TW201542108A - Low-tar menthol cigarette - Google Patents

Low-tar menthol cigarette Download PDF

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TW201542108A
TW201542108A TW104110659A TW104110659A TW201542108A TW 201542108 A TW201542108 A TW 201542108A TW 104110659 A TW104110659 A TW 104110659A TW 104110659 A TW104110659 A TW 104110659A TW 201542108 A TW201542108 A TW 201542108A
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Taiwan
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menthol
filter
cigarette
amount
tar
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TW104110659A
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Chinese (zh)
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TWI598049B (en
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Nobuyuki Ishikawa
Shinjiro Kagawa
Hiroyuki Kubota
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Japan Tobacco Inc
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/08Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
    • A24D3/10Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/002Cigars; Cigarettes with additives, e.g. for flavouring
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/02Cigars; Cigarettes with special covers
    • A24D1/027Cigars; Cigarettes with special covers with ventilating means, e.g. perforations
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/04Cigars; Cigarettes with mouthpieces or filter-tips
    • A24D1/045Cigars; Cigarettes with mouthpieces or filter-tips with smoke filter means
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • A24D3/048Tobacco smoke filters characterised by their shape or structure containing additives
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/061Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/062Use of materials for tobacco smoke filters characterised by structural features
    • A24D3/066Use of materials for tobacco smoke filters characterised by structural features in the form of foam or having cellular structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

Abstract

The present invention provides a low-tar menthol cigarette having a cigarette rod part and a filter part winded with a tipping paper, wherein the amount of the tar is 5 mg or less. The filter part comprises a single segment consisting of cellulose acetate tow, an airflow resistance of the filter part is 25 to 80 mm H2O/27 mm, and ventilation of air flowing from ventilation holes penetrating the tipping paper is 55% or more, and the filter part is added with menthol.

Description

低焦油薄荷醇香煙 Low tar menthol cigarette

本發明係有關一種低焦油量且添加有薄荷醇的帶濾嘴香煙。 The present invention relates to a filter cigarette having a low tar content and added with menthol.

帶濾嘴香煙中,為調整吸煙時的煙中成分之目的,已知有在濾嘴上設置通氣孔以調整空氣流量的方法。 In the filter cigarette, for the purpose of adjusting the components in the smoke during smoking, a method of providing a vent hole in the filter to adjust the air flow is known.

同時,在一般的帶濾嘴香煙中,已知可配合煙中成分量而調整濾嘴的通氣阻力。 Meanwhile, in a general filter cigarette, it is known that the ventilation resistance of the filter can be adjusted in accordance with the amount of components in the smoke.

專利文獻1中揭示的帶濾嘴香煙,係具有濾嘴的通氣阻力為50mmH2O/100mm(相當於13.5mmH2O/27mm)、通氣比率為20至80%的濾嘴。 The filter cigarette disclosed in Patent Document 1 has a filter having a filter having a ventilation resistance of 50 mmH 2 O/100 mm (corresponding to 13.5 mm H 2 O/27 mm) and a ventilation ratio of 20 to 80%.

同時,專利文獻2中記載一種具有2個濾段的帶濾嘴香煙,2個濾段之中,因可將1個濾段的通氣阻力調整成比另一個者更大,使來自包捲濾嘴的水松紙(tipping paper,又稱外層紙)之空氣流量調整為固定範圍,故不論是減少主流煙中的尼古丁及焦油的濃度,也可呈現充分的吸食感。 Meanwhile, Patent Document 2 describes a filter cigarette having two filter segments, and among the two filter segments, since the ventilation resistance of one filter segment can be adjusted to be larger than the other, the filter is supplied from the package. The air flow of the tipping paper (also known as the outer paper) is adjusted to a fixed range, so that it can exhibit a sufficient sense of sucking regardless of the concentration of nicotine and tar in the mainstream smoke.

另一方面,日本市場中對薄荷醇香煙的需求逐年增 高,而投入過去一直未曾有過的高薄荷醇香煙市場。專利文獻3中記載一種在濾嘴中添加如薄荷醇的香料之方法,係將濾嘴的製程使用的塑化劑中溶解或分散有薄荷醇的芳香液添加在乙酸纖維絲束(tow)中。 On the other hand, the demand for menthol cigarettes in the Japanese market is increasing year by year. High, and invest in the high menthol cigarette market that has never been seen before. Patent Document 3 describes a method of adding a fragrance such as menthol to a filter by adding a menthol-dissolved fragrance in a plasticizer used in a filter process to an acetic acid tow (tow). .

專利文獻4中記載一種使薄荷醇保存在香料的載體上以防薄荷醇量隨著經過時日而降低之方式。 Patent Document 4 describes a method in which menthol is stored on a carrier of a fragrance to prevent the amount of menthol from decreasing as time passes.

同時,專利文獻5中記載一種使用具有保香性的薄片以防薄荷醇量隨著經過時日而降低之方式。 Meanwhile, Patent Document 5 describes a method of using a sheet having a fragrance-preserving property to prevent the amount of menthol from decreasing as time passes.

同時,專利文獻6中記載一種為了防止煙中薄荷醇量隨著經過時日降低而預先將香料添加吸附的濾嘴之製造方法等。 At the same time, Patent Document 6 describes a method for producing a filter for preventing the amount of menthol in the smoke from being adsorbed and adsorbed in advance in order to prevent the amount of menthol in the smoke from decreasing.

[先前技術文獻] [Previous Technical Literature] [專利文獻] [Patent Literature]

[專利文獻1]日本實開昭62-86894號公報 [Patent Document 1] Japanese Unexamined Publication No. 62-86894

[專利文獻2]日本特開平11-069965號公報 [Patent Document 2] Japanese Patent Laid-Open No. Hei 11-069965

[專利文獻3]日本特公昭43-28077號公報 [Patent Document 3] Japanese Patent Publication No. 43-28077

[專利文獻4]日本特開2012-29637號公報 [Patent Document 4] Japanese Patent Laid-Open Publication No. 2012-29637

[專利文獻5]國際公開第2011/118040號公報 [Patent Document 5] International Publication No. 2011/118040

[專利文獻6]國際公開第2012/004853號公報 [Patent Document 6] International Publication No. 2012/004853

上述專利文獻1中記載之發明,雖然是已將濾嘴的通氣阻力與空氣自設在水松紙上的開孔部位流入之 比率調整為固定範圍者,但並不了解其目的。 The invention described in the above Patent Document 1 has infiltrated the ventilation resistance of the filter and the opening portion of the air which is set on the tipping paper. The ratio is adjusted to a fixed range, but the purpose is not understood.

同時,在專利文獻2中記載之發明,其目的是一邊使煙中成分的尼古丁或焦油之量減少,一邊使香煙製品的通氣阻力提高,而可呈現充分的吸食感。 Meanwhile, the invention described in Patent Document 2 has an object of improving the ventilation resistance of a cigarette product while reducing the amount of nicotine or tar in the smoke component, thereby exhibiting a sufficient feeling of smoking.

香煙用濾嘴的性質,一般在通氣比率低且具有高焦油量的帶濾嘴香煙中係使用低通氣阻力的濾嘴,而在具有高通氣比率的低焦油量之帶濾嘴香煙中係使用高通氣阻力的濾嘴。 The nature of the filter for cigarettes is generally a filter with low ventilation resistance in a filter cigarette with a low ventilation ratio and a high tar amount, and is used in a filter cigarette with a low tar amount having a high ventilation ratio. Filter with high ventilation resistance.

如上述,雖然已有進行專注於濾嘴的通氣阻力或通氣比率(空氣流入量)之研究,但尚未嘗試將添加有薄荷醇之濾嘴香煙,尤其是將專門低焦油量之帶濾嘴香煙調整其通氣阻力或通氣比率。 As mentioned above, although studies have been conducted focusing on the ventilation resistance or ventilation ratio (air inflow) of the filter, it has not been attempted to add a filter cigarette with menthol, especially a filter cigarette with a special low tar amount. Adjust the ventilation resistance or ventilation ratio.

另一方面,具有薄荷醇的帶濾嘴香煙在吸煙時的煙中薄荷醇量,雖然可依添加在香煙中的薄荷醇之芳香量而調整,但要單純地增加添加在香煙中的芳香量時,由於在覆蓋香煙絲的捲紙上發生已溶解香煙色素的薄荷醇之暈染而附著在捲紙上,而使外觀造成不佳的狀態。同時,由於煙中薄荷醇係依香煙的焦油量之比例變高,故一般對於所謂低焦油的焦油量為5mg以下之香煙,通常會使煙中薄荷醇量變低,其解決對策除了在香煙中儘可能地添加不致引起暈染等問題的最大量以外,並無其他的方法。 On the other hand, the amount of menthol in the smoke of the filter cigarette having menthol during smoking can be adjusted according to the amount of menthol added to the cigarette, but simply increase the amount of aroma added to the cigarette. At this time, since the menthol which dissolves the cigarette coloring occurs on the roll paper covering the cigarette thread, it adheres to the roll paper, and the appearance is not good. At the same time, since the proportion of menthol in the cigarette is higher than that of the cigarette, generally, for a cigarette having a low tar tar content of 5 mg or less, the amount of menthol in the cigarette is generally lowered, and the solution is in addition to the cigarette. There is no other way to add as much as possible to the maximum amount that does not cause problems such as blooming.

在專利文獻3記載之方法中,係使添加在濾嘴部的薄荷醇,在製品存放中吸附於濾嘴之絲束,會有煙中薄荷醇隨著經過時日而明顯降低的問題。 In the method described in Patent Document 3, the menthol added to the filter portion is adsorbed to the tow of the filter during storage of the product, and there is a problem that the menthol in the smoke significantly decreases as time passes.

在專利文獻4記載之方法中,在使用香料的載體而增加成本或在濾嘴內部添加載體時,由於必需另外設置載體的添加步驟,而可舉出使製造適性變得複雑且困難等問題。 In the method described in Patent Document 4, when the carrier of the fragrance is used to increase the cost or the carrier is added to the inside of the filter, it is necessary to additionally provide a step of adding the carrier, and it is difficult to reproduce the manufacturing suitability.

專利文獻5中記載之發明,也與專利文獻4中所述的發明相同,恐有成本增加或隨著對香煙絲添加保香性之薄片的對香煙製造適性之問題。 The invention described in Patent Document 5 is also the same as the invention described in Patent Document 4, and there is a fear that the cost is increased or the compatibility with the cigarette is added to the tobacco yarn.

在專利文獻6記載之發明中,欲增加煙中薄荷醇量的方式,雖然已說明對濾嘴增加薄荷醇添加量之方式,但欲在濾嘴的塑化劑中添加薄荷醇,則必須選定可溶解薄荷醇的塑化劑。由於薄荷醇不易溶解於通常使用作為塑化劑的三乙酸甘油酯中,故必須混合如聚乙二醇的溶劑,使薄荷醇溶解而調製芳香液。同時如欲添加較多量的薄荷醇時,由於必須有多量的塑化劑及可溶解薄荷醇的其他溶劑,故恐有芳香液的暈染或對濾嘴的硬度等的影響。同時,意圖使薄荷醇吸附到濾嘴內部時,由於僅將薄荷醇混合添加至塑化劑中的效果低,同時花費較長的時間,故例如同時將薄荷醇與塑化劑添加至乙酸酯纖維中時,必須進行高溫處理。不過,此等步驟必須在濾嘴的製造時或剛製造後就設置其它步驟,難以說是適用在實際步驟上的技術。 In the invention described in Patent Document 6, in order to increase the amount of menthol in the smoke, although the method of adding the amount of menthol to the filter has been described, it is necessary to add menthol to the plasticizer of the filter. A plasticizer that dissolves menthol. Since menthol is not easily dissolved in triacetin which is usually used as a plasticizer, it is necessary to mix a solvent such as polyethylene glycol to dissolve menthol to prepare a fragrance. At the same time, if a large amount of menthol is to be added, since a large amount of plasticizer and other solvents which can dissolve menthol must be present, there is a fear that the fragrance may be smudged or the hardness of the filter may be affected. Meanwhile, when it is intended to adsorb menthol to the inside of the filter, since the effect of merely adding menthol to the plasticizer is low and takes a long time, for example, menthol and a plasticizer are simultaneously added to the acetic acid. In the case of ester fibers, high temperature treatment must be carried out. However, these steps must be performed at the time of manufacture of the filter or immediately after manufacture, and it is difficult to say that it is a technique applicable to actual steps.

濾嘴的通氣阻力及帶濾嘴香煙的通氣比率,並無與吸煙時的煙中薄荷醇濃度相關的探討例,即使在薄荷醇製品中,也在探求提高低焦油香煙的吸煙時之煙中薄荷醇量或貯存後的煙中薄荷醇量之安定性的技術。 The ventilation resistance of the filter and the ventilation ratio of the filter cigarette are not related to the concentration of menthol in the smoke when smoking. Even in the menthol product, it is also sought to improve the smoking of low-tar cigarettes. A technique for the stability of the amount of menthol or the amount of menthol in the smoke after storage.

本發明中係提供一種低焦油薄荷醇香煙, 其可提高吸煙時的煙中薄荷醇量,同時可使貯存後的煙中薄荷醇量之變化少。 In the present invention, a low tar menthol cigarette is provided. It can increase the amount of menthol in the smoke when smoking, and at the same time can reduce the amount of menthol in the smoke after storage.

本發明人等深入探討的結果瞭解,低焦油薄荷醇香煙可解決上述問題,而完成本發明,其係具有煙桿部與經水松紙包捲的濾嘴部之焦油量為5mg以下的低焦油薄荷醇香煙,前述濾嘴部包含以纖維素乙酸酯絲束(tow)構成的單一節段,前述濾嘴部的通氣阻力為25至80mmH2O/27mm,同時空氣自穿設在前述水松紙上的通氣孔流入之通氣比率為55%以上,而前述濾嘴中添加有薄荷醇。 As a result of intensive investigation by the present inventors, it is understood that the low tar menthol cigarette can solve the above problems, and the present invention has the low tar content of the tobacco rod portion and the filter portion wrapped with the tipping paper of 5 mg or less. a tarp citric acid cigarette, wherein the filter portion comprises a single segment composed of cellulose acetate tow, and the filter portion has a ventilation resistance of 25 to 80 mm H 2 O/27 mm, and air is self-piercing at the foregoing The ventilation ratio of the vent hole in the tipping paper is 55% or more, and menthol is added to the filter.

亦即,本發明係如下述。 That is, the present invention is as follows.

[1]一種低焦油薄荷醇香煙,係具有煙桿部與經水松紙包捲的濾嘴部之焦油量為5mg以下的低焦油薄荷醇香煙,前述濾嘴部包含以纖維素乙酸酯絲束構成的單一節段,前述濾嘴部的通氣阻力為25至80mmH2O/27mm,同時空氣自穿設在前述水松紙上的通氣孔流入之通氣比率為55%以上,且前述濾嘴部中添加有薄荷醇。 [1] A low tar menthol cigarette, which is a low tar menthol cigarette having a tar portion of a tobacco rod portion and a filter portion wrapped with tipping paper of 5 mg or less, wherein the filter portion comprises cellulose acetate. a single segment formed by the tow, wherein the filter portion has a ventilation resistance of 25 to 80 mmH 2 O/27 mm, and the air has a ventilation ratio of 55% or more from the vent hole penetrating the tipping paper, and the filter is Menthol is added to the part.

[2]如[1]所述之低焦油薄荷醇香煙,其中,薄荷醇對濾嘴部的添加量,係每支低焦油薄荷醇香煙為8mg/支以上。 [2] The low tar menthol cigarette according to [1], wherein the amount of menthol added to the filter portion is 8 mg/piece or more per low tar menthol cigarette.

[3]如[1]或[2]所述之低焦油薄荷醇香煙,其中,前述煙桿部或濾嘴部具有阻力體。 [3] The low tar menthol cigarette according to [1] or [2] wherein the tobacco rod portion or the filter portion has a resistance body.

[4]如[3]所述之低焦油薄荷醇香煙,其中,前述阻力體為膠囊或孔口。 [4] The low tar menthol cigarette according to [3], wherein the aforementioned resistance body is a capsule or an orifice.

[5]如[1]至[4]中任一項所述之低焦油薄荷醇香煙,其中, 前述濾嘴部的通氣阻力為25至50mmH2O/27mm,同時空氣流入的通氣比率為70%以上。 [5] The low tar menthol cigarette according to any one of [1] to [4] wherein the filter portion has a ventilation resistance of 25 to 50 mmH 2 O/27 mm, and the air inflow ratio is 70. %the above.

[6]如[1]至[5]中任一項所述之低焦油薄荷醇香煙,其中,前述低焦油薄荷醇香煙的圓周為20.0至27.0mm。 [6] The low tar menthol cigarette according to any one of [1] to [5] wherein the aforementioned low tar menthol cigarette has a circumference of 20.0 to 27.0 mm.

本發明的低焦油薄荷醇香煙,可提高吸煙時的煙中薄荷醇量,同時可使貯存後的煙中薄荷醇量之變化少。 The low tar menthol cigarette of the present invention can increase the amount of menthol in the smoke when smoking, and at the same time, can reduce the amount of menthol in the smoke after storage.

第1圖表示帶濾嘴香煙的貯存期間與煙中薄荷醇量的減少率之關係圖。 Fig. 1 is a graph showing the relationship between the storage period of the filter-tipped cigarette and the reduction rate of the amount of menthol in the cigarette.

第2圖表示貯存後的帶濾嘴香煙中的初期薄荷醇添加量與薄荷醇釋放率之關係圖。 Fig. 2 is a graph showing the relationship between the amount of initial menthol added and the menthol release rate in the filter-tipped cigarette after storage.

以下,雖呈示實施形態及例示物等以詳細地說明本發明,但本發明並不侷限於以下的實施形態及例示物等,在不偏離本發明的主旨之範圍中可實施任意的改變。 In the following, the present invention is not limited to the following embodiments and examples, and the present invention is not limited to the scope of the invention.

本發明的低焦油薄荷醇香煙,係具有煙桿部與經水松紙包捲的濾嘴部之帶濾嘴香煙,前述濾嘴部包含以單一的纖維素乙酸酯絲束構成的單一節段,前述濾嘴部的通氣阻力為25至80mmH2O/27mm,同時空氣自穿設在前述水松紙上的通氣孔流入之通氣比率為55%以上,前述濾嘴中添加有薄荷醇。 The low tar menthol cigarette of the present invention is a filter cigarette having a tobacco stem portion and a filter portion wrapped with tipping paper, the filter portion comprising a single section composed of a single cellulose acetate tow. In the section, the ventilation resistance of the filter portion is 25 to 80 mmH 2 O/27 mm, and the air is infused with a vent ratio of 55% or more from the vent hole penetrating the tipping paper, and menthol is added to the filter.

煙桿可採用習知的形態。香煙的煙絲種類並無特別的限定,可使用習知者,係將此以捲紙包捲的煙桿。煙桿中,為了調整低焦油薄荷醇香煙(帶濾嘴香煙)的通氣阻力之目的,可在桿的內部配置如膠囊或孔口的阻力體。 The tobacco rod can take a conventional form. The type of cut tobacco of the cigarette is not particularly limited, and a conventionally used person may be a tobacco rod wrapped in a roll paper. In the tobacco rod, in order to adjust the ventilation resistance of the low tar menthol cigarette (with a filter cigarette), a resistance body such as a capsule or an orifice may be disposed inside the rod.

構成本發明的低焦油薄荷醇香煙之濾嘴部,係以水松紙包捲。本發明中可使用的水松紙並無特別的限制,可使用不透氣者。 The filter portion constituting the low tar menthol cigarette of the present invention is wrapped with tipping paper. The tipping paper which can be used in the present invention is not particularly limited, and those which are impermeable can be used.

水松紙中,因設置可使空氣沿者包捲濾嘴的圓周方向穿設之數個開孔(通氣孔)形成的空氣流入手段,而可調整空氣自穿設在低焦油薄荷醇香煙的前述水松紙上的通氣孔流入之通氣比率。開孔的形態,可舉出設置成沿著濾嘴的圓周方向為一列以上的形態。 In the tipping paper, the air inflow means formed by the plurality of openings (vent holes) through which the air is circulated in the circumferential direction of the packaged filter is provided, and the air can be adjusted from being immersed in the low tar menthol cigarette. The ventilation ratio of the vent hole in the aforementioned tipping paper. The form of the opening may be in the form of one or more rows along the circumferential direction of the filter.

形成有數個穿設開孔的水松紙之透氣度,通常是100至7,000C.U.。此處的C.U.,係表示差壓為100mmH2O(980.665Pa)時,1分鐘(60秒)內可通過水松紙1cm2(100mm2)的流量(mL,(0.001L))。 The air permeability of the tipping paper formed with several openings is usually 100 to 7,000 CU. Here, CU means a flow rate (mL, (0.001 L)) of 1 cm 2 (100 mm 2 ) of tipping paper in 1 minute (60 seconds) when the differential pressure is 100 mmH 2 O (980.665 Pa).

本發明的低焦油薄荷醇香煙之空氣流入的通氣比率為55%以上。此通氣比率是以61%以上為佳,並以70%以上更佳。成為此等的通氣比率時,可使吸煙者更強烈地感覺到薄荷醇的香味。此通氣比率時的濾嘴的通氣阻力,係如後述的80mmH2O/27mm以下。 The low tar menthol cigarette of the present invention has an air inflow ratio of 55% or more. The ventilation ratio is preferably 61% or more, and more preferably 70% or more. When these ventilation ratios are obtained, the smoker can feel the scent of menthol more strongly. The ventilation resistance of the filter at this ventilation ratio is 80 mmH 2 O/27 mm or less which will be described later.

本發明中的空氣流入之通氣比率,係指以百分率表示相對於以標準流量17.5cm3/秒吸取帶濾嘴香煙(製品)時吸 口端中的空氣流量,通過(具有空氣流入手段)水松紙而攝入帶濾嘴香煙內部的空氣流量之比。 The air inflow ratio in the present invention means the flow rate of air in the mouth end when sucking the filter cigarette (product) at a standard flow rate of 17.5 cm 3 /sec, in percentage (by means of air inflow means) The ratio of air flow in the interior of a cigarette with filter paper.

空氣流入的通氣比率,例如可因改變上述數個開孔的大小、數及列的個數,或改變水松紙的材質而改變透氣度而調整。例如,開孔的位置可配置在離吸口端12至20mm的位置上。 The ventilation ratio of the air inflow can be adjusted, for example, by changing the size, number, and number of the plurality of openings, or changing the material of the tipping paper to change the air permeability. For example, the position of the opening may be disposed at a position of 12 to 20 mm from the end of the suction port.

本發明中,濾嘴部的通氣阻力,係指不使空氣自濾嘴部的側面流入之方式以不透氣性橡膠覆蓋濾嘴部,自其一端以17.5cm3/秒的流量吸取時之濾嘴部中的壓差PD(mmH2O)。 In the present invention, the ventilation resistance of the filter portion refers to a filter that covers the filter portion with a gas-impermeable rubber so as not to allow air to flow from the side surface of the filter portion, and is filtered at a flow rate of 17.5 cm 3 /sec from one end thereof. The pressure difference PD (mmH 2 O) in the mouth.

構成本發明的低焦油薄荷醇香煙之濾嘴部,係包含單一節段者。換言之,本發明的帶濾嘴香煙中使用的濾嘴部,具有由纖維素乙酸酯絲束構成的單一節段。同時,在由纖維素乙酸酯絲束構成的節段中,可具有如膠囊或孔口的阻力體。 The filter portion constituting the low tarp menthol cigarette of the present invention includes a single segment. In other words, the filter portion used in the filter cigarette of the present invention has a single segment composed of cellulose acetate tow. Meanwhile, in the segment composed of the cellulose acetate tow, there may be a resistance body such as a capsule or an orifice.

本發明的低焦油薄荷醇香煙的濾嘴部之通氣阻力,在濾嘴部上配置如膠囊或孔口的阻力體時,係以不包含該阻力體的濾嘴之該值為基準。 In the ventilation resistance of the filter portion of the low tarp menthol cigarette of the present invention, when a resistance body such as a capsule or an orifice is disposed on the filter portion, the value of the filter that does not include the resistance body is used as a reference.

膠囊或孔口的形狀並無特別的限制,可適用習知者。 The shape of the capsule or the orifice is not particularly limited and can be applied to a person skilled in the art.

本發明中使用的濾嘴部之以纖維素乙酸酯絲束構成單一節段之構成材料,係纖維素乙酸酯。構成纖維素乙酸酯絲束的纖維素乙酸酯纖維,可列舉:例如單紗纖度為1.0至8.0丹尼左右,且總纖度為15,000至70,000丹尼的形態,同時,可舉出纖維剖面形狀為圓形、橢圓形、Y字型、X 字型、I字型者。濾嘴內部係可列舉例如:經纖維素乙酸酯絲束均勻充填者。 The filter portion used in the present invention is a constituent material of a single segment composed of cellulose acetate tow, which is cellulose acetate. The cellulose acetate fiber constituting the cellulose acetate tow may, for example, be a single yarn having a fineness of about 1.0 to 8.0 denier and a total fineness of from 15,000 to 70,000 denier, and a fiber cross section is exemplified. The shape is circular, elliptical, Y-shaped, X Font type, I type. The inside of the filter may, for example, be a uniform filling with cellulose acetate tow.

本發明的低焦油薄荷醇香煙中使用的濾嘴部之通氣阻力,係25至80mmH2O/27mm。又,通氣阻力的單位中使用的「27mm」,係指濾嘴部的縱向長度。 The ventilation resistance of the filter portion used in the low tar menthol cigarette of the present invention is 25 to 80 mmH 2 O/27 mm. Further, "27 mm" used in the unit of the ventilation resistance means the longitudinal length of the filter portion.

因濾嘴部之通氣阻力為25mmH2O/27mm以上,故可在吸煙時充分進行煙的過濾。另一方面,因濾嘴部的通氣阻力為80mmH2O/27mm以下,故在吸煙時不會引起過度的煙過濾,而可有效地降低薄荷醇之過濾率。同時,因濾嘴的密度低,故在貯存中不易使薄荷醇吸附。 Since the ventilation resistance of the filter portion is 25 mmH 2 O/27 mm or more, the smoke can be sufficiently filtered at the time of smoking. On the other hand, since the ventilation resistance of the filter portion is 80 mmH 2 O/27 mm or less, excessive smoke filtration is not caused during smoking, and the filtration rate of menthol can be effectively reduced. At the same time, because of the low density of the filter, it is not easy to adsorb menthol during storage.

因使濾嘴的通氣阻力在此範圍,且將帶濾嘴香煙的通氣比率設在後述的固定範圍,故可使煙中薄荷醇濃度容納在所需的範圍內。同時,在前述濾嘴部的通氣阻力為25至50mmH2O/27mm,同時空氣流入的通氣比率為70%以上時,此效果更為良好。 Since the ventilation resistance of the filter is within this range, and the ventilation ratio of the filter cigarette is set to a fixed range to be described later, the concentration of menthol in the smoke can be accommodated within a desired range. At the same time, when the ventilation resistance of the filter portion is 25 to 50 mmH 2 O/27 mm, and the air inflow ratio is 70% or more, the effect is further improved.

對於調整濾嘴的通氣阻力,可如過去所知的例如適當地選擇纖維素乙酸酯絲束之總纖度(充填量)及單紗纖度而調整,具體上,纖維素乙酸酯絲束的規格,如增大單紗纖度、減小總纖度時,即可減少通氣阻力。 For adjusting the ventilation resistance of the filter, it can be adjusted as previously known, for example, by appropriately selecting the total fineness (filling amount) of the cellulose acetate tow and the single yarn fineness, specifically, the cellulose acetate tow. Specifications, such as increasing the single yarn fineness and reducing the total fineness, can reduce the ventilation resistance.

濾嘴中使用的絲束重量,係將濾嘴長度設為27mm時之值,可列舉:例如0.100至0.200g,也可用此範圍調節重量而調整濾嘴的密度。 The weight of the tow used in the filter is a value obtained by setting the length of the filter to 27 mm, and for example, 0.100 to 0.200 g, and the weight can be adjusted by adjusting the range to adjust the density of the filter.

本發明的低焦油薄荷醇香煙中,如不存在阻力體時,每1支的通氣阻力(1支帶濾嘴香煙的通氣阻 力),可舉出大約20至70mmH2O的形態。 In the low tar menthol cigarette of the present invention, when there is no resistance body, the ventilation resistance per one branch (the ventilation resistance of the one-pack filter cigarette) may be in the form of about 20 to 70 mmH 2 O.

此處,1支帶濾嘴香煙的通氣阻力,係指含有由濾嘴的一端以17.5cm3/秒的流量吸取時之通氣效果的1支帶濾嘴香煙中的壓差PD(mmH2O)。換言之,帶濾嘴香煙1支的通氣阻力,係以將桿部與濾嘴部連結的製品狀態測定之通氣阻力。 Here, the ventilation resistance of one filter cigarette is a pressure difference PD (mmH 2 O) in a filter cigarette containing a ventilating effect when one end of the filter is sucked at a flow rate of 17.5 cm 3 /sec. ). In other words, the ventilation resistance of one of the filter cigarettes is the ventilation resistance measured by the state of the product connecting the rod portion and the filter portion.

本發明的低焦油薄荷醇香煙,其焦油量為5mg以下。本發明中所言之焦油量,係指吸煙時吸煙者吸入的焦油量。 The low tar menthol cigarette of the present invention has a tar amount of 5 mg or less. The amount of tar referred to in the present invention refers to the amount of tar inhaled by the smoker at the time of smoking.

欲使焦油量成為5mg以下,即欲使目標焦油量成為5mg以下時,可藉由改變含在煙桿中的煙絲組成,或使濾嘴部的通氣阻力或低焦油薄荷醇香煙的通氣比率變化而調整。 If the amount of tar is to be 5 mg or less, that is, when the target tar amount is 5 mg or less, the composition of the tobacco contained in the tobacco rod may be changed, or the ventilation resistance of the filter portion or the ventilation ratio of the low tar menthol cigarette may be changed. And adjust.

5mg以下的焦油量之形態,例如可在0.5至5mg的範圍中適當地調整。在本發明的低焦油薄荷醇香煙中,即使為如此低焦油量者,也可提供吸煙者十足的薄荷醇之香味感。 The form of the tar amount of 5 mg or less can be appropriately adjusted, for example, in the range of 0.5 to 5 mg. In the low tar menthol cigarette of the present invention, even if it is such a low tar amount, the scent of menthol of the smoker can be provided.

帶濾嘴香煙的焦油量,係遵照ISO吸煙條件(ISO4387),例如將20支作為1次測定而測定。測定是利用氣體層析儀。 The amount of tar with a filter cigarette is in accordance with ISO smoking conditions (ISO 4387), for example, 20 measurements are taken as one measurement. The measurement was performed using a gas chromatograph.

本發明的低焦油薄荷醇香煙,係在濾嘴中添加薄荷醇。濾嘴中的薄荷醇之添加處,可列舉:例如在構成濾嘴的纖維束乙酸酯絲束之10至100體積%的部添加的形態。其添加方法,可舉出在構成帶濾嘴香煙之前預先 於濾嘴的纖維素乙酸酯絲束中添加的方法,也可在構成帶濾嘴香煙之後添加的方法。 The low tar menthol cigarette of the present invention is added with menthol to the filter. The addition of menthol in the filter may be, for example, a form of addition of 10 to 100% by volume of the fiber bundle acetate tow constituting the filter. The method of addition can be exemplified before the cigarette with the filter is formed. The method of adding to the cellulose acetate tow of the filter may also be a method of adding after the filter cigarette is constructed.

薄荷醇的添加方法,並無特別的限制,可使用已知的方法。薄荷醇可為合成者,亦可為來自天然物者。 The method of adding menthol is not particularly limited, and a known method can be used. Menthol can be either a synthetic or a natural product.

本發明的低焦油薄荷醇香煙中,添加至濾嘴中的薄荷醇之量,係以8mg/支以上為佳。薄荷醇的添加量為8mg/支以上時,可使貯存後的煙中薄荷醇之量更為安定。使貯存後的煙中薄荷醇之量更為安定,係指帶濾嘴香煙經貯存後的吸煙時薄荷醇自濾嘴部釋放之量,即使經過貯存時間也可保持在接近固定範圍。薄荷醇對濾嘴部的添加量,係以10mg/支以上更佳,並以12mg/支以上為特佳。另一方面,薄荷醇量的上限,可舉出20mg/支以下的形態。 In the low tar menthol cigarette of the present invention, the amount of menthol added to the filter is preferably 8 mg / more. When the amount of menthol added is 8 mg/piece or more, the amount of menthol in the smoke after storage can be made more stable. The amount of menthol in the stored cigarette is more stable, which means that the amount of menthol released from the filter portion after smoking with the filter cigarette is kept close to a fixed range even after storage time. The amount of menthol added to the filter portion is preferably 10 mg/piece or more, and particularly preferably 12 mg/piece or more. On the other hand, the upper limit of the amount of menthol is 20 mg/min or less.

本發明的低焦油薄荷醇香煙中可使用的濾嘴之軸向(長度向)長度,例如可使用15至35mm者。 The axial (lengthwise) length of the filter which can be used in the low tarp menthol cigarette of the present invention can be, for example, 15 to 35 mm.

同時,本發明的低焦油薄荷醇香煙之圓周,可舉出20.0至27.0mm的形態,並以24.0至26.0mm的形態更佳。在此等範圍內時,可適於確保煙中的高薄荷醇濃度,與安定的保存貯存後之薄荷醇濃度。 Meanwhile, the circumference of the low tarp menthol cigarette of the present invention may be in the form of 20.0 to 27.0 mm, and more preferably in the form of 24.0 to 26.0 mm. Within these ranges, it may be suitable to ensure a high menthol concentration in the smoke, and a menthol concentration after storage and storage.

本發明的低焦油薄荷醇香煙之全長,可舉出80至100mm的形態。 The total length of the low tar menthol cigarette of the present invention is in the form of 80 to 100 mm.

<低焦油薄荷醇香煙的製造方法> <Method for producing low tar menthol cigarette>

本發明的低焦油薄荷醇香煙,係除了使用已在濾嘴中添加有薄荷醇且設定濾嘴的通氣阻力為固定範圍者,並且將空氣流入的通氣比率設定在固定範圍以外,可使用習知 的方法製造。 The low tar menthol cigarette of the present invention can be used in addition to the use of menthol added to the filter and setting the ventilation resistance of the filter to a fixed range, and setting the ventilation ratio of the air inflow outside the fixed range. Method of manufacturing.

即使在煙桿中摻入如孔口的阻力體時,亦可使用習知的方法。 Even if a resistance body such as an orifice is incorporated into the tobacco rod, a conventional method can be used.

構成本發明的低焦油薄荷醇香煙之煙桿部,可舉出包含形成煙桿的煙絲與包捲其之捲紙的形態,其材料或形狀,只要是可成為本發明中規定的低焦油者,即可無限定地使用習知者。 The tobacco rod portion constituting the low tarp menthol cigarette of the present invention may be in the form of a tobacco sheet including a tobacco rod and a roll paper wrapped therein, and the material or shape thereof may be a low tar oil which can be specified in the present invention. , the conventional person can be used without limitation.

煙桿部的圓周,可舉出與上述說明之本發明的低焦油薄荷醇香煙的圓周相同的範圍。 The circumference of the tobacco rod portion may be the same as the circumference of the low tarp menthol cigarette of the present invention described above.

煙桿部的軸向長度,可列舉:例如50至75mm。 The axial length of the tobacco rod portion may be, for example, 50 to 75 mm.

[實施例] [Examples]

雖以實施例更具體地說明本發明,但本發明在不超出其主旨下,並不侷限於以下實施例中所述之範圍。 The present invention will be more specifically described by the examples, but the present invention is not limited to the scope of the embodiments described below.

<實施例1> <Example 1>

實施例1、2及比較例1、2 Examples 1, 2 and Comparative Examples 1, 2

以設計成濾嘴的通氣阻力低、空氣流入的通氣比率高之香煙,驗證可使煙中薄荷醇量變高的目的,而製作具有表1所示的濾嘴通氣阻力及通氣比率之香煙,進行每支香煙的煙中薄荷醇量及焦油量之測定。此時,製作的濾嘴是以3週、溫度22℃、濕度60%的條件貯存保管,使薄荷醇充分地吸附在纖維素乙酸酯絲束中並穩定,而使用於煙捲上。同時製作的香煙,通常是在鋁箔包裝後的3週內以溫度22℃、濕度60%的條件貯存保管,實施煙中薄荷醇量及 焦油量之測定。又,表中的絲束規格,係表示單紗纖度.剖面形狀.總纖度,例如5.9Y35000,係指單紗纖度為5.9丹尼、剖面形狀為Y型及總纖度為35,000丹尼的纖維素乙酸酯絲束。 By designing a cigarette having a low ventilation resistance of a filter and a high ventilation ratio of air inflow, it is verified that the amount of menthol in the smoke can be increased, and a cigarette having a filter ventilation resistance and a ventilation ratio shown in Table 1 is produced. Determination of the amount of menthol and the amount of tar in the smoke of each cigarette. At this time, the produced filter was stored and stored under the conditions of 3 weeks, a temperature of 22 ° C, and a humidity of 60%, and the menthol was sufficiently adsorbed to the cellulose acetate tow and stabilized, and used for the cigarette. The cigarettes produced at the same time are usually stored and stored at a temperature of 22 ° C and a humidity of 60% within 3 weeks after packaging of the aluminum foil, and the amount of menthol in the smoke is carried out. Determination of the amount of tar. Also, the tow specification in the table indicates the single yarn fineness. Section shape. The total fineness, for example, 5.9Y35000, refers to a cellulose acetate tow having a single yarn fineness of 5.9 denier, a cross-sectional shape of Y type, and a total fineness of 35,000 denier.

試驗中使用的香煙,係使用全長長度為84mm、濾嘴長為27mm者。煙絲是使用美國混合型,煙絲的充填量設為0.580g,對於煙絲重量加入12,000ppm之薄荷醇。同時使濾嘴出口的焦油量成為5mg之方式,設定各香煙濾嘴的通氣阻力及通氣比率。 The cigarette used in the test was a full length of 84 mm and a filter length of 27 mm. The shredded tobacco was mixed with American type, the filling amount of shredded tobacco was set to 0.580 g, and 12,000 ppm of menthol was added to the shredded tobacco weight. At the same time, the amount of tar at the outlet of the filter was set to 5 mg, and the ventilation resistance and the ventilation ratio of each cigarette filter were set.

香煙的抽吸,係依照ISO吸煙條件實施,薄荷醇測定是將20支作為1次測定之支數,重複測定2次,焦油測定是將20支作為1次測定之支數,測定1次。煙中薄荷醇量及焦油量,係利用Agilent公司製的GC-FID7693(薄荷醇測定、尼古丁測定)、Agilent公司製的GC-TCD-7890A(水份測定),實施每支香煙的薄荷醇量及焦油量之測定。通氣比率,係利用SODIM公司製的SODIMAX, 測定自水松紙的開孔部流入的空氣流入比率。 The smoking of cigarettes was carried out in accordance with ISO smoking conditions, and the measurement of menthol was carried out by repeating the measurement of 20 counts as one count of the first measurement, and the tar measurement was performed by measuring 20 counts as the count of one measurement. The amount of menthol and the amount of tar in the smoke were measured by GC-FID7693 (menthol measurement, nicotine measurement) manufactured by Agilent, and GC-TCD-7890A (moisture measurement) manufactured by Agilent Co., Ltd., and the amount of menthol per cigarette was carried out. And the determination of the amount of tar. The ventilation ratio is based on SODIMAX made by SODIM. The inflow rate of air flowing in from the opening portion of the tipping paper was measured.

同時對於製作的表1所示之4種香煙合併薄荷醇感覺的感官評估。評估方法,係在4種的香煙中,以最一般的條件組合的比較例1為對照,進行和其他3個的薄荷醇感覺為高或相同或低之2擇1的問題。本評估時,係以10人作為對象人數,藉由累積二項式分佈概率(單側),合併實施顯著差異確認在5%的顯著性水準。 At the same time, a sensory evaluation of the menthol sensation of the four cigarettes shown in Table 1 was prepared. In the evaluation method, Comparative Example 1 in which the most common conditions were combined among the four kinds of cigarettes was used as a control, and the other three menthols were perceived to be high or the same or lower. In this assessment, 10 people were used as the target number, and by accumulating the binomial distribution probability (one side), the significant difference was combined and confirmed at the 5% significance level.

以下的表2,係除了煙中薄荷醇量及焦油量之外,也表示以薄荷醇量除以焦油量之值(以下,簡記為M/T比),可獲得同等焦油量時的不同薄荷醇量為指標。通常由於煙中薄荷醇量是以焦油量而比例變高,故此處係使用經焦油量規格化之值比較薄荷醇量。同時,合併的感官評估結果,係記載為顯著差異之有無。 Table 2 below shows the difference between the amount of menthol and the amount of tar in addition to the amount of menthol in the smoke (hereinafter, abbreviated as M/T ratio), and different mints when the same amount of tar is obtained. The amount of alcohol is an indicator. Usually, since the amount of menthol in the smoke is increased in proportion to the amount of tar, the amount of mentol normalized is used to compare the amount of menthol. At the same time, the combined sensory evaluation results are recorded as the presence or absence of significant differences.

由表2可知,設計成濾嘴的通氣阻力較低、空氣流入的通氣比率較高之香煙,可使煙中薄荷醇量及 M/T比變高值。此可認為乃因在濾嘴的通氣阻力與通氣比率之關係中,焦油與薄荷醇之過濾率不同而致。具體上,使用低通氣阻力的濾嘴時,除了濾嘴內部的物理性之煙的過濾現象以外,可使凝縮/吸附在濾嘴之絲束纖維中的薄荷醇之量,因絲束的總量少而減少,使煙中薄荷醇量及M/T比變高。此外,設計成高通氣比率時,將使煙通過濾嘴內部的時間變長,雖然通常焦油及薄荷醇的過濾率變高,但在絲束總量少的低通氣阻力之濾嘴中,不易使薄荷醇的過濾率變高,而增加M/T比。結果,與焦油的過濾率比較,有可能使薄荷醇的過濾率減低。即使在感官評估中,也可在薄荷醇感覺中獲得產生差異的結果,相對於比較例1,可確認實施例1及2有顯著高的薄荷醇之感覺。 It can be seen from Table 2 that the cigarette designed to have a low ventilation resistance of the filter and a high ventilation ratio of air inflow can make the amount of menthol in the smoke and The M/T ratio becomes high. This is considered to be due to the difference in the filtration rate between tar and menthol in the relationship between the ventilation resistance of the filter and the ventilation ratio. Specifically, when a filter having a low-ventilation resistance is used, in addition to the filtration phenomenon of the physical smoke inside the filter, the amount of menthol which can be condensed/adsorbed in the tow fiber of the filter, due to the total amount of the tow The amount is reduced and the amount of menthol and the M/T ratio in the smoke are increased. Further, when the ventilation ratio is designed to increase the time during which the smoke passes through the inside of the filter, although the filtration rate of tar and menthol is generally high, it is difficult to make the filter having low ventilation resistance with a small total amount of tow. The filtration rate of menthol becomes higher, and the M/T ratio is increased. As a result, it is possible to reduce the filtration rate of menthol as compared with the tar filtration rate. Even in the sensory evaluation, a difference in the feeling of menthol was obtained, and in Comparative Example 1, it was confirmed that Examples 1 and 2 had a significantly high menthol feeling.

可認為更優於本實施例及比較例的範圍,假設是濾嘴的通氣阻力為80mmH2O/27mm以下,且通氣比率為55%以上,並以61%以上更佳,而又更佳的範圍,可假設成為實施例1的條件係50mmH2O/27mm以下且通氣比率為70%以上。如考量濾嘴的實際製程時,則現實可製造的通氣阻力範圍為25mmH2O/27mm以上。濾嘴的材質,其特徵在於由纖維素乙酸酯絲束構成 It is considered to be more preferable than the range of the present embodiment and the comparative example, and it is assumed that the ventilation resistance of the filter is 80 mmH 2 O/27 mm or less, and the ventilation ratio is 55% or more, and more preferably 61% or more, and more preferably The range is assumed to be 50 mm H 2 O/27 mm or less and the ventilation ratio is 70% or more. When considering the actual process of the filter, the realistically achievable ventilation resistance range is 25mmH 2 O/27mm or more. The material of the filter, characterized by a cellulose acetate tow

由上述可證實,因設計成空氣流入之通氣比率高的香煙,而可使煙中的薄荷醇量變高。本實施例中,雖然是使用濾嘴長度為27mm者,但不侷限於本形態中者,即便是任何的長度也可望有相同的效果。同時,對於此香煙的圓周,在本實施例中雖然是使用24.8mm的條件, 但如接近於本實施例的圓周區,也可望有相同的效果,具體上是20.0mm至27.0mm的範圍,並以24.0mm至26.0mm的範圍更佳。 From the above, it was confirmed that the amount of menthol in the smoke can be increased due to the cigarette having a high ventilation ratio designed to flow into the air. In the present embodiment, although the filter length is 27 mm, it is not limited to this embodiment, and even if it is any length, the same effect is expected. Meanwhile, for the circumference of the cigarette, in the present embodiment, although the condition of 24.8 mm is used, However, it is also expected to have the same effect as in the circumferential area of the present embodiment, specifically in the range of 20.0 mm to 27.0 mm, and more preferably in the range of 24.0 mm to 26.0 mm.

<參考例1至4> <Reference Examples 1 to 4>

在使用通氣阻力低的濾嘴,且將加有薄荷醇的濾嘴貯存時,以驗證煙中薄荷醇量成為安定為目的,係變更濾嘴的貯存期間及以香煙包裝形態的貯存期間,以表3所示的濾嘴之通氣阻力及濾嘴芳香量,隨著濾嘴及香煙的貯存期間之變更,實施煙中薄荷醇量之試驗。由於此時是摒除其他因素的影響,故在濾嘴部不設置通氣孔,僅改變濾嘴的通氣阻力進行試驗。 When a filter having a low ventilation resistance is used and a filter containing menthol is stored, the purpose of verifying the amount of menthol in the smoke is to change the storage period of the filter and the storage period in the form of a cigarette package. The ventilating resistance of the filter and the fragrant amount of the filter shown in Table 3 were tested for the amount of menthol in the smoke as the filter and the storage period of the cigarette were changed. Since the influence of other factors is eliminated at this time, no vent hole is provided in the filter portion, and only the ventilation resistance of the filter is changed to perform the test.

濾嘴的貯存條件、通氣阻力及通氣比率以外,係以與之前的實施例1、2及比較例1、2的相同步驟進行試驗。 The test was carried out in the same manner as in the previous Examples 1 and 2 and Comparative Examples 1 and 2 except for the storage conditions, the ventilation resistance, and the ventilation ratio of the filter.

表4是表示濾嘴及以香煙包裝形態的貯存期間之條件者。最短期間的貯存條件,可舉出在剛製作濾 嘴之後就直接使用於香煙的製造,且不以香煙的包裝形態進行貯存者(條件A),另一方面,在最長期間的貯存條件中,可舉出在製作濾嘴後貯存2個月,在使用該濾嘴製作香煙之後,再以包裝形態貯存2個月的條件(條件G)。對於經過條件A至G的各香煙,實施煙中薄荷醇量及焦油量之測定。 Table 4 shows the conditions of the filter and the storage period in the form of a cigarette package. The storage conditions in the shortest period can be exemplified in just making the filter. After the mouth is used directly for the manufacture of cigarettes, and the storage is not carried out in the form of packaging of cigarettes (Condition A). On the other hand, in the storage conditions for the longest period of time, storage can be carried out for 2 months after the filter is manufactured. After the cigarette was produced using the filter, it was stored in a package form for 2 months (condition G). For each of the cigarettes subjected to the conditions A to G, the amount of menthol in the smoke and the amount of tar were measured.

將試驗結果呈示於表5及第1圖中。表5中所示的減少率,係在無實施濾嘴貯存及以香煙包裝形態貯存之條件A與M/T比作比較時,表示各條件中的M/T比的減少率之值。第1圖是各條件中的M/T之減少率的圖示。 The test results are shown in Table 5 and Figure 1. The reduction rate shown in Table 5 indicates the value of the decrease rate of the M/T ratio in each condition when the condition A and the M/T ratio were stored without performing filter storage and storage in a cigarette package. Fig. 1 is a graph showing the rate of decrease of M/T in each condition.

由表5及第1圖可知,濾嘴的貯存期間及以香煙的包裝形態之貯存期間愈長,可獲得所得的薄荷醇量之值變小的結果。同時,可確認濾嘴的通氣阻力愈大,M/T比的減少率增大之結果,可知參考例2至4在與滿足申請專利範圍第1項的濾嘴通氣阻力之要件的參考例1比較 時,M/T比的低減率較大。可認為此乃因低通氣阻力的濾嘴中之絲束重量低,與高通氣阻力者相比可減少薄荷醇對濾嘴之吸附,即每單位薄荷醇量之釋放效率高之故。 As can be seen from Table 5 and Fig. 1, the longer the storage period of the filter and the storage period of the packaged form of the cigarette, the smaller the value of the obtained amount of menthol can be obtained. At the same time, it can be confirmed that the larger the ventilation resistance of the filter and the decrease rate of the M/T ratio, the reference example 1 of the reference examples 2 to 4 which satisfy the requirements of the filter ventilation resistance of the first application of the scope of the patent application. Comparison At the time, the M/T ratio has a large reduction rate. It is considered that this is because the weight of the tow in the filter having low ventilation resistance is low, and the adsorption of the menthol to the filter is reduced as compared with the case of the high ventilation resistance, that is, the release efficiency per unit of menthol is high.

由以上的結果可證實,因使用濾嘴之通氣阻力低的濾嘴,易使煙中薄荷醇量安定地維持。此效果,即使在與對於低通氣阻力的濾嘴為高通氣比率的條件合併進行時,也同樣的可獲得,故可製作使煙中薄荷醇量變高且在貯存後也容易使薄荷醇安定地維持的香煙。 From the above results, it was confirmed that the amount of menthol in the smoke was easily maintained stably by using a filter having a low ventilation resistance of the filter. This effect can be obtained in the same manner even when combined with the condition of the high ventilation ratio of the filter for low ventilation resistance, so that the amount of menthol in the smoke can be made high and the menthol can be easily stabilized after storage. Maintain the cigarettes.

<參考例5至8> <Reference Examples 5 to 8>

將濾嘴中的薄荷醇芳香量設為每支含量為8mg以上時,驗證煙中薄荷醇量可更安定的目的,將濾嘴通氣阻力設為固定,實施變更濾嘴中的薄荷醇芳香量及濾嘴的貯存期間之試驗。表6中所示為濾嘴中的薄荷醇芳香量。由於此中是與參考例1至4同樣的摒除其他影響因素的影響,故在濾嘴部並未設置通氣孔,而僅改變濾嘴的通氣阻力進行試驗。 When the amount of menthol in the filter is 8 mg or more per part, the purpose of verifying the amount of menthol in the smoke can be more stable, and the filter ventilation resistance is fixed, and the amount of menthol in the filter is changed. And testing of the filter during storage. The amount of menthol fragrant in the filter is shown in Table 6. Since this is the same as the reference examples 1 to 4 except for the influence of other influencing factors, the vent hole is not provided in the filter portion, and only the ventilation resistance of the filter is changed to test.

濾嘴的貯存環境,係與參考例1至4在相同溫度22℃、濕度60%中實施,濾嘴的貯存期間是從無實施貯存者(標記為0W)、2週(標記為2W)、5週(標記為5W)、最長的2個月(標記為2M)貯存之條件進行試驗,將自濾嘴中之薄荷醇芳香量釋放作為煙中薄荷醇量的釋放率以百分率表示進行比較。此中,雖然不實施以香煙包裝形態之貯存,係僅以改變濾嘴的貯存期間,調查僅受到濾嘴貯存的影響,但因再實施以香煙包裝形態之貯存,故可推估釋放率比先前的參考例1至4更為減低。所以,此處的試驗,對煙桿部的煙絲並未添加薄荷醇,而僅有薄荷醇自濾嘴部的釋放。煙絲/濾嘴的薄荷醇芳香量、通氣比率及濾嘴的貯存期間以外,係以之前的實施例1、2及比較例1、2之相同步驟進行試驗。將試驗結果呈示於表7及第2圖中。 The storage environment of the filter was carried out at the same temperature of 22 ° C and humidity of 60% with reference examples 1 to 4. The storage period of the filter was never stored (marked as 0 W), 2 weeks (marked as 2 W), The conditions of storage for 5 weeks (labeled as 5W) and the longest 2 months (labeled as 2M) were tested, and the release rate of menthol from the filter as a release rate of menthol in the smoke was compared as a percentage. In this case, although the storage in the form of a cigarette package is not carried out, the storage period is only changed by changing the storage period of the filter, and the investigation is only affected by the storage of the filter. However, since the storage is in the form of a cigarette package, the release ratio can be estimated. The previous reference examples 1 to 4 were further reduced. Therefore, in the test here, menthol was not added to the tobacco of the tobacco rod portion, and only the release of menthol from the filter portion was observed. The test was carried out in the same manner as in the previous Examples 1 and 2 and Comparative Examples 1 and 2 except for the menthol flavor amount of the cut tobacco/filter, the aeration ratio, and the storage period of the filter. The test results are shown in Tables 7 and 2.

由表7及第2圖可知,濾嘴的薄荷醇芳香量愈多,隨經時變化的釋放率愈安定,與參考例5、6比較,可說參考例7、8的經時變化耐性較強。此乃因使大量添加的薄荷醇量成為絲束吸附的薄荷醇量以上,可使受到薄荷醇之吸附的影響變小。此效果,由於在使用比參考例5至 8更低通氣阻力的濾嘴時,可使吸附到絲束的薄荷醇量自行減少,故預估更可發揮效果。由以上的結果,濾嘴中的薄荷醇芳香量,在每支含量設為8mg以上時,可證實煙中薄荷醇量是呈安定。可預估更理想的濾嘴中之薄荷醇芳香量為10mg以上,又更理想的是符合參考例8的條件之12mg以上。 As can be seen from Tables 7 and 2, the more the menthol aroma of the filter, the more stable the release rate with time, and compared with Reference Examples 5 and 6, it can be said that the time-dependent change resistance of Reference Examples 7 and 8 is relatively better. Strong. This is because the amount of menthol added in a large amount is equal to or greater than the amount of menthol adsorbed by the tow, and the influence by the adsorption of menthol can be made small. This effect, due to the use of Reference Example 5 8 When the filter with lower ventilation resistance can reduce the amount of menthol adsorbed to the tow, it is estimated that it can exert its effect. From the above results, the amount of menthol scent in the filter was such that when the content per liter was 8 mg or more, it was confirmed that the amount of menthol in the smoke was stable. It is estimated that the menthol fragrant amount in the more desirable filter is 10 mg or more, and more desirably, it is 12 mg or more in accordance with the conditions of Reference Example 8.

<實施例3及比較例3、4> <Example 3 and Comparative Examples 3 and 4>

在實施例1、2及比較例1、2中,係焦油量為5mg時的比較試驗,即使本技術是以更低焦油量的1mg為目標時,為驗證其為有效,故以表8中所示的試驗水準實施與實施例1、2及比較例1、2相同的試驗。同時,同様的也進行合併感官評估的評估。 In Examples 1, 2 and Comparative Examples 1 and 2, a comparative test when the amount of tar was 5 mg, even if the technique is aimed at 1 mg of a lower tar amount, in order to verify that it is effective, it is shown in Table 8. The test tests shown below were carried out in the same tests as in Examples 1 and 2 and Comparative Examples 1 and 2. At the same time, peers also conducted an assessment of the combined sensory assessment.

表9是表示試驗結果,除了煙中薄荷醇及焦油量以外,也表示M/T比。 Table 9 shows the test results, which indicate the M/T ratio in addition to the amount of menthol and tar in the smoke.

由表9可知,實施例3成為最高的薄荷醇量,即使在比較M/T比時,也可獲得最高的結果。對於以感官評定而評定薄荷醇的感覺,在實施例3中可獲得明顯高的薄荷醇之感覺,與之前實施的實施例1、2及比較例1、2的評定相同,由於薄荷醇量之值大為不同,故可預估是產生顯著差異者。由以上可確認,即使在焦油量極低的範圍中,本技術亦為有效。 As is clear from Table 9, Example 3 was the highest amount of menthol, and the highest result was obtained even when the M/T ratio was compared. For the feeling of menthol evaluated by sensory evaluation, a significantly high menthol sensation was obtained in Example 3, which was the same as the evaluation of Examples 1, 2 and Comparative Examples 1, 2 previously performed, due to the amount of menthol. The values are quite different, so it can be estimated that there is a significant difference. From the above, it was confirmed that the present technology is effective even in the range where the amount of tar is extremely low.

Claims (6)

一種低焦油薄荷醇香煙,係具有煙桿部與經水松紙(tipping paper)包捲的濾嘴部之焦油量為5mg以下者,前述濾嘴部包含以纖維素乙酸酯絲束構成的單一節段,前述濾嘴部的通氣阻力為25至80mmH2O/27mm,同時空氣自穿設在前述水松紙上的通氣孔流入之通氣比率為55%以上,且前述濾嘴部中添加有薄荷醇。 A low tar menthol cigarette comprising a tobacco rod portion and a filter portion wrapped by tipping paper having a tar content of 5 mg or less, wherein the filter portion comprises a cellulose acetate tow. In a single section, the ventilation resistance of the filter portion is 25 to 80 mmH 2 O/27 mm, and the air is ventilated from the vent hole of the tipping paper to a ventilation ratio of 55% or more, and the filter portion is added Menthol. 如申請專利範圍第1項所述之低焦油薄荷醇香煙,其中薄荷醇對前述濾嘴部的添加量,係每支低焦油薄荷醇香煙為8mg/支以上。 The low tar menthol cigarette according to claim 1, wherein the amount of menthol added to the filter portion is 8 mg/piece or more per low tar menthol cigarette. 如申請專利範圍第1或2項所述之低焦油薄荷醇香煙,其中,前述煙桿部或濾嘴部具有阻力體。 The low tar menthol cigarette according to claim 1 or 2, wherein the tobacco rod portion or the filter portion has a resistance body. 如申請專利範圍第3項所述之低焦油薄荷醇香煙,其中,前述阻力體為膠囊或孔口。 The low tar menthol cigarette according to claim 3, wherein the resistance body is a capsule or an orifice. 如申請專利範圍第1至4項中任一項所述之低焦油薄荷醇香煙,其中,前述濾嘴部的通氣阻力為25至50mmH2O/27mm,同時空氣流入的通氣比率為70%以上。 The low tar menthol cigarette according to any one of claims 1 to 4, wherein the filter portion has a ventilation resistance of 25 to 50 mmH 2 O/27 mm, and the air inflow ratio is 70% or more. . 如申請專利範圍第1至5項中任一項所述之低焦油薄荷醇香煙,其中,前述低焦油薄荷醇香煙的圓周為20.0至27.0mm。 The low tar menthol cigarette according to any one of claims 1 to 5, wherein the aforementioned low tar menthol cigarette has a circumference of 20.0 to 27.0 mm.
TW104110659A 2014-04-03 2015-04-01 Low-tar menthol cigarette TWI598049B (en)

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