TW202342232A - Carrier for double-sided polishing, and double-sided polishing method and apparatus for silicon wafer using same - Google Patents
Carrier for double-sided polishing, and double-sided polishing method and apparatus for silicon wafer using same Download PDFInfo
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- TW202342232A TW202342232A TW112107747A TW112107747A TW202342232A TW 202342232 A TW202342232 A TW 202342232A TW 112107747 A TW112107747 A TW 112107747A TW 112107747 A TW112107747 A TW 112107747A TW 202342232 A TW202342232 A TW 202342232A
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- carrier
- double
- polishing
- sided
- silicon wafer
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- 238000005498 polishing Methods 0.000 title claims abstract description 99
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title claims abstract description 57
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 57
- 239000010703 silicon Substances 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims abstract description 21
- 235000012431 wafers Nutrition 0.000 claims abstract description 114
- 239000000835 fiber Substances 0.000 claims abstract description 76
- 229920005989 resin Polymers 0.000 claims abstract description 36
- 239000011347 resin Substances 0.000 claims abstract description 36
- 239000000463 material Substances 0.000 claims abstract description 21
- 238000000227 grinding Methods 0.000 claims description 42
- 239000002002 slurry Substances 0.000 claims description 15
- 239000002131 composite material Substances 0.000 claims description 10
- 239000004744 fabric Substances 0.000 claims description 9
- 239000003365 glass fiber Substances 0.000 claims description 7
- 239000002759 woven fabric Substances 0.000 claims description 6
- 239000000758 substrate Substances 0.000 claims description 4
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 3
- 239000004593 Epoxy Substances 0.000 claims description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000004917 carbon fiber Substances 0.000 claims description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 3
- 239000000969 carrier Substances 0.000 description 17
- 239000002585 base Substances 0.000 description 14
- 238000005259 measurement Methods 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000006061 abrasive grain Substances 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000007731 hot pressing Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000001000 micrograph Methods 0.000 description 3
- 238000007781 pre-processing Methods 0.000 description 3
- 239000003513 alkali Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000008119 colloidal silica Substances 0.000 description 1
- 229940075614 colloidal silicon dioxide Drugs 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000007517 polishing process Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B37/00—Lapping machines or devices; Accessories
- B24B37/04—Lapping machines or devices; Accessories designed for working plane surfaces
- B24B37/07—Lapping machines or devices; Accessories designed for working plane surfaces characterised by the movement of the work or lapping tool
- B24B37/08—Lapping machines or devices; Accessories designed for working plane surfaces characterised by the movement of the work or lapping tool for double side lapping
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B37/00—Lapping machines or devices; Accessories
- B24B37/27—Work carriers
- B24B37/28—Work carriers for double side lapping of plane surfaces
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having at least one potential-jump barrier or surface barrier, e.g. PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic System or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/30—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
- H01L21/302—Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
- H01L21/304—Mechanical treatment, e.g. grinding, polishing, cutting
Abstract
Description
本發明係關於兩面研磨用載具及使用此之矽晶圓的兩面研磨方法及裝置。The present invention relates to a carrier for double-side polishing and a method and device for double-side polishing of a silicon wafer using the same.
半導體裝置的基板材料廣泛使用矽晶圓。矽晶圓係藉由對矽單晶錠依序施行外圈研削、切片、研磨、蝕刻、兩面研磨、單面研磨、洗淨等步驟而製造。其中,兩面研磨步驟係將晶圓加工為既定厚度、且為提高晶圓平坦度的必要步驟,使用對晶圓雙面同時施行研磨的兩面研磨裝置實施。Silicon wafers are widely used as substrate materials for semiconductor devices. Silicon wafers are manufactured by sequentially performing steps such as outer ring grinding, slicing, grinding, etching, double-sided grinding, single-sided grinding, and cleaning on a silicon single crystal ingot. Among them, the double-side polishing step is a necessary step to process the wafer to a predetermined thickness and improve the flatness of the wafer, and is performed using a double-side polishing device that polishes both sides of the wafer simultaneously.
兩面研磨裝置有使用在研磨中保持晶圓的兩面研磨用載具。兩面研磨用載具的素材係有如金屬製載具與樹脂製載具。金屬製載具因為耐磨損性高故壽命長,但會有晶圓端面遭刮傷、金屬成分熔融等問題。樹脂製載具雖不會有晶圓端面刮傷、金屬成分熔融情形,但卻有耐磨損性低、壽命短的問題。The double-side polishing device uses a double-side polishing carrier that holds the wafer during polishing. The material of the carrier for double-sided polishing includes metal carriers and resin carriers. Metal carriers have a long life due to their high wear resistance, but there are problems such as scratches on the wafer end surface and melting of metal components. Although resin carriers do not suffer from scratches on the wafer end surface or melting of metal components, they have problems with low wear resistance and short lifespan.
專利文獻1有記載:一邊使用樹脂製兩面研磨用載具保持矽晶圓,一邊施行兩面研磨的方法。兩面研磨用載具係由使親水性纖維基材含潤樹脂的樹脂積層板構成,接觸到研磨布的表背面對純水的接觸角平均值係45°以上且60°以下。又,纖維基材的表面露出率達50%以上。根據專利文獻1所記載的樹脂製載具,可提升矽晶圓的研磨速率。
再者,專利文獻2有記載:在將載具投入兩面研磨機實際對晶圓施行加工前,便使用晶圓研磨用裝置外的其他裝置,實施由使用有摻磨粒漿料的一次研磨、與未摻磨粒漿料的二次研磨構成的2階段載具研磨(前處理)。
[先行技術文獻]
[專利文獻]
Furthermore,
[專利文獻1]國際公開第2018/105306號公報 [專利文獻2]日本專利特開2017-104958號公報 [Patent Document 1] International Publication No. 2018/105306 [Patent Document 2] Japanese Patent Application Publication No. 2017-104958
[發明所欲解決之課題][Problem to be solved by the invention]
然而,專利文獻1所記載習知的兩面研磨用載具,因為纖維基材的表面露出率高達50%以上,因而即使提升研磨速率,但載具磨耗快導致載具更換的頻度增加,造成生產成本提高的問題。又,一般晶圓平坦度品質變動係在剛更換載具後時最大,因而載具更換頻度越高,則未滿足所需平坦度品質的晶圓片數越增加。又,含有玻璃纖維基材的樹脂製載具,因玻璃纖維的磨耗片導致晶圓表面遭刮傷的機率提高。However, the conventional double-sided polishing carrier described in
緣是,本發明目的在於提供:藉由提升耐磨損性俾能達長壽命化的兩面研磨用載具及使用此之矽晶圓的兩面研磨方法及裝置。 [解決課題之手段] Therefore, the object of the present invention is to provide a carrier for double-side polishing that can achieve a longer life by improving wear resistance, and a method and device for double-side polishing of a silicon wafer using the carrier. [Means to solve the problem]
為解決上述課題,本發明的兩面研磨用載具係在對矽晶圓施行兩面研磨時,保持上述矽晶圓的兩面研磨用載具,具備有:由含纖維基材之樹脂積層板所構成略圓盤狀載具本體、以及在上述載具本體中形成的晶圓保持孔;上述載具本體主面的纖維露出率係未滿50%。In order to solve the above problems, the double-sided polishing carrier of the present invention is a double-sided polishing carrier that holds the silicon wafer when performing double-sided polishing on the silicon wafer, and is composed of a resin laminate containing a fiber base material. The roughly disc-shaped carrier body and the wafer holding hole formed in the carrier body; the fiber exposure rate on the main surface of the carrier body is less than 50%.
根據本發明,藉由載具本體主面的纖維露出率未滿50%,便可達提升耐磨損性。所以,可利用減少載具更換頻度而提升生產性,且能提升滿足所需平坦度品質的矽晶圓良率。According to the present invention, when the fiber exposure rate on the main surface of the carrier body is less than 50%, the wear resistance can be improved. Therefore, productivity can be improved by reducing the frequency of carrier replacement, and the silicon wafer yield that meets the required flatness quality can be improved.
本發明中,上述載具本體的平坦度較佳係5μm以下。依此,藉由使用平坦度5μm以下且纖維露出率未滿50%的載具,便可確保載具的耐磨損性,且能提高晶圓的平坦度品質。In the present invention, the flatness of the carrier body is preferably 5 μm or less. Accordingly, by using a carrier with a flatness of 5 μm or less and a fiber exposure rate of less than 50%, the wear resistance of the carrier can be ensured and the flatness quality of the wafer can be improved.
本發明中,上述載具本體的厚度較佳係較薄於上述矽晶圓研磨前厚度,且厚度差5~20μm。即使因在兩面研磨步驟中重複使用載具,致載具厚度逐漸減少,導致矽晶圓研磨前厚度與載具厚度的差在5~20μm範圍內變化的情況,但載具的纖維露出率仍維持未滿50%,因而可防止載具磨耗速度急遽增加。In the present invention, the thickness of the carrier body is preferably thinner than the thickness of the silicon wafer before grinding, and the thickness difference is 5~20 μm. Even if the thickness of the carrier gradually decreases due to the repeated use of the carrier in the double-sided grinding step, resulting in a situation where the difference between the thickness of the silicon wafer before grinding and the thickness of the carrier changes within the range of 5 to 20 μm, the fiber exposure rate of the carrier is still Keep it below 50%, thus preventing the vehicle wear rate from rapidly increasing.
較佳上述樹脂積層板係具有由使上述纖維基材含潤樹脂的複合片材,複數片重疊的多層構造;上述樹脂係環氧、酚或芳醯胺;上述纖維基材係玻璃纖維織布、碳纖維織布或有機纖維織布;上述多層構造係達3層以上。Preferably, the above-mentioned resin laminated board has a multi-layer structure in which a plurality of composite sheets are made of a composite sheet containing a moistening resin as the above-mentioned fiber base material; the above-mentioned resin is epoxy, phenol or arylamine; the above-mentioned fiber base material is a glass fiber woven fabric , carbon fiber fabric or organic fiber fabric; the above-mentioned multi-layer structure has more than 3 layers.
再者,本發明矽晶圓的兩面研磨方法,係包括有:準備兩面研磨用載具的步驟;以及在分別已黏貼研磨布的上定盤與下定盤間所配設的上述兩面研磨用載具上,裝填矽晶圓後,一邊朝上述上定盤與上述下定盤間供應漿料,一邊分別使上述上定盤與上述下定盤旋轉,而將上述矽晶圓施行兩面研磨的步驟;其中,上述兩面研磨用載具係具備有:由含纖維基材之樹脂積層板構成的略圓盤狀載具本體、以及在上述載具本體中形成的晶圓保持孔;上述載具本體主面的纖維露出率係未滿50%。Furthermore, the double-sided polishing method of the silicon wafer of the present invention includes: the step of preparing a double-sided polishing carrier; and disposing the above-mentioned double-sided polishing carrier between the upper fixed plate and the lower fixed plate to which the polishing cloth has been pasted. After loading the silicon wafer on the tool, while supplying slurry between the upper fixed plate and the lower fixed plate, the upper fixed plate and the lower fixed plate are rotated respectively, and the silicon wafer is ground on both sides; wherein , the above-mentioned carrier for double-sided polishing is equipped with: a substantially disc-shaped carrier body composed of a resin laminate containing a fiber base material, and a wafer holding hole formed in the above-mentioned carrier body; the main surface of the above-mentioned carrier body The fiber exposure rate is less than 50%.
根據本發明,可防止因纖維露出率增加導致載具磨耗速度急遽增加,俾可達載具長壽命化。所以,可利用減少載具更換頻度而提升生產性,且能提升滿足所需平坦度品質的矽晶圓良率。According to the present invention, the rapid increase in the wear rate of the carrier caused by the increase in fiber exposure rate can be prevented, so that the service life of the carrier can be prolonged. Therefore, productivity can be improved by reducing the frequency of carrier replacement, and the silicon wafer yield that meets the required flatness quality can be improved.
本發明矽晶圓的兩面研磨方法,最好在對上述矽晶圓施行兩面研磨的步驟前,更進一步包括有:依上述載具本體的平坦度在5μm以下、且上述纖維露出率未滿50%的方式,對上述兩面研磨用載具施行預研磨的步驟。依此,藉由使用平坦度5μm以下且纖維露出率未滿50%的載具,便可確保載具的耐磨損性、且提高晶圓的平坦度品質。The double-sided grinding method of the silicon wafer of the present invention preferably further includes: before the double-sided grinding step of the silicon wafer, the flatness of the carrier body is less than 5 μm, and the fiber exposure rate is less than 50 % method, a pre-grinding step is performed on the above-mentioned double-sided grinding carrier. Accordingly, by using a carrier with a flatness of 5 μm or less and a fiber exposure rate of less than 50%, the wear resistance of the carrier can be ensured and the flatness quality of the wafer can be improved.
本發明中,對上述兩面研磨用載具施行預研磨的步驟,最好依較薄於上述矽晶圓的研磨前厚度、且厚度差成為5~10μm的方式,調整上述載具本體的厚度。又,對上述矽晶圓施行兩面研磨的步驟,最好使用與上述矽晶圓研磨前厚度之厚度差在20μm以下範圍的上述兩面研磨用載具。即使因在兩面研磨步驟中重複使用載具,導致載具厚度逐漸減少,矽晶圓研磨前厚度與載具厚度差在5~20μm範圍內變化的情況,載具的纖維露出率仍維持未滿50%,因而可防止載具磨耗速度急遽增加。In the present invention, in the step of pre-polishing the double-sided polishing carrier, it is preferable to adjust the thickness of the carrier body so that it is thinner than the pre-polishing thickness of the silicon wafer and the thickness difference is 5 to 10 μm. Furthermore, in the step of double-side polishing the silicon wafer, it is preferable to use the double-side polishing carrier whose thickness difference from the thickness before polishing of the silicon wafer is within a range of 20 μm or less. Even if the thickness of the carrier gradually decreases due to repeated use of the carrier in the double-sided polishing step, and the difference between the thickness of the silicon wafer before polishing and the thickness of the carrier changes within the range of 5~20 μm, the fiber exposure rate of the carrier still remains less than 10 μm. 50%, thus preventing a sudden increase in vehicle wear rate.
再者,本發明的兩面研磨裝置,係具備有:分別已黏貼研磨布的上定盤與下定盤、以及配置於上述上定盤與上述下定盤間且保持矽晶圓的兩面研磨用載具;其中,上述兩面研磨用載具係具備有:由含纖維基材之樹脂積層板構成的略圓盤狀載具本體、以及在上述載具本體中形成的晶圓保持孔;上述載具本體主面的纖維露出率係未滿50%。Furthermore, the double-side polishing device of the present invention is provided with: an upper fixed plate and a lower fixed plate to which polishing cloths are respectively attached, and a double-sided polishing carrier that is disposed between the upper fixed plate and the lower fixed plate and holds the silicon wafer. ; Wherein, the above-mentioned carrier for double-sided polishing is equipped with: a substantially disc-shaped carrier body composed of a resin laminate containing a fiber base material, and a wafer holding hole formed in the above-mentioned carrier body; the above-mentioned carrier body The fiber exposure rate of the main surface is less than 50%.
根據本發明,可防止因纖維露出率增加導致載具磨耗速度急遽增加,俾能達載具長壽命化。所以,可利用減少載具更換頻度而提升生產性,且能提升滿足所需平坦度品質的矽晶圓良率。 [發明效果] According to the present invention, the rapid increase in the wear rate of the carrier caused by the increase in fiber exposure rate can be prevented, so that the service life of the carrier can be prolonged. Therefore, productivity can be improved by reducing the frequency of carrier replacement, and the silicon wafer yield that meets the required flatness quality can be improved. [Effects of the invention]
根據本發明可提供:藉由提升耐磨損性而達長壽命化的兩面研磨用載具及使用此之矽晶圓的兩面研磨方法及裝置。According to the present invention, it is possible to provide a carrier for double-side polishing that has a longer life by improving wear resistance, and a method and device for double-side polishing of a silicon wafer using the carrier.
以下,參照所附圖式,針對本發明較佳實施形態進行詳細說明。Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings.
圖1與圖2所示係本發明實施形態的兩面研磨裝置之構成圖,圖1係略剖視圖,圖2係略平面圖。Figures 1 and 2 show the structure of a double-sided polishing device according to an embodiment of the present invention. Figure 1 is a schematic cross-sectional view, and Figure 2 is a schematic plan view.
如圖1與圖2所示,兩面研磨裝置1係具備有朝上下方向呈相對向設置的上定盤2與下定盤3,在該上定盤2與下定盤3的研磨面上分別黏貼著研磨布4。研磨布4係可使用例如:使不織布含潤胺酯樹脂者、發泡聚胺酯墊。As shown in Figures 1 and 2, the double-
在上定盤2的上方設有為對上定盤2與下定盤3之間供應漿料用的漿料供應裝置5。漿料供應裝置5係從插入於上定盤2的貫通孔2a中之噴嘴6供應漿料。漿料係可使用含膠體二氧化矽的無機鹼水溶液。A
在上定盤2與下定盤3間的中心部設有太陽齒輪7,在外圈部設有內齒輪8,構成行星齒輪式兩面研磨裝置。上定盤2、下定盤3、太陽齒輪7及內齒輪8係具有相同的旋轉中心軸,可相互獨立進行旋轉運動。A
在上定盤2與下定盤3之間配置複數(此處為3個)兩面研磨用載具10(以下簡稱「載具」)。各載具10係配置於太陽齒輪7與內齒輪8之間,載具10的外環齒係與太陽齒輪7及內齒輪8雙方嚙合。上定盤2與下定盤3係若利用未圖示驅動源進行旋轉驅動,便連動於太陽齒輪7與內齒輪8一起進行旋轉。藉此,載具10在上定盤2與下定盤3間一邊自轉,一邊圍繞太陽齒輪7進行公轉。此時,因為矽晶圓W係被封鎖保持於在載具10中所設置的晶圓保持孔內,因而利用上下研磨布4同時對兩面施行研磨。又,在研磨步驟中從噴嘴6經由貫通孔2a供應漿料。A plurality (three in this case) of double-sided polishing carriers 10 (hereinafter referred to as "carriers") are arranged between the upper
圖3所示係載具10的構成略平面圖。FIG. 3 shows a schematic plan view of the structure of the
如圖3所示,載具10係具備有:具略圓盤狀外形的載具本體11、供保持矽晶圓W用的晶圓保持孔12(以下簡稱「保持孔」)、以及設置於載具本體11外圈部的外環齒13。保持孔12係依從載具本體11其中一主面(表面或上面),貫穿至另一主面(背面或下面)方式形成的圓形開口,保持孔12的直徑略等於矽晶圓W的直徑。因為保持孔12的中心位置偏離載具10的中心位置,因而保持孔12內的矽晶圓W係在載具10旋轉時進行偏心旋轉。本實施形態中,載具10中所形成保持孔12的數量係僅為一個,但亦可設置複數個保持孔12。As shown in FIG. 3 , the
圖4所示係構成載具10的樹脂積層板之截面構造剖視圖。FIG. 4 is a sectional view showing the cross-sectional structure of the resin laminated board constituting the
如圖4所示,兩面研磨用載具10的載具本體11,係由使纖維基材21含潤樹脂22的複合片材20(FRP片),呈複數片重疊的多層構造樹脂積層板構成。纖維基材21較佳係使用玻璃纖維織布、碳纖維織布等。樹脂22較佳係使用環氧、酚、芳醯胺等。樹脂積層板較佳係由複合片材20呈3層以上積層,較佳係如圖示的5層構造。As shown in Fig. 4, the
本實施形態中,載具10(載具本體11)主面的纖維露出率係未滿50%。即,在兩面研磨步驟中,使用纖維露出率未滿50的載具10,不用纖維露出率達50%以上的載具10。理由係若纖維露出率達50%以上,載具的耐磨損性會急遽降低,導致載具壽命縮短。In this embodiment, the fiber exposure rate on the main surface of the carrier 10 (carrier body 11) is less than 50%. That is, in the double-sided polishing step, the
兩面研磨步驟中所使用載具10的纖維露出率理想係0%。但是,經常使用纖維露出率0%的載具10係屬於極困難。通常樹脂積層板係將複數片的複合片材20施行熱壓形成一體化而製作。在熱壓時,因為最表面的樹脂會流落,因而即使增加樹脂對纖維基材的含潤量,但仍不會增加最表面的樹脂厚度。The fiber exposure rate of the
此外,因為剛完成後未使用全新載具係平坦度差,因而在實際使用前便施行全新載具的預研磨(前處理)(參照圖5)。具體而言,依與加工對象矽晶圓研磨前厚度的差成為5~10μm、載具平坦度在5μm以下的方式施行預研磨。若施行此種前處理,在載具10主面上一定會露出纖維基材21,依照研磨量判斷纖維露出率會達50%以上。若纖維露出率達50%以上,載具的磨耗速度會急遽增加,導致載具壽命縮短。In addition, because the flatness of the new carrier is poor if it is not used immediately after completion, pre-grinding (pre-processing) of the new carrier is performed before actual use (see Figure 5). Specifically, pre-polishing is performed so that the difference from the pre-polishing thickness of the silicon wafer to be processed is 5 to 10 μm and the carrier flatness is 5 μm or less. If such pretreatment is performed, the
但是,本實施形態中,兩面研磨步驟中所使用載具主面的纖維露出率維持未滿50%,且當對完全未使用過的全新載具施行預研磨時,剛施行預研磨後理所當然就不用說,就連因重複使用載具導致到達厚度下限值時,亦均依維持未滿50%纖維露出率的方式調整研磨量,因而可提升載具耐磨損性,俾達長壽命化。However, in this embodiment, the fiber exposure rate of the main surface of the carrier used in the double-sided grinding step is maintained at less than 50%, and when pre-polishing is performed on a completely unused new carrier, it is natural that the fiber exposure rate immediately after the pre-polishing is performed. Needless to say, even when the lower limit of thickness is reached due to repeated use of the carrier, the grinding amount is adjusted to maintain the fiber exposure rate below 50%, thereby improving the wear resistance of the carrier and extending its life. .
圖6所示係本發明實施形態矽晶圓的兩面研磨方法流程圖。Figure 6 shows a flow chart of a method for polishing both sides of a silicon wafer according to an embodiment of the present invention.
如圖6所示,本實施形態矽晶圓的兩面研磨方法,首先準備未使用的載具10(步驟S1)。如上述,載具10係將複數片(例如5片)的複合片材20施行熱壓而形成樹脂積層板後,施行打穿加工形成包含保持孔12與外環齒13在內的既定形狀而製作。As shown in FIG. 6 , in the double-sided polishing method of the silicon wafer in this embodiment, an
其次,為載具10的厚度調整及提升平坦度,便實施載具的預研磨(前處理)(步驟S2)。載具的預研磨係使用晶圓研磨用裝置外的其他裝置,使用摻磨粒漿料實施載具研磨。又,載具的預研磨時,依纖維露出率未滿50%方式,設定研磨的研磨量。例如依成為較晶圓研磨前厚度(例如785μm)更薄5~10μm的既定厚度(厚度上限值)方式,設定研磨的研磨量實施研磨加工。藉此,獲得1套組內的載具平坦度調整於5μm以下,且纖維露出率未滿50%的載具。因為1套組內的載具平坦度成為5μm以下,當然各個載具的平坦度亦在5μm以下。Next, in order to adjust the thickness of the
其次,使用預研磨後的載具10,實際實施矽晶圓W的兩面研磨步驟(步驟S3)。加工對象矽晶圓係依成為目標厚度與平坦度方式施行兩面研磨。待研磨加工完成,便從載具上取出矽晶圓W,送往下一加工步驟(單面研磨步驟)。Next, the
載具10係可再利用,重複使用直到成為既定厚度下限值為止(步驟S4N、S5、S6、S3)。若載具使用於兩面研磨步驟,則載具厚度亦會減少,藉由重複施行晶圓研磨,載具本身亦會隨之磨耗。特別因為樹脂製載具的磨耗較金屬製載具嚴重,因而可重複使用的次數減少,導致生產性降低。The
為對晶圓W施行兩面研磨必需使用較薄於晶圓W的載具10,但當使用相對於晶圓W目標厚度呈非常薄的載具10時,將無法確保晶圓所需平坦度。所以,將兩面研磨步驟時可使用載具的厚度下限值,規定於晶圓的目標厚度附近,在下限值以下的過薄載具被排除(廢棄)於使用對象外(步驟S4Y、S7)。載具的厚度下限值係例如設定為晶圓研磨前厚度(例如785μm)減20μm。In order to perform double-side polishing of the wafer W, a
再者,載具主面的纖維露出率達50%以上之載具亦被從持續使用的對象外(步驟S5Y、S7)。通常載具的纖維露出率會隨使用次數增加而增加,纖維露出率達50%以上載具的磨耗速度非常快。但是,因為本實施形態的載具係依即使從既定厚度上限值重複使用到厚度下限值,但纖維露出率仍經常未滿50%的方式形成,因而可抑制載具的磨耗速度增加,俾能達長壽命化。Furthermore, vehicles with a fiber exposure rate of more than 50% on the main surface of the vehicle are also excluded from continuous use (steps S5Y, S7). Generally, the fiber exposure rate of a vehicle will increase with the number of uses. Vehicles with a fiber exposure rate of more than 50% will wear out very quickly. However, since the carrier of this embodiment is formed in such a way that even if the carrier is repeatedly used from the predetermined upper thickness limit to the lower thickness limit, the fiber exposure rate is always less than 50%, it is possible to suppress an increase in the wear rate of the carrier. In order to achieve long life.
如以上所說明,本實施形態矽晶圓的兩面研磨方法,係使用由樹脂積層板所構成的兩面研磨用載具,對矽晶圓施行兩面研磨,且載具主面的纖維露出率未滿50%,因而可提升耐磨損性,俾能達載具長壽命化。As described above, the double-sided polishing method of the silicon wafer in this embodiment uses a double-sided polishing carrier made of a resin laminated board to perform double-sided polishing of the silicon wafer, and the fiber exposure rate on the main surface of the carrier is less than 100%. 50%, thus improving wear resistance and extending the life of the vehicle.
以上,針對本發明較佳實施形態進行說明,惟本發明並不僅侷限於上述實施形態,在不脫逸本發明主旨之範圍內可進行各種變更,當然該等亦均涵蓋於本發明範圍內。The preferred embodiments of the present invention have been described above. However, the present invention is not limited to the above-described embodiments. Various changes can be made without departing from the gist of the present invention. Of course, these are also included in the scope of the present invention.
例如上述實施形態中,舉可裝填3片樹脂製載具的兩面研磨裝置例,惟兩面研磨裝置的構成並無特別的限定,可採用能使用樹脂製載具的各種裝置。又,在載具中可裝填的晶圓片數、載具形狀亦無特別的限定。 [實施例] For example, in the above embodiment, a double-sided polishing device capable of loading three resin carriers is given as an example. However, the structure of the double-sided polishing device is not particularly limited, and various devices capable of using resin carriers can be used. In addition, the number of wafers that can be loaded in the carrier and the shape of the carrier are not particularly limited. [Example]
<載具平坦度與晶圓平坦度品質之關係> 針對載具平坦度對晶圓平坦度品質所造成影響進行評價。兩面研磨裝置係使用可裝填5片直徑500mm載具者。載具係具有單一的晶圓保持孔,可裝填1片直徑300mm的晶圓。晶圓係使用直徑300mm的p型矽單晶晶圓。研磨墊係使用未含磨粒的氨酯製研磨墊。漿料係使用含有粒徑60~110nm之二氧化矽磨粒、且pH11~12的無機鹼水溶液。 <The relationship between carrier flatness and wafer flatness quality> Evaluate the impact of carrier flatness on wafer flatness quality. The double-sided grinding device uses a carrier that can load 5 pieces with a diameter of 500mm. The carrier system has a single wafer holding hole and can load one 300mm diameter wafer. The wafer system uses a p-type silicon single crystal wafer with a diameter of 300mm. As the polishing pad, a urethane polishing pad containing no abrasive grains is used. The slurry uses an inorganic alkali aqueous solution containing silica abrasive particles with a particle size of 60 to 110 nm and a pH of 11 to 12.
所製作的載具經事先施行預研磨後,使用雷射位移計施行載具的厚度測定,求取1批次內的載具平坦度。1批次內的載具平坦度係從距載具保持孔中心朝上下左右四方向,距離載具保持孔中心1.01r(mm)的位置,設為測定點。After the produced carriers are pre-polished in advance, the thickness of the carriers is measured using a laser displacement meter to determine the flatness of the carriers within a batch. The flatness of the carrier within a batch is measured from the position 1.01r (mm) away from the center of the carrier holding hole in the four directions up, down, left, and right, and is set as the measurement point.
載具的平坦度計算方法係如圖7所示。將從保持孔中心C朝載具中心的方向設為基準方位(θ=0°),分別求取θ=0°、90°、180°、270°四方向在外圈附近的4個地方之厚度測定值X
1、X
2、X
3、X
4。保持孔12中心C距厚度測定點的距離設為1.01r(mm)。r係晶圓保持孔的半徑。
The calculation method of the flatness of the carrier is shown in Figure 7. Set the direction from the center C of the holding hole toward the center of the carrier as the reference orientation (θ=0°), and calculate the thickness of four places near the outer ring in the four directions of θ=0°, 90°, 180°, and 270°. Measured values X 1 , X 2 , X 3 , X 4 . The distance between the center C of the holding
從5片載具分別各4個地方獲得合計20地方的測定值中,將最大值X max與最小值X min之差ΔX=X max-X min,設為1批次內的載具平坦度(μm)。 From a total of 20 measured values obtained from 4 places on each of the 5 carriers, the difference between the maximum value X max and the minimum value X min ΔX = (μm).
接著,測定經兩面研磨後的矽晶圓之ESFQR(Edge Site flatness Front reference least Square Range)。著眼於平坦度容易惡化的晶圓邊緣之平坦度評價指標(部位平整度),表示邊緣塌邊(edge roll off)的大小。晶圓邊緣的平坦度係將設定為距晶圓最外圈例如2~32mm範圍(扇區長度30mm)的環狀外圈區域,更進一步朝圓周方向均等分割而獲得單位區域(部位),再依每個單位區域(部位)求取。ESFQR測定時係使用晶圓平坦度測定裝置(KLA-Tencor公司製Wafer Sight)。測定條件係將測定範圍設為296mm(最外圈2mm除外),邊緣部位測定時的扇區數(部位數)設為72,扇區長度設為30mm。載具平坦度與經研磨後晶圓的EFSQR之關係如圖8所示。另外,ESFQR係1批次內的5片晶圓測定值之平均值。Next, the ESFQR (Edge Site flatness Front reference least Square Range) of the double-sided polished silicon wafer is measured. The flatness evaluation index (site flatness) focuses on the edge of the wafer, where flatness is prone to deteriorate, and indicates the size of edge roll off. The flatness of the wafer edge is set to an annular outer ring area ranging from 2 to 32 mm (sector length 30 mm) from the outermost ring of the wafer, and is further divided equally in the circumferential direction to obtain unit areas (parts), and then Obtained based on each unit area (part). When measuring ESFQR, a wafer flatness measuring device (Wafer Sight manufactured by KLA-Tencor) was used. The measurement conditions are as follows: the measurement range is set to 296mm (excluding the outermost 2mm), the number of sectors (number of parts) when measuring the edge portion is set to 72, and the sector length is set to 30mm. The relationship between the flatness of the carrier and the EFSQR of the polished wafer is shown in Figure 8. In addition, ESFQR is the average of the measured values of 5 wafers in one batch.
如圖8所示,得知若載具的平坦度大於5μm,則晶圓的ESFQR會急遽惡化。此現象可認為因1批次內的載具厚度變動(平坦度)較大,導致1批次內的晶圓研磨狀態出現變動。As shown in Figure 8, it is found that if the flatness of the carrier is greater than 5 μm, the ESFQR of the wafer will deteriorate rapidly. This phenomenon can be considered to be due to the large variation in carrier thickness (flatness) within one batch, resulting in variations in the polishing state of the wafers within one batch.
<載具之纖維露出率與載具磨耗速度之關係> 其次,針對載具主面的纖維露出率對載具磨耗速度所造成影響進行評價。載具的材料係使用由5片使玻璃纖維布基材含潤環氧樹脂的片材,重疊的5層構造樹脂積層板構成。 <The relationship between the fiber exposure rate of the carrier and the wear rate of the carrier> Secondly, the impact of the fiber exposure rate on the main surface of the carrier on the wear rate of the carrier was evaluated. The material of the carrier is composed of a five-layer structure resin laminate made of five overlapping sheets made of glass fiber cloth base material moistened with epoxy resin.
載具主面的纖維露出率係將從載具晶圓保持孔外圈端距50mm以內的外圈部區域中,隨機選取的10個地方設為觀察地方,拍攝各觀察地方的CCD顯微鏡影像,再將拍攝影像施行二值化處理而計算出纖維部分的面積比。圖9(a)與(b)所示係載具表面的CCD顯微鏡影像一例。圖9(a)所示係二值化處理前的影像,圖9(b)所示係二值化處理後的影像。各測定地方的影像尺寸係2.8×2.1(mm)。載具表面的纖維露出率調整係藉由在為調整載具厚度或平坦度,而對載具施行預研磨的步驟中,調整研磨量而實施。The fiber exposure rate on the main surface of the carrier is determined by randomly selecting 10 places from the outer ring area within 50mm of the outer ring end of the carrier wafer holding hole as observation places, and taking CCD microscope images of each observation place. The captured image is then binarized to calculate the area ratio of the fiber part. Figure 9(a) and (b) show an example of CCD microscope images of the carrier surface. Figure 9(a) shows the image before binarization processing, and Figure 9(b) shows the image after binarization processing. The image size of each measurement location is 2.8 × 2.1 (mm). The fiber exposure rate adjustment on the surface of the carrier is performed by adjusting the polishing amount in the step of pre-polishing the carrier to adjust the thickness or flatness of the carrier.
載具磨耗速度係在裝填稍微薄於載具厚度的虛設矽晶圓後,使用含有膠體二氧化矽的矽晶圓研磨用漿料,施行載具的兩面研磨,從此時載具厚度每單位時間的減少量(研磨前後的厚度差)計算出。結果如圖10所示。圖10中,縱軸載具磨耗速度係將纖維露出率90%時的值,設為基準值100時的相對值。The carrier wear rate is determined by loading a dummy silicon wafer that is slightly thinner than the carrier thickness and using a silicon wafer polishing slurry containing colloidal silicon dioxide to polish both sides of the carrier. From this point on, the carrier thickness per unit time The reduction (thickness difference before and after grinding) is calculated. The results are shown in Figure 10. In Figure 10, the vertical axis carrier wear rate is the value when the fiber exposure rate is 90%, and is the relative value when the reference value is 100.
由圖10得知,纖維露出率42%以下時載具磨耗速度在27以下的較低值,但當纖維露出率50%前後時載具磨耗速度出現急速增加,當纖維露出率達60%以上時載具磨耗速度接近約100。反之,得知載具磨耗速度從纖維露出率低於60%時開始急遽降低,當纖維露出率50%時載具磨耗速度係纖維露出率90%時的載具磨耗速度一半以下。依此,若纖維露出率達50%以上則載具容易磨耗的理由,可認為因高鹼性研磨用漿料,對載具表面露出的玻璃纖維部分進行腐蝕所致。It can be seen from Figure 10 that when the fiber exposure rate is below 42%, the carrier wear rate is a low value below 27. However, when the fiber exposure rate is around 50%, the carrier wear rate increases rapidly. When the fiber exposure rate reaches more than 60%, At this time, the vehicle wear rate is close to about 100. On the contrary, it is found that the carrier wear rate starts to decrease sharply when the fiber exposure rate is less than 60%. When the fiber exposure rate is 50%, the carrier wear rate is less than half of the carrier wear rate when the fiber exposure rate is 90%. Based on this, the reason why the carrier is prone to wear when the fiber exposure rate reaches 50% or more is considered to be due to the corrosion of the exposed glass fiber portion on the surface of the carrier by the highly alkaline polishing slurry.
<載具之纖維露出率與晶圓處理片數的關係> 針對經考慮某晶圓厚度與平坦度規格所設定的載具厚度規格,在從上限至下限內重複使用載具時的晶圓處理片數進行評價。結果如圖11所示。 <Relationship between the fiber exposure rate of the carrier and the number of wafers processed> The number of wafers processed when the carrier is reused from the upper limit to the lower limit is evaluated for a carrier thickness specification set by considering a certain wafer thickness and flatness specification. The results are shown in Figure 11.
由圖11中得知,纖維露出率42%以下的載具時,晶圓處理片數係400前後,但纖維露出率48%時的晶圓處理片數則降低至250,又當纖維露出率達60%以上時,晶圓處理片數降低至100左右。It can be seen from Figure 11 that when the fiber exposure rate is less than 42%, the number of wafers processed is around 400, but when the fiber exposure rate is 48%, the number of wafers processed is reduced to 250. When the fiber exposure rate is 48%, the number of wafers processed is reduced to 250. When it reaches more than 60%, the number of wafers processed is reduced to about 100.
載具的纖維露出率係如上述對會載具磨耗速度造成影響,因而纖維露出率最好維持未滿50%,藉此可確認到能延長載具壽命。The fiber exposure rate of the carrier affects the wear rate of the carrier as mentioned above. Therefore, it is best to keep the fiber exposure rate less than 50%. This can be confirmed to extend the carrier life.
1:兩面研磨裝置
2:上定盤
2a:貫通孔
3:下定盤
4:研磨布
5:漿料供應裝置
6:噴嘴
7:太陽齒輪
8:內齒輪
10:兩面研磨用載具
11:載具本體
12:晶圓保持孔
13:外環齒
20:複合片材
20a:複合片材
20b:複合片材
21:纖維基材
22:樹脂
W:矽晶圓
1:Double-sided grinding device
2: Set the
圖1係本發明實施形態的製造裝置之構成略剖視圖; 圖2係本發明實施形態的單結晶製造裝置之構成略平面圖; 圖3係載具的構成略平面圖; 圖4係構成載具的樹脂積層板之截面構造剖視圖; 圖5係載具的預研磨(前處理)說明示意圖; 圖6係本發明實施形態的矽晶圓的兩面研磨方法之說明流程圖; 圖7係載具的平坦度計算方法說明示意圖; 圖8係載具平坦度與晶圓外圈平坦度(ESFQR)之關係圖; 圖9中,圖9(a)與(b)係載具表面的CCD顯微鏡影像,圖9(a)係二值化處理前的影像,圖9(b)係二值化處理後的影像; 圖10係載具的纖維露出率與磨耗速度之關係圖;以及 圖11係載具纖維露出率與晶圓處理片數之關係圖。 Figure 1 is a schematic cross-sectional view of the structure of a manufacturing device according to an embodiment of the present invention; Figure 2 is a schematic plan view of the structure of a single crystal manufacturing apparatus according to an embodiment of the present invention; Figure 3 is a schematic plan view of the vehicle; Figure 4 is a cross-sectional structural cross-sectional view of the resin laminated board constituting the carrier; Figure 5 is a schematic diagram illustrating the pre-grinding (pre-processing) of the carrier; Figure 6 is a flow chart illustrating a method for polishing both sides of a silicon wafer according to an embodiment of the present invention; Figure 7 is a schematic diagram illustrating the flatness calculation method of the vehicle; Figure 8 is a graph showing the relationship between carrier flatness and wafer outer ring flatness (ESFQR); In Figure 9, Figures 9(a) and (b) are CCD microscope images of the carrier surface, Figure 9(a) is the image before binarization processing, and Figure 9(b) is the image after binarization processing; Figure 10 is a graph showing the relationship between fiber exposure rate and wear rate of the carrier; and Figure 11 is a graph showing the relationship between carrier fiber exposure rate and the number of wafers processed.
10:兩面研磨用載具 10: Carrier for double-sided grinding
11:載具本體 11: Vehicle body
12:晶圓保持孔 12: Wafer holding hole
13:外環齒 13:Outer ring teeth
Claims (9)
Applications Claiming Priority (2)
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JP2022068746A JP2023158771A (en) | 2022-04-19 | 2022-04-19 | Carrier for double-sided polishing, double-sided polishing method and device for silicon wafer using the same |
JP2022-068746 | 2022-04-19 |
Publications (1)
Publication Number | Publication Date |
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TW202342232A true TW202342232A (en) | 2023-11-01 |
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JP (1) | JP2023158771A (en) |
TW (1) | TW202342232A (en) |
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JP4698178B2 (en) * | 2004-07-13 | 2011-06-08 | スピードファム株式会社 | Carrier for holding an object to be polished |
JP2008044083A (en) * | 2006-08-18 | 2008-02-28 | Kyocera Chemical Corp | Holding material for grinding |
KR20100065562A (en) * | 2008-12-08 | 2010-06-17 | 주식회사 실트론 | Lapping carrier |
TWI465317B (en) * | 2012-06-25 | 2014-12-21 | Sumco Corp | Polishing method of workpiece and polishing device of workpiece |
JP6152340B2 (en) * | 2013-12-26 | 2017-06-21 | Hoya株式会社 | Manufacturing method of disk-shaped substrate and carrier for grinding or polishing |
JP2020055065A (en) * | 2018-10-01 | 2020-04-09 | マーベリックパートナーズ株式会社 | Resin-made polishing carrier and method for producing the same |
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- 2022-04-19 JP JP2022068746A patent/JP2023158771A/en active Pending
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