in vitro to kill silkworm larvae and hemolysis The main effect is the local mucosal stimulating effect. In the central nervous system, it can cause itching after sputum and finally death of respiratory failure. Pharmacological application, purpose to achieve the insecticidal sterilization by soap, burning, alcohol and other ingredients contained in the acacia Target; and with other drugs to promote penetration. ^〇U97〇NO; 4 --- According to ^--- According to *^ origin, harvesting season, site processing, extraction process, method original record pharmacological action Department Baibu Dish ^^^^3 Stemona tuberosa Lour 卓第8页第189页 (Shanghai, China, China's production) 3 years of mining, in the winter above the ground: or before the spring germination, excavate the roots, remove the fine 隼') 2 kg slice 'water immersion 3 When the 'secondary frying = liquid 'secret water system 5 liters of extract extract, into the tail of cattle 2 kg to give uniform; 6 〇. 匸 dry, smashed = leaves, roots containing hundreds of bases, on the leaves of Bai base, different 13 kinds of alkalis such as leaf = base; also contains sugar, lipids, egg two and oxalic acid, etc. [• Anti-pathogenic microorganisms. 2. Anti-carrying insects; by experts in vitro tests, 5〇% concentration, liquid medicine It can cause the mites to die within 2 hours. Ten and the cockroaches are touched, and the 100 parts of the water immersion liquid and the alcohol immersion liquid have a killing effect on the body lice and the phlegm, and make the eggs difficult to hatch. For the rope sister m, insects, wealth, filling, ground tigers, etc., killing insects, reducing bacteria, eliminating diseases. -14- (10)0970

、採收 季節、部位 炮製、 過程、 萃取 方法Harvest season, location processing, process, extraction method

Brucea jauanica 有 成 效 分 鴉膽子 中華本草第5冊第7 主產於福建、台 地秋冬季果貫成熟,待果皮變黑色時、,、揚淨、晒 鴉膽子12 kg,水浸6小時,分二次煎集藥 液,去水分使剩5公升流浸膏,入萆藓末2 kg攪勻;60°C乾燥,粉碎過12〇目篩為細 備用。___ 、 =3〇餘種結構上類似菩木素的菩味成分; 避含黃花菜木脂素、香$酸、金絲桃武等 數種武類;又含油酸、三酸甘油酯等鴉膽 子油。 α 原記載藥理 作Brucea jauanica has a good effect. The main production of the Chinese medicinal herb is the 7th main production in Fujian and Taiwan. The fruit is ripe in autumn and winter. When the peel becomes black, the net is clean, the stalk is 12 kg, and the water is immersed for 6 hours. After the decoction, the solution was dehydrated to make 5 liters of the remaining extract, and 2 kg was added to the end of the crucible; the mixture was dried at 60 ° C, and the sieve was pulverized to a fine reserve. ___, =3〇The rest of the structure is similar to the botanical ingredient of bodhiin; avoiding several kinds of martial arts such as day lily lignan, fragrant acid, and gold silk peach; also contains oleic acid, triglyceride and other crows Bile oil.原 original record pharmacology

=癔、殺滅瘧原蟲,殺滅阿米巴原蟲。相 疋取物能驅除大腸道線蟲和條蟲,對鞭盖 也有驅除的作用 '" —-— — 可與朴硝、皂莢等發揮相乘效用,發揮牙丨 有的殺蟲功能。 _ ———— ~15- 1260970 NO: 6 中草藥名稱 萆蘚 學名 Beixie Dioscorea collettii Hook 依 據 中華本草第8冊第231頁(中國上海科學技 術出版社) 產地、採收 季節、部位 主產於浙江、安徽、江西、湖南等地。秋 冬二季挖取根莖,除去須根,去淨泥土, 切片晒乾。 炮製、萃取 過程、方法 取萆蘚片l〇kg,粉碎過100目篩為細末, 供為濃縮收取流浸膏的賦形藥。 有 效 成 分 含有9個留類成分:薯蕷皂甙元,雅姆皂 武元,^3,5-去氧替告急武元,Z\3,5—去 氧新替告皂武元,薯蕷皂武元棕櫚酸酯, 雅姆皂甙元棕櫚酸酯,/3谷甾醇。另有1 對差向異構體,以及2個甾武。 原記載藥理 作 用 水提取物具有殺昆蟲的作用,其有效成分 為薯蕷皂甙等。有抗真菌、如毛髮癖菌、 梨形孢子菌的作用,而對細菌無效。有部 分舊藥書記載,萆蘚有毒魚作用,試之並 不明顯。 藥理應用、 目 的 殺蟲,賦形。= 癔, killing the malaria parasite, killing the amoeba. The extract can remove the large intestine nematodes and worms, and also has the effect of repelling the whip cover. '" —-- — It can be used in combination with Pu Ni, Suso, etc. to play the insecticidal function of the gums. _ ———— ~15- 1260970 NO: 6 Chinese herbal medicine name Beixie Dioscorea collettii Hook According to Chinese Materia Medica No. 8 (page 231 (China Shanghai Science and Technology Press) Origin, harvest season, parts are mainly produced in Zhejiang, Anhui, Jiangxi, Hunan and other places. In the autumn and winter seasons, the roots are excavated, the roots are removed, the soil is removed, and the slices are dried. Processing, extraction process, method Take 萆藓 〇 〇 , , , , , , , , , 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 。 The active ingredient contains 9 kinds of retention ingredients: Diosgenin, Yam Soap, ^3,5-Deoxygenate, Wuyuan, Z\3,5-Deoxygenate, Wushu, Dioscorea Palmitate, yum saponin palmitate, /3 sitosterol. There are 1 pair of epimers, and 2 scorpions. Originally described pharmacological action The water extract has an insecticidal action, and its active ingredient is diosgenin or the like. It has anti-fungal properties such as hair sputum and pear-shaped spores, but it is not effective against bacteria. Some of the old drug books recorded that the cockroach had the effect of poisonous fish, and the test was not obvious. Pharmacological application, purpose insecticide, shaping.

-16- 1260970 NO: 7 中草藥名稱 華薺寧 Mosla chinensis 學名 Howgining Maxim. 依 據 中華本草第7冊第91頁(中國上海科學技術 出版社) 產地、採收 季節、部位 分布於華東、台灣、貴州。夏秋花初開、 莖葉茂盛時採割,陰乾、綑成小把。 炮製、萃取 過程、方法 華薺葶12 kg細切,入蒸顧桶中壓實,加熱 分濾出揮發油約240 m卜去渣、留油密貯 於玻璃瓶中備用。 有 效 成 分 華薺葶即石香薷,全草含揮發油2%,内含 香荊芥酚71.64%,對聚傘花素10.10%, 對異丙基苯曱醇5.00%,/5-蒎烯1.52%, 4瞽烯5·28%,松油烯1.23%,百里香酚 1.40%,葎草烯1.36%,/3-金合歡烯0.25 %,擰檬烯0.15%。 原記載藥理 作 用 石香薷揮發油有較強的廣譜抗菌作用。抗 菌有效成分為百里香酚,香荊芥酚,對聚 傘花素等。 藥理應用、 目 的 作為乳化油劑,使發揮油中殺蟲、滅菌的 作用,並帶動其他殺蟲滅菌藥的加倍效益。-16- 1260970 NO: 7 Name of Chinese herbal medicine Huashunning Mosla chinensis Scientific name Howgining Maxim. According to Chinese herbal medicine No. 7 (page 91 (Shanghai Science and Technology Press, China) Origin, harvest season, location distributed in East China, Taiwan, Guizhou. Summer and autumn flowers are opened, and when the leaves are flourishing, they are cut, dried, and bundled into small pieces. Processing, extraction process, method Huajiao 12 kg fine-cut, into the steaming barrel to compact, heated to filter out the volatile oil about 240 m to slag, leaving oil and stored in glass bottles for use. The active ingredient, Huajing, is Shixiang, which contains 2% volatile oil, contains 71.64% of cedar, 10.10% of cymene, 5.00% of cumene, and 1.52% of pentene. 4 terpene 5.28%, terpinene 1.23%, thymol 1.40%, valerene 1.36%, /3-farnesene 0.25%, chlormonene 0.15%. Originally recorded pharmacological action The volatile oil of Shixiangjing has a strong broad-spectrum antibacterial effect. The antibacterial active ingredients are thymol, carvacrol, and cymene. Pharmacological application, purpose As an emulsified oil agent, it can play the role of insecticide and sterilization in oil, and promote the double benefit of other insecticides.

ΛΊ- 1260970 NO: 8乳化油劑 中草藥名稱 松節油 Pimis 學名 Songlievou 依 據 中華本草第2冊第305頁(中國上海科學技 術出版社) 產地、採收 季節、部位 主產廣東、其他各省亦產,以植物中滲出 的油樹脂,經蒸餾或提取得到的揮發油。 炮製、萃取 過程、方法 購買原廠純淨松節油備用。 有 效 成 分 含樹脂酸、脂肪酸、單萜、倍半菇類等。 原記載藥理 作 用 1.抗菌作用,體外抑菌實驗及對動物實驗 性體癬、癖菌病治療觀察表明,具有較 強的抗真菌(白色念珠菌等)作用,對 金黃色葡萄球菌、大腸桿菌等也有一定 的抑菌作用。在本制劑中,用作乳化油 劑。 藥理應用、 目 的 乳化用藥,殺菌、驅蟲。ΛΊ-1260970 NO: 8 emulsified oil Chinese herbal medicine name turpentine Pimis scientific name Songlievou according to Chinese herbal medicine, Book 2, page 305 (Shanghai Science and Technology Press, China) Origin, harvest season, location main production in Guangdong, other provinces are also produced, with plants The oleoresin which is exuded, the volatile oil obtained by distillation or extraction. Processing, extraction process, method Purchase the original pure turpentine for use. Effective ingredients include resin acids, fatty acids, monoterpenes, and sesquitertes. Originally recorded pharmacological effects 1. Antibacterial effect, in vitro bacteriostatic test and observation of animal experimental sputum and sputum disease showed that it has strong antifungal (Candida albicans, etc.) effect on Staphylococcus aureus and Escherichia coli Also have a certain antibacterial effect. In the present preparation, it is used as an emulsified oil. Pharmacological application, purpose emulsification, sterilization, deworming.

-18- 1260970 中草藥名稱 明膠學名 Colla corii Bon,s 依 據 產地、採收 季節、部位 炮製、萃取 過程、方法 有 成 效 分 中華本草第9冊第680頁(中國上海科學技 版社)__ 將乾燥的黃牛皮鋼成小方塊,置清水中浸 洗2天,經常攪拌換水,至牛皮柔軟時洗 淨取出,入銅鋼内,加入約5倍量的清水, 加熱使徐徐沸騰,並隨時添水,每24小時 濾取清液,如此反覆3次;濾液用明矾沈 澱,傾取清汁,再入銅鍋内加熱濃縮,至 滴於濾紙上不化為度,加入黃酒或冰糖等 辅料收膠,倒入膠盤内,俟冷,切成小塊 晾乾 取市售純淨黃明膠,研為細末 經長時間的水朗膠原轉變為能溶於水的 黃明膠。含氮、糖,多種氨基酸;對植物 生長促進有幫助 原記載藥理Λ_^ 藥理應用、 J—的 =植物生長;在本發明中主要用為乳化 Μ劑 -19 - 1260970 NO: 10增效劑 中草藥名稱 朴消 Puxiao 學名 Mirabilite 依 據 中華本草第1冊第269頁(中國上海科學技 術出版社) 產地、採收 季節、部位 炮製、萃取 過程、方法 購買正廠朴消備用 有 效 成 分 主要為含水硫酸鈉(Na2So4-10H2O),另含 微量氯化鈉及約、鎂、鉀等無機元素,用 以穿透、軟化。 原記載藥理 作 用 藥理應用、 目 的 用以與蘆薈、皂莢、鴉膽子等藥物内之成 分產生相乘或輔助效果,促進殺蟲、減菌 及穿透力。 1260970 田間實驗例1細之小白蚊毒蛾、茶浮塵子、荼紅㈣ 時間——--口 艾禾 2003年4月13日 地號 高雄縣六龜鄉新開段1123 現場環境 蟲害實況 病蟲名稱 及簡介 海拔 800 吟雜檳榔樹。 • $ 分莖處、老葉背面 幼蟲,少數老葉枯落。 ^ 2. ίϊίϋ有Ϊ吮傷痕跡’搖動茶欉,見 ^子塵子飛濺,情況將漸趨嚴重。 之幼蟲。 务,二、雄蟎盾形,略小。紫紅色或深紅 月上較淡,體上疏生白色細毛,足淡紅 ,,幼3對,後變4對;為宝老荦筆片佶 枯褐、脫落。 勹口老業業片,使 2· 又^余葉輝’纖弱,體長1〜3公 m#:、、、彔色,半透明,前翅僅帶黃色。吸食 、、炎葉ί終葉J!,被害茶碳萎縮、黃 人葉、味蜒褐色,葉捲成船形而脫落。 m蛾ϋί頭毒毛蟲、刺毛狗;體 fi2〜3G公厘,觀因發生季節而異,生於 的頭部赤色,體淡黃色。全身生多數 色長毛塊,觸人皮膚即引發過敏痒痛。3〜士 個月為害最盛,喷食〇 j j^2〇000 # J ^ 21- 1260970 效果檢評 4月14日中午檢視之,茶蟎不復見,茶葉背蟎 卵由淡紅色較白色;搖動茶樹,並無飛藏的浮 塵子;小白蚊毒蛾幼蟲死於地上。4月20日再 檢視,茶芽已正常發育,害蟲亦不見。 附註說明 實際上,自茶園開耕至今,一直採用中藥製劑, 但原為粉劑混稀150倍已有效。今改良為乳化 劑,且用100倍稀釋,因而效果顯著。-18- 1260970 Chinese herbal medicine name gelatin scientific name Colla corii Bon, s According to the origin, harvest season, site processing, extraction process, method is effective, divided into Chinese herbal medicine, Volume 9, page 680 (China Shanghai Science and Technology Press) __ will be dry Yellow cowhide steel into small squares, immersed in clear water for 2 days, often stir and change water, when the cowhide is soft, wash and take out, into the copper steel, add about 5 times the amount of water, heat to make it boil, and add water at any time, every time The supernatant was filtered for 24 hours, and the mixture was repeated three times. The filtrate was precipitated with alum, and the clear juice was poured. The mixture was heated and concentrated in a copper pot until it was dropped on the filter paper. The addition of yellow wine or rock sugar was added to the gel and poured. Inside the rubber plate, it is cold, cut into small pieces and dried to obtain pure yellow gelatin. It is turned into a yellow gelatin which is soluble in water after a long period of time. Containing nitrogen, sugar, and various amino acids; helpful for plant growth promotion; original pharmacological Λ _ ^ pharmacological application, J - = plant growth; in the present invention mainly used as emulsified tincture - 19 - 6060970 NO: 10 synergist Chinese herbal medicine Name Puxiao Puxiao Scientific name Mirabelite According to Chinese Herbal Medicine Book No. 269 (Shanghai Science and Technology Press, China) Origin, harvesting season, location processing, extraction process, method of purchase Na2So4-10H2O), containing a trace amount of sodium chloride and inorganic elements such as magnesium, potassium, etc., for penetration and softening. Originally recorded pharmacological application Pharmacological application, purpose to produce multiplication or auxiliary effect with ingredients in aloe, acacia, brucea and other drugs to promote insecticidal, bacteriostatic and penetrating power. 1260970 Field experiment example 1 Small white mosquito moth, tea floating dust, blush (4) Time——--Ming Aihe April 13, 2003 No. 1123, Xinkai Section, Liugui Township, Kaohsiung County No. 1123 Live pest status Introduction to an altitude of 800 noisy betel trees. • $ tiller, old leaf back larvae, a few old leaves withered. ^ 2. ϊ ϊ ϋ ϋ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ ’ Larva. Business, two, male shield, slightly smaller. Fuchsia or dark red The moon is lighter, the body is sparsely white and fine hair, the foot is reddish, and the young pair is 3 pairs, and the later is 4 pairs; for the old man, the pen is brown and falls off. The old business of the mouth of the mouth, so that 2 · and ^ Yu Yehui 'slim, body length 1 ~ 3 male m #:,,, tan, translucent, the front wing only with yellow. Smoking, yan leaves 终 end leaves J!, the victim tea carbon shrinking, yellow leaves, miso brown, leaves rolled into a boat shape and fell off. m moth ϋ 头 poisonous caterpillar, bristled dog; body fi2~3G mm, depending on the season of occurrence, born in the head red, pale yellow. Most of the body has long hairs, which can cause allergic itching. 3~Shiyue is the most dangerous, sprayed 〇jj^2〇000 # J ^ 21- 1260970 The effect check is checked at noon on April 14th, the tea sputum is no longer seen, the tea raccoon is made of light red and white; Tea trees, there are no flying floats; small white mosquito moth larvae die on the ground. On April 20th, the tea buds have developed normally and the pests have disappeared. Note Note In fact, since the tea garden has been cultivated, traditional Chinese medicine preparations have been used, but the original powder is diluted 150 times. It has been improved as an emulsifier and is diluted by 100 times, so that the effect is remarkable.

-22- 1260970 田間實驗例π玉蘭樹之桑介殼蟲 實驗目的 本發明複方製劑;實施於玉蘭樹之桑介殼蟲的效 果。 時間地點 2003年11月24日。高雄縣六龜鄉新開段1123地 號。 現場環境 玉蘭樹植於農舍右前方,樹齡已20年,為休閒樹 蟲害實況 本次實驗有二棵玉蘭樹,患桑介殼蟲已多年,基f 中段常呈白粉狀外觀,或延伸至分枝部,致使患部 上面的綠葉逐漸萎黃,開花普遍弱小,終至枝莖枯 死,因樹大、排水、空氣良好,故能存活至今。以 手摩擦蟲害莖表,可覺幼蟲之濕度與氣味。 病蟲名稱及 簡 介 桑介殼蟲L別名崦。主要寄主有桑、菩楝、梅、李、 桃、杏、蘋果、玉蘭、木芙蓉等植物。初附生於枝 幹基部,被害處皮表形成灰白色或粉狀的異徵。幼 今和雌今吸食汁液,漸次向枝梢展延,受害枝幹萎 縮、枯落。雄蟲〇·75公厘,赤色、頭部褐色,有 觸角,口吻退化,有透明翅一對,足細長,交接器 針狀。雌成蟲長〇公厘,身體藏於灰白色之介殼 淡紅撥色,扁平而硌圓,無觸角及翅,口吻發 達。介,白色或灰白色,圓或短橢圓形,中央有臍 點’直徑1·8〜2.5公厘。幼蟲扁平橢圓,淡黃色, 經一次蛻皮後,便分泌介殼而居於其下。 實施概況 倍清水稀釋’以機動喷霧器周詳、^ 枝莖上,崎沾濕為度。 效果檢評 了,,试以手摩擦蟲害莖表,顯覺乾燥, ,味。14日後,灰白色介殼逐漸脫落, 原触告上鳊的葉片,已漸轉音翠。 ' ----- 附註說明 1260970 田間實驗例nr龍葵菜之蚜蟲 實驗目的 時間地點 現場環境 方製劑;實施於龍葵菜之蚜蟲的效桌了 H年11月17日。高雄縣六龜鄉新開段 蟲害實況 病蟲名稱 及簡介 ψ/f tJfe Λ : 1 ~ΙΓ~7-;~;---- ρΐϋΐ^ 以=3蔽含,多成:群吸食為害。 別常而識可呈現瑪 實施概況 效果檢評 附註說明 1------ 11 月 ~---——_ 不見蹤跡;原捲曲之之巧已 中有煤污潰,但亦不展開現象,硯察其 ϊ 龜鄉 ~ ——___-22- 1260970 Field experimental example π Magnolia sinensis scale insect experiment Experimental object The compound preparation of the present invention; the effect of the mulberry scale insect on the Yulan tree. Time and place November 24, 2003. No. 1123, the newly opened section of Liugui Township, Kaohsiung County. The environment environment Magnolia tree planted in the right front of the farmhouse, the age of the tree has been 20 years, for the live tree pests live. This experiment has two magnolia trees, suffering from the mulberry scale insects for many years, the base f often has a white powder appearance, or extended to the points Branches, causing the green leaves on the affected part to gradually sallow, the flowering is generally weak, and finally the stems die, because the trees are large, drainage, and the air is good, so they can survive to this day. Rubbing the stems with the hands can help the larvae's humidity and smell. Names of pests and diseases and sylvestris L. The main hosts are mulberry, bud, plum, plum, peach, apricot, apple, magnolia, wood hibiscus and other plants. The initial attachment is born at the base of the branch, and the skin of the victim is formed into an off-white or powdery sign. Young and today, the female sucks the juice and gradually spreads to the branches, and the damaged branches shrink and fall. Male cockroach 75 75 mm, red, brown in the head, tentacles, degenerate muzzle, a pair of transparent wings, slender feet, needles in the junction. The female adult is long and sturdy, and the body is hidden in the gray-white capsule. It is light red, flat and round, without tentacles and wings, and the muzzle is developed. Intermediary, white or off-white, round or short elliptical, with umbilical point in the center' diameter of 1·8~2.5 mm. The larvae are flat and elliptical, pale yellow. After one molting, they secrete the shell and reside below it. Implementation Overview Double-dilution water dilution was performed on a motorized sprayer, on the stems, and on the stems. The effect was checked, and the hand was used to rub the insect stem table to reveal the dryness and taste. After 14 days, the gray-white shell gradually fell off, and the leaves that had been touched by the cockroaches had gradually turned to sound. ' ----- Notes 1260970 Field experiment example nr Longkui's aphid Experimental purpose Time and place Site environment Formulation; Implemented in the dragonweed vegetable locust effect table on November 17th. Newly opened section of Liugui Township, Kaohsiung County Name of pests and pests Name and introduction ψ/f tJfe Λ : 1 ~ΙΓ~7-;~;---- ρΐϋΐ^ With =3 cover, more into: group smoking. Don't be acquainted with the presentation of the implementation of the implementation of the results of the implementation of the notes 1------ November ~---- _ no trace; the original curl of the clever has been coal-stained, but does not expand , 砚察ϊ 龟 turtle town ~ ——___

-24- 1260970 田間實驗例ιν木瓜輪班毒素病 實驗目的 g發^複謂劑;實施於木瓜彻 時間地點 號u月2 3。台灣省高雄縣兒涵硫 現场Ϊ辰境 農舍前階段中。 —--〜· 蟲害實況 原正¥發育之木瓜株,已於8、9月〜 至yjo月’其心葉(新生頂葉)發現點色 百化縮小’葉脈綠色帶化,具明顯崁紋, 病蟲名稱及 簡 介 2輪巧毒素病(Ring spGt virusy^^^ 辰咅,與蛾害、菌害並不相同;1975年首次發. f高在一、二年間遍傳全省,俗稱X「狂 縣研究記載,謂彳㈣有姆蟲和機 械所傳播,傳染迅速。 郎々恢 其病彳政首先是心葉黃化縮小,葉脈綠色帶化, ,,病葉比正常葉片小,葉緣漸乾:化葉片】 束絲麟祕植株死亡。病株的 f柄和!邛亦出現油浸狀斑點或條斑;植株、葦拓 =縮短小。花瓣上也出現油浸狀斑紋,往往開^不 要”、橢圓形的輪紋。病株無法 、%、、、貝結果,病果失去商品或使用價值。 實施概況 f有木瓜7株,依其位置分^"iTS'^STST ,平時風向關係,故擇北區為試驗區。以本發製 =稀,3G,,用機動喷霧II喷灑北區植株之葉柄 〜-!心葉’並在根部四周喷灌約10妨4音。 效果檢評 二日 新茱/病茱)緣呈現褐色斑。30日後,南區新生 葉仍出現點線黃色斑,葉勢萎弱;北區新生之 3 =呈現正常的翠綠色,葉勢壯盛,下層成長葉 ’但對照南區之下層生長葉則漸萎普。 1260970-24- 1260970 Field experiment example ιν papaya shift toxin disease Experimental purpose g hair ^ complexing agent; implemented in papaya time point location number u month 2 3 . The sulphur sulphur in Kaohsiung County, Taiwan Province, was in the pre-stage of the farmhouse. —--~· Pests in the original situation of the original development of the papaya strain, has been in August, September ~ to yjo month 'the heart leaf (new top parietal) found that the color of the localization shrinks 'leaf vein green belt, with obvious crepe Names of pests and diseases 2 Round toxin disease (Ring spGt virusy^^^ 辰咅, not the same as moths and fungi; first issued in 1975. f high throughout the province in one or two years, commonly known as X "The mad county study records that 彳 (4) is transmitted by worms and machinery, and the infection is rapid. Lang 々 其 其 其 其 其 其 其 其 其 其 其 其 其 其 其 其 其 其 首先 首先 首先 首先 首先 首先 首先 首先 首先 首先 首先 首先 首先 首先 心 心 心 心 心 心 心 心Gradually dry: the leaves of the leaves] The stalks of the stalks are dead. The f-stalks and sputum of the diseased plants also appear oil-immersed spots or streaks; the plants, 苇 extension = shortened small. Oil-like plaques also appear on the petals, often open ^Do not", elliptical wheel pattern. Diseased plants can not, %,,, shell results, the disease fruit lost goods or use value. Implementation profile f there are 7 papaya, according to its location ^ "iTS'^STST, usually Wind direction relationship, so the North District is selected as the test area. With the hair system = thin, 3G, sprayed with motorized spray II Petiole region of the plant ~-! Leaf 'and brown spots around the base of the sprinkler 4 to about 10 harm tone. Evaluation for effect of the 2nd new dogwood / dogwood disease) exhibit edge. After 30 days, the southern leaves of the southern area still showed yellow spots on the dotted line, and the leaf potential was weak. The fresh 3 of the northern area showed a normal emerald green, the leaves were strong, and the lower leaves grew, but the lower leaves of the southern area were compared. Gradually weak. 1260970

台灣木瓜的輪班毒素病已傳播近30年,一直缺乏 有效藥物之出現,只得採用網室栽培5每年之農業 損失甚鉅;本發明之出現顯係一大福音,且每年只 需喷霧3〜4次即可。Taiwan's papaya's shift toxin disease has been spread for nearly 30 years, and there has been a lack of effective drugs. It has to be cultivated in the net room. 5 The annual agricultural loss is very large. The emergence of this invention is a great boon, and only 3~ per year is sprayed. 4 times.

-26 - 1260970 田間實驗例v萊豆的瓜實繩防治 實驗目的 本發明複方製劑;實施於萊豆瓜實蠅害的效果。 時間地點 2003年11月9日。高雄縣六龜鄉新開段1123地 號。 現場環境 -棚張網式,面積約7平方公尺,種植萊豆(皇帝 豆)2株,施肥、灌派如常,莖葉已展佈於全網, 正值開花結莢期。 蟲害實況 豆花後的嫩丑莢呈現軟化、脫落現象,觀察嫩莢近 頭部有蛀痕,剝開後有幼蟲,黃白色,豆實有啃食 ,。同時,在豆棚白色繁花間,有似蠅似蜂的昆蟲 停聚、飛舞。 病蟲名稱及 簡 介 東方果繩大,經查閱農業蟲害資料,證實為 瓜貝蠅」,學名Daus cucrbitae Coeuilltt,別名瓜 ^翅目、果實婦。主要寄主為瓜類, f或加、五科作物的果實。成蟲身體黃褐 ,,長8〜14么厘,足赤黃、翅大,似蜂、類蠅, ϊίίϊϊί ί ,在於增強生殖能力、,並 ”,果,產卵’幼蟲孵化後即在果實内 幼瓜二3而變形、脫落’或停止生長; ^果洛地後,再於地面結繭繁殖。 實施概況 之了均勻城,使王部m濕;並於地面上喷灑 效果檢評 見瓜每蟎之,日11月16日觀察之,已不 見瓜貝狀_,且有部存 附註說明 11 月 25 日檢损,~~~---- 宜二曰現少數瓜實蠅,其防治至少 卻繁殖機會。 要贺灑地面,使瓜實蠅的繭失-26 - 1260970 Field experiment example v Bean solid rope prevention and control experiment Objective The compound preparation of the present invention; the effect of the implementation on the lyophilized fruit fly. Time and place November 9, 2003. No. 1123, the newly opened section of Liugui Township, Kaohsiung County. On-site environment - shed-net type, with an area of about 7 square meters, planted 2 beans of Laidou (Emperor Bean), fertilization and irrigation as usual, the stems and leaves have been spread over the whole network, which is in the flowering and pod-forming period. Insect pests The tender and ugly pods after the bean blossoms showed softening and shedding. The scars were observed near the head of the tender pods. After peeling, there were larvae, yellowish white, and the beans were foraging. At the same time, in the white flowers of the bean shed, insects like fly bees are gathering and flying. Names of pests and diseases Oriental fruit ropes, after reviewing agricultural pest data, confirmed as melon flies, the scientific name Daus cucrbitae Coeuilltt, alias melons, fruit, women. The main hosts are melons, f or plus, and the fruits of the five crops. The adult body is yellowish brown, 8~14 long, with red feet and large wings, like bees, flies, ϊίίϊϊί ί, which enhances reproductive ability, and ", fruit, spawning" larvae are in the fruit after hatching The young melon 2 deformed and fell off or stopped growing; ^ After the fruit was planted, it spread on the ground. The implementation of the generality of the city, so that the king m wet; and the effect of spraying on the ground to see melon Every cockroach, observed on November 16th, has no melon-like _, and there are some notes to explain the damage on November 25, ~~~---- At least but the opportunity to breed. To spread the ground, so that the loss of the fruit fly

-27- 1260970 室内實驗例i (轉化藥效的比較) 實驗 目的 地點 害蟲 取樣 吾蟲 簡介 實驗 預備 製 乳化,果 '—----------------- 2003年12月14日。高雄縣岡山鎮壽華路幻號實驗室 從私立實驗菜圃(岡山鎮岡山北路2號)之甘藍菜上拾 粉蝶,蟲(青蟲),以及自豆科植物「馬蹄決明」葉 嗅,即大菜_蟲各若干隻,均係不經喷g ^粕蝶·學名:Piens rapae CruCiuora Boisdurol,別名青 ,、菜青蟲;幼蟲體、頭部綠色,體上有細毛,可大至葉心' ’受害植株葉基之近莖處, 大菜暝:學名Hellula rogatalis Hulst,別明菜暝、豆暝, 2〜2.5公分,頭黑褐色,身綠色,有環節3條白' 二側ί粗灰色縱線,嘴食葉片至剩葉柄;葉與葉 巧^触糞及蛾絲連接,鑽入十字花科葉株的心葉,甘 監球内取食者,多係3齡大蟲 次甘 實驗 形成 慮紙上1防 π,位置為中心,分別由左自右、由右向左、由J =各育—次,共3次,再_、紙及蟲體移至玻璃櫃中 硕為㈠不lilL 化^ 類。 f— ②ft為5倍稀釋、10倍、15倍、2〇倍、 等6程次。 υ 1口 前提下,各程妙取豆喊6隻、青蟲4 ④觀察結果時間,第一次為喷藥後2分鐘 第 180分鐘後。 n乐人疋 -28- Ϊ260970 說明 與 依據藥理及歷次貫驗所得,21鐘内甘 或停止活動,並不能確定其已死亡,有因荜物府;J ,或有效藥物不能充分透入蟲體之緣以以 在30〜60分鐘内復活者;必須在2小時後呈;^ g 動狀態者,才能確定該蟲已難復活,為怛重起 ^ 以3小時後決定之。 、&見而 2· 他成分及添加 3·在5倍稀釋(原藥液卜清水5)下,(一)之立 =鐘内)停止活動者10,(二)之1〇則反呈次級藥kg ,位動^象二這是(二)加入乳化液,液態過濃厚的關 係,因έ有藥物成分均充足,故在18〇分鐘後,全益 可爬動之蟲,原位動者實際上亦呈衰疲,將隨時間g 進入死亡境界。 4·詳細觀察15倍〜30倍情況及變化,可發現(一)之原位 ,、爬動,蟲數逐漸增加,且原位動者並無衰疲的態 勢,^有復活之虞。反觀(二)之原位動者,只見30倍 之1中的2隻,而180分鐘後全已呈現死亡狀態。 5. 6· 气士表數據中可證,經乳化過程的中藥殺蟲菌製劑, 確貫可以增加六倍的效力。 f乳t匕的制備形式,以提昇中草藥的殺蟲滅菌效 力’疋本舍明^劑重要的特徵之一,是新穎的創見。 -29« 1260970-27- 1260970 Laboratory experiment example i (comparison of conversion efficacy) Experimental destination point pest sampling My insect introduction experiment preparation emulsification, fruit '------------------ 2003 December 14. The phantom laboratory of Shouhua Road, Okayama Town, Kaohsiung County, picks up butterflies, insects (green worms), and the legume "Horse Cassia" leaf scent from the cabbage of the private experimental dish (No. 2, Okayama North Road, Okayama Town). That is, a large number of vegetables, worms, are not sprayed g ^ 粕 butterfly · scientific name: Piers rapae CruCiuora Boisdurol, alias green, cabbage caterpillar; larvae body, head green, fine hair on the body, can be as large as the leaf heart ' 'The roots of the affected plant are near the stem, the big dish: the scientific name Hellula rogatalis Hulst, the other vegetables, the cardamom, 2~2.5 cm, the head is dark brown, the body is green, there are links 3 white' two sides ί coarse gray vertical line The leaf of the mouth is the leaf to the remaining petiole; the leaf and the leaf are connected with the feces and the moth, and the heart leaves of the cruciferous leaf plant are drilled into the heart of the cruciferous leaf, and the three-year-old insects are considered to be formed. Paper 1 is anti-π, the position is centered, from left to right, from right to left, by J = each breeding - times, a total of 3 times, then _, paper and worms moved to the glass cabinet (1) not lilL ^ Class. F—2ft is 5 times diluted, 10 times, 15 times, 2 times times, etc. 6 times. υ 1 mouth Under the premise, each process takes 6 beans, and the worms 4 4 observe the results, the first time is 2 minutes after spraying, 180 minutes later. n乐人疋-28- Ϊ260970 Description and based on pharmacology and previous tests, within 21 hours of gestation or cessation of activity, it is not certain that it has died, there is a cause of sputum; J, or effective drugs can not fully penetrate the worm The reason is to resurrect within 30~60 minutes; it must be presented after 2 hours; ^g move state, to determine that the insect has been difficult to resurrect, for the 怛 怛 ^ ^ to determine after 3 hours. , & see and 2 · his ingredients and additions 3 · in 5 times dilution (original liquid liquid water 5), (a) standing = clock) stop activities 10, (2) 1 〇 reverse The secondary drug kg, the position of the action ^ 2 This is (2) the addition of the emulsion, the liquid is too thick, because the drug ingredients are sufficient, so after 18 minutes, the whole benefit can crawl the insect, in situ In fact, the actor is also weak, and will enter the state of death with time g. 4. Detailed observation of 15 times to 30 times of the situation and changes, we can find (a) in situ, crawling, the number of insects gradually increased, and there is no debilitating situation in the in situ movement, ^ there is a resurrection. On the other hand, the in-situ movement of (2) only saw 2 of 30 times, and all of them showed death after 180 minutes. 5. 6· The data of the gas table can prove that the Chinese medicine insecticide preparation by the emulsification process can increase the efficacy by six times. The preparation form of f milk t匕 to enhance the insecticidal sterilization effect of Chinese herbal medicines. One of the important characteristics of 疋本舍明^ is a novel originality. -29« 1260970

ϊί受體位在原位不動,但以試棒推之猶 2⑽分鐘後之原位動,須 ,丁〜、哀疲14否?哀疲者必漸入死亡界限。 攸 動是指蟲體仍然有攸行的能力。 -30- ^260970 室内實驗例π(小菜蛾的殺滅) 日。高藏號蘇] 樣2得玻璃繁祕油菜苗上之幼蟲,委託工作人員The ϊί receptor is not in the position, but it is moved by the test rod after 2 (10) minutes, and it is necessary, Ding~, sorrow 14? The sorrowful person gradually entered the death limit. Turbulence is the ability of a worm to still have a limp. -30- ^260970 Indoor experiment example π (killing of Plutella xylostella) Day. High Tibetan No. Su] 2 larvae of glassy rapeseed seedlings, commissioned staff

xyi^S^IT^T^^TXyi^S^IT^T^^T

間” ίϊ!、%科;幼蟲均寄主於十字花科的植物,偏 f,Μ'匕采、蘿蔔、油菜。常見的幼蟲為3、4齡, JiJ.i么分以内,綠色或土黃色,分節明顯,遇驚 ΐ a掉^,以絲連接葉片,飄盪於空中,故稱「吊絲 触」。幼触潛入葉肉取食,2齡以後移至犖背,佶辇U ίί;ι—幼何,常聚食中央 〆:、繁殖遍1致死亡。本蟲年發生20世代左” 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 、 The subsection is obvious. In case of horror, a drop ^, the wire is connected to the blade, and floats in the air, so it is called "hanging silk touch". Young children sneak into the leaf flesh to feed, and after 2 years of age, they move to the back of the donkey, 佶辇U ίί; ι—young, often gather in the central 〆:, and breed to die. This insect year occurs in the 20th generation left

If 過度浸泡,~^指動If excessive soaking, ~^ fingering

’共3次,碰孰賴體移到乾I 吊絲蟲各10隻試驗之。 顏呈角弓反^^7^^ SM1隻卻殺;但㈣倍時,其中 -31- 1260970 小菜蛾(吊絲蟲)實驗表 稀釋倍數 蟲體狀 >兄 1· (2分鐘内) 2。(180分鐘後) 15 倍 停止活動 10 10 原位動 0 0 爬 動 0 0 20 倍 停止活動 10 10 原位動 0 0 爬 動 0 0 25 倍 停止活動 10 10 原位動 0 0 爬 動 0 0 30 倍 停止活動 8 10 原位動 1 0 爬 動 1 0 40 倍 停止活動 6 8 原位動 2 2 爬 動 2 0 1260970 眘路 目的 室内實驗例m(鑽心蟲的殺滅) 倍數對「灰 時間 地點 害蟲 取樣 害蟲 簡介 實驗 預備 實驗 形成 與結 論 20〇3年12月7 5^高雄縣六龜鄉 先生,種植於 采’乾其勿用農樂’以備試驗之小區〇 灰斑%蛾’學名:OebiaundalisFabriciuS. 「菜螟」、「菜心螟」、「蘿蔔螟」、「鑽心蟲」,鱗 蛾科;幼蟲為害,在本省以蘿蔔受害較嚴重, 其他十字花科的作物,侵入心葉蛀食,也常轉 iff露,出地面的根部,穿孔為害,常於受害孔外堆 ίτί ’笆卩i其受害部,可發現長約〇·8公分的幼蟲, 長ί t公交至尾有5條灰褐色縱線;成熟的幼蟲 照蟲位置, 2別由左向右、由右向左、由遠向近各喷一次,丘3 =5使tti傾斜15度’以防浸泡現象,2 “ 體移人通氣_膠瓶中,並略放潔淨 清水、15 倍、 用大小均勻之鑽心蟲10隻試齡 /γ〇7~7^ ^Γ~τγ——-~~--- 倍顧ϋ稀?下,蟲隻經180分鐘後仍有1〜2 触抗殺力強於青蟲、吊絲蟲等。故 $又滅的取佳在〜20倍之間。 — —---- -33- 1260970 灰斑螟蛾(鑽心蟲)實驗表 稀釋倍數 蟲體狀況 1· (2分鐘内) 2· (180分鐘後) 10 倍 停止活動 10 10 原位動 0 0 爬 動 0 0 15 倍 停止活動 10 10 原位動 0 0 爬 動 0 0 20 倍 停止活動 8 9 原位動 2 1 爬 動 0 0 25 倍 停止活動 6 7 原位動 2 2 爬 動 2 1 30 倍 停止活動 5 4 原位動 3 4 爬 動 2 2'A total of 3 times, hit the body to move to the dry I hanging silkworms each 10 trials. Yan Chengjiao bow reverse ^^7^^ SM1 only kills; but (four) times, which -31- 1260970 Plutella xylostella (spirulina) experimental table dilution factor worm body shape > brother 1 · (within 2 minutes) 2 . (after 180 minutes) 15 times stop activity 10 10 in-position movement 0 0 creeping 0 0 20 times stop activity 10 10 in-position movement 0 0 creeping 0 0 25 times stop activity 10 10 in-situ movement 0 0 creeping 0 0 30 times stop activity 8 10 in-situ movement 1 0 crawling 1 0 40 times stop activity 6 8 in-situ movement 2 2 crawling 2 0 1260970 cautious road indoor experimental example m (killing of borer) multiple to "grey time Location Pest sampling pest introduction Experimental preparation experiment formation and conclusion 20 〇 3 years December 7 5 ^ Mr. Liu Guixiang, Kaohsiung County, planted in the mining 'dry its do not use agricultural music' for the test of the community 〇 gray spot% moth' scientific name :OebiaundalisFabriciuS. "菜菜", "菜菜螟", "radish 螟", "rockworm", scale moth; larvae are harmful, radish is more seriously damaged in the province, other cruciferous crops, invading the heart leaf foraging It is also often turned to iff, the roots of the ground, the perforation is harmful, often piled outside the victim hole ίτί '笆卩i its victim, you can find larvae about 8 cm long, long t t bus to the end 5 Grayish brown vertical line; mature larva Insect position, 2 do not spray from left to right, from right to left, from far to near, mound 3 = 5 tilt tti 15 degrees 'to prevent soaking phenomenon, 2 "body shifting ventilation _ plastic bottle, and Slightly clean the clean water, 15 times, use the size of the borer 10 test age / γ 〇 7 ~ 7 ^ ^ Γ ~ τ γ —— ~ ~ ~ ~ 倍 倍 倍 倍 , , , , , , , , , , , , , , There are still 1~2 touch anti-killing ability stronger than the green insects, hanging silkworms, etc. Therefore, the best value of $ is less than ~20 times. — ——————— -33- 1260970 Gray spotted moth (Darkworm) experiment Table dilution factor worm status 1 · (within 2 minutes) 2 · (after 180 minutes) 10 times stop activity 10 10 in-situ movement 0 0 creep 0 0 15 times stop activity 10 10 in-situ movement 0 0 creep 0 0 20 times stop activity 8 9 in-position movement 2 1 crawling 0 0 25 times stop activity 6 7 in-situ movement 2 2 crawling 2 1 30 times stopping activity 5 4 in-situ movement 3 4 crawling 2 2

-34- 1260970 田間實驗例νι甘藍菜的吊絲蟲、青蟲防治 g ^ 物 Θ 的 子内段 014¾¾^-34- 1260970 Field experiment ν 甘 的 的 吊 、 、 、 、 、 、 、 、 、 、 g 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

丙為對照區。施 霧本製劑30倍每釋液一 11月10日γ 11月17日C is the control area. Application of the spray preparation 30 times per release solution 1 November 10 γ November 17

區無蟲吾,亦不發現蟲卵,本日無喷藥。 吊絲蟲6隻,偶見蟲卵。 曱區一株蟲害,檢得青蟲1隻,喷3〇倍藥液< 3隻、吊絲蟲4隻。 甲區不見蟲害,檢無蟲隻。本曰無喷藥。 青蟲2隻,吊絲蟲6隻 對照區不喊Μ -There is no insect in the area, and no eggs are found. There is no spraying today. 6 hanging silkworms, occasionally see eggs. One insect pest in the reclamation area was detected, and one black worm was detected, and three medicinal liquids were sprayed, three larvae, and four larvae. No insects were found in the A area, and no insects were detected. This is no spray. 2 green worms, 6 hanging silkworms, no control area -

曱^不見蟲害,改以5〇倍稀釋噴霧。 ,檢得2齡小吊j^_8隻。 了區不見蟲害,檢無蟲隻。本曰無喷藥。 麗青蟲3隻,吊絲蟲6售。 甲區不見蟲害,改以6〇倍稀釋噴霧c 蟲2隻,吊絲蟲4售 帀氐 >C a -;-—^ ----,一乂 ,「-r 叉 w 甲£不見虫虫告’檢無蟲隻。本曰無喷藥 隻,吊絲蟲4 1 ' .II j m1益气,3 u+月17曰檢得青蟲1隻外, a μ 均無蛛告,贺霧藥可由3〇倍稀釋逐漸这 ,60倍稀釋,即逐漸減輕藥量亦有效。饰早啊 .I丨2月29日,甘藍已結球待收其 狀況不良。 、、 -35-曱^ No insects, change the spray by 5 times. , 2 small hangs j^_8 were detected. No insects were found in the area, and no insects were detected. This is no spray. 3 larvae, snails 6 sold. No damage was found in the area A, and 2 sprays were used to dilute the spray c insects, and the silkworms were sold out. >C a -;--^ ----, one, "-r fork w A 'Check no insects only. This is not sprayed only, hanging silkworm 4 1 '. II j m1 Yiqi, 3 u + month 17曰 detected 1 green worm, a μ no spider, He fog drug can be 3 〇 The dilution is gradually reduced by 60 times, that is, the dosage is gradually reduced. It is also early. I丨 On February 29, the cabbage has been in the ball for a bad condition. ,, -35-

Claims (1)

1260970 蒸餾水60〜80%、乙醇15〜25%、甘油8〜12%。 8. 依據申請專利範圍第6項所述之園藝殺蟲用製劑,其 中更包含有蘆薈60〜100 gm。 9. 依據申請專利範圍第6項所述之園藝殺蟲用製劑,其 5 中該乳化劑係包含有黃明膠或阿拉伯膠40〜60gm、松 節油40〜60m卜石薺葶蒸餾油30〜50m卜 10. —種園藝殺蟲用製劑之製造方法,係備取皂莢、苦參 、百部、鴉膽子之中藥粉劑,入浸液作濾出作業,再 進行乳化作業,加入朴消混合均勻。 ίο 1L依據申請專利範圍第10項所述之園藝殺蟲用製劑之 製造方法,其中每3000 ml之浸液中,含有下列比例 的中藥精粉。皂莢80〜120 gm、苦參80〜120gm、百部 100〜140 gm、鸦膽子 100〜140 gm、朴消 30〜120gm。 12. 依據申請專利範圍第11項所述之園藝殺蟲用製劑之 15 製造方法,其中乳化作業中之乳化劑係包含有黃明膠 或阿拉伯膠40〜60gm、松節油40〜60ml、石薺葶蒸顧 油 30〜50ml。 13. 依據申請專利範圍第11項所述之園藝殺蟲用製劑之 製造方法,其中浸液濾出作業中,將中藥精粉於第1 2〇 次入浸液1200ml,經硃磨機2〜3次,浸2h濾出,第 2次入浸液1000ml經2h濾出,第3次入蒸餾水1200ml 浸4h再濾出,合三次濾液備用。 14. 依據申請專利範圍第11項所述之園藝殺蟲用製劑之 製造方法,其中乳化作業中,係將黃明膠或阿拉伯膠 -37- 1260970 50gm,混合松節油及石薺葶油各50ml,入膠質磨中 高速研磨,然後取蒸餾水l〇〇ml —次加入,續研磨3〜5 分鐘,反復3次;再加入浸液濾出後之濾液研磨3次。 15. 依據申請專利範圍第13項所述之園藝殺蟲用製劑之 5 製造方法,其中乳化作業中,係將黃明膠或阿拉伯膠 50gm,混合松節油及石薺葶油各50ml,入膠質磨中 高速研磨,然後取蒸德水1⑽ml —次加入,續研磨3〜5 分鐘,反復3次;再加入浸液濾出後之濾液研磨3次。 16. 依據申請專利範圍第11項所述之園藝殺蟲用製劑之 ίο 製造方法,其中中藥精粉更包含有蘆薈60〜100 gm。 17. 依據申請專利範圍第15項所述之園藝殺蟲用製劑之 製造方法,其中中藥精粉更包含有蘆薈60〜100 gm。 18. 依據申請專利範圍第11項所述之園藝殺蟲用製劑之 製造方法,朴消混合作業中,係以加入朴消50gm, 15 安息香酸3gm與乳化作業後浸液混合均勻,再經硃磨 機(GOLDEN MILL·)研磨2〜3次即成。 19. 依據申請專利範圍第16項所述之園藝殺蟲用製劑之 製造方法,朴消混合作業中,係以加入朴消50gm, 安息香酸3gm與乳化作業後浸液混合均勻,再經硃磨 2〇 機(GOLDEN MILL)研磨2〜3次即成。 苦 -38-1260970 distilled water 60~80%, ethanol 15~25%, glycerol 8~12%. 8. The horticultural insecticidal preparation according to claim 6, further comprising aloe vera 60 to 100 gm. 9. The horticultural insecticidal preparation according to claim 6, wherein the emulsifier comprises yellow gelatin or gum arabic 40~60 gm, turpentine 40~60 m buckwheat distilled oil 30~50 mb 10. A method for preparing a horticultural insecticidal preparation, which is prepared by taking a powder of acacia, Kushen, Baibu, and Brucea javanica, and filtering the infusion solution, and then performing an emulsification operation, and adding the mixture to a uniformity. Ίο 1L The method for producing a horticultural insecticidal preparation according to claim 10, wherein the 3,000 ml of the immersion liquid contains the following proportions of the traditional Chinese medicine powder. Acacia 80~120 gm, Kushen 80~120gm, 100 parts 100~140 gm, Brucea 100~140 gm, Parkxiao 30~120gm. 12. The method for producing a horticultural insecticidal preparation according to claim 11, wherein the emulsifier in the emulsification operation comprises yellow gelatin or gum arabic 40 to 60 gm, turpentine 40 to 60 ml, and stone sputum steaming. Gu oil 30~50ml. 13. The method for producing a horticultural insecticidal preparation according to claim 11, wherein in the immersion liquid filtering operation, the fine powder of the traditional Chinese medicine is 1200 ml in the first immersion liquid, and the pulverizer 2~ 3 times, dip 2h filtration, the second infusion 1000ml was filtered out for 2h, the third time into distilled water 1200ml dip 4h and then filtered out, three times the filtrate was used. 14. The method for producing a horticultural insecticidal preparation according to claim 11, wherein in the emulsification operation, yellow gelatin or gum arabic-37-1260970 50 gm, 50 ml of turpentine and sarcophagus oil are mixed into each other. The gel mill is ground at a high speed, and then distilled water is added to the mixture of l〇〇ml, and the mixture is continuously ground for 3 to 5 minutes, and repeated three times; and the filtrate after the addition of the immersion liquid is ground for 3 times. 15. The method for manufacturing a horticultural insecticidal preparation according to claim 13, wherein in the emulsification operation, 50 gm of yellow gelatin or gum arabic, 50 ml of turpentine and sarcophagus oil are mixed into the colloid mill. High-speed grinding, then take 1 (10) ml of steamed water for the first time, continue to grind for 3 to 5 minutes, repeat 3 times; and then filter the filtrate after adding the immersion liquid to grind 3 times. 16. The method of manufacturing a horticultural insecticidal preparation according to claim 11, wherein the fine powder of the traditional Chinese medicine further comprises 60 to 100 gm of aloe. The method for producing a horticultural insecticidal preparation according to claim 15, wherein the fine powder of the traditional Chinese medicine further comprises 60 to 100 gm of aloe. 18. According to the manufacturing method of the horticultural insecticidal preparation described in claim 11 of the patent application, in the simple mixing operation, the plant is added with 50gm, 15 benzoic acid 3gm, and the immersion liquid is uniformly mixed after the emulsification operation, and then the Zhu is mixed. Grinding machine (GOLDEN MILL) is ground 2 to 3 times. 19. According to the manufacturing method of the horticultural insecticidal preparation described in claim 16 of the patent application, in the simple mixing operation, the plant is added with 50gm, the benzoic acid 3gm is mixed with the immersion liquid after the emulsification operation, and then the Zhu mill is mixed. 2 GOLDEN MILL is ground 2 to 3 times. Bitter -38-
TW93121528A 2004-06-02 2004-07-19 Preparation of Chinese herbal composite recipe used in horticulture TWI260970B (en)

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