201236841 六、發明說明： 【發明所屬之技術領域】 本發明係關於一種橡膠包的製造方法。 【先前技術】 在許多情況中，例如苯乙烯丁二烯橡膠或乙烯丙烯二 烯橡膠之合成橡膠係以包（bale )的形式運送。在本文中 ’ 「包」意指經壓縮成型成實質上爲矩形平行六面體形之 橡膠。 有關合成橡膠包的製造方法，舉例而言，專利文件1 揭露以下方法：將乙烯/α-烯烴/非共軛多烯聚合物橡膠及 聚烯烴樹脂饋入至擠壓機以熔化及混合，且將自擠壓機通 過擠壓機模具擠壓所得橡膠組成物藉由旋轉刀連續切割成 九粒形狀’該九粒於6 0 °C至1 0 0 °C下以運輸用水運輸，並 將該經運輸九粒加以壓縮成型，以產生包。 專利文件1係日本專利公開第1 1 -90926號。 【發明內容] 然而’在前述方法中，因爲該壓縮成型係於分離出運 輸用水後立即進行，由於水分仍在九粒表面上，因此九粒 間的融合強度（fusion strength)降低，於儲存時會改變 包的形狀，也因此就包的形狀之穩定觀點，該方法不足以 令人滿意。 在前述的情況下，本發明欲達到的目的係在於提供— -5- 201236841 種在包的形狀上具有極佳穩定性的橡膠包之製造方法，其 係藉由將例如苯乙烯丁二烯橡膠之合成橡膠以擠壓機熔化 及混合、藉由將經擠壓之橡膠切割以產生九粒、以及將該 九粒壓縮成型。 本發明提供一種橡膠包的製造方法，其包含：藉由使 用配有擠壓機模具之擠壓機將橡膠熔化及混合：將熔化態 之橡膠擠壓通過該擠壓機模具；藉由切割該經擠壓之橡膠 以產生九粒；於冷卻水中冷卻該九粒，冷卻時間爲5秒或 更多且爲20秒或更少；將該九粒與該冷卻水分開；於5 °C 或更高且40°C或更低之氣流中乾燥該九粒；稱重取得所需 量之九粒：以及將稱重取得之九粒壓縮成型一段時間，其 中將稱重取得之九粒分離後的平均經過時間爲30秒或更 多且爲100秒或更少。 本發明可提供一種在包的形狀上具有極佳穗定性的橡 膠包之製造方法，其係藉由將例如苯乙烯丁二烯橡膠之合 成橡膠以擠壓機熔化及混合、藉由將經擠壓之橡膠切割以 產生九粒、以及將該九粒壓縮成型。 【實施方式】 本發明中待使用之橡膠的實例爲芳香族乙烯基化合物 /共軛二烯共聚物橡膠、共軛二烯聚合物橡膠及乙烯/α-烯 烴/非共軛二烯共聚物橡膠。該芳香族乙烯基化合物/共軛 二烯共聚物橡膠的實例爲苯乙烯丁二烯共聚物橡膠。該共 軛二烯聚合物橡膠的實例爲聚丁二烯橡膠、聚異戊二烯橡201236841 VI. Description of the Invention: TECHNICAL FIELD OF THE INVENTION The present invention relates to a method of manufacturing a rubber bag. [Prior Art] In many cases, a synthetic rubber such as styrene butadiene rubber or ethylene propylene diene rubber is shipped in the form of a bale. As used herein, "pack" means a rubber that is compression molded into a substantially rectangular parallelepiped shape. Regarding the manufacturing method of the synthetic rubber bag, for example, Patent Document 1 discloses a method of feeding an ethylene/α-olefin/non-conjugated polyene polymer rubber and a polyolefin resin to an extruder to melt and mix, and The rubber composition extruded from the extruder through an extruder die is continuously cut into nine shapes by a rotary knife. The nine pellets are transported by transport water at 60 ° C to 100 ° C, and the Nine pellets were transported and compressed to produce a packet. Patent Document 1 is Japanese Patent Laid-Open No. 11-90926. SUMMARY OF THE INVENTION However, in the foregoing method, since the compression molding is performed immediately after the separation of the transportation water, since the moisture is still on the surface of the nine particles, the fusion strength between the nine particles is lowered during storage. This will change the shape of the bag, and therefore the method is not satisfactory in terms of the stability of the shape of the bag. In the foregoing case, the object of the present invention is to provide a method for producing a rubber bag having excellent stability in the shape of a bag by using -5 - 201236841 by, for example, styrene butadiene rubber. The synthetic rubber is melted and mixed by an extruder, cut by pressing the extruded rubber to produce nine pellets, and the nine pellets are compression molded. The present invention provides a method of manufacturing a rubber bag, comprising: melting and mixing a rubber by using an extruder equipped with an extruder die: extruding a molten rubber through the extruder die; The extruded rubber to produce nine particles; the nine particles are cooled in cooling water for a cooling time of 5 seconds or more and 20 seconds or less; the nine particles are separated from the cooling water; at 5 ° C or more The nine pieces are dried in a gas stream at a high temperature of 40 ° C or lower; the weight is obtained to obtain nine pieces of the desired amount: and the nine pieces obtained by weighing are compression-molded for a period of time, wherein the nine pieces obtained by weighing are separated. The average elapsed time is 30 seconds or more and is 100 seconds or less. The present invention can provide a method for producing a rubber bag having excellent sharpness in the shape of a bag by melting and mixing an elastomer such as styrene butadiene rubber in an extruder, by being squeezed The pressed rubber is cut to produce nine pieces, and the nine pieces are compression molded. [Embodiment] Examples of the rubber to be used in the present invention are an aromatic vinyl compound/conjugated diene copolymer rubber, a conjugated diene polymer rubber, and an ethylene/α-olefin/non-conjugated diene copolymer rubber. . An example of the aromatic vinyl compound/conjugated diene copolymer rubber is a styrene butadiene copolymer rubber. Examples of the conjugated diene polymer rubber are polybutadiene rubber, polyisoprene rubber
-6- S 201236841 膠及聚氯平橡膠。該乙烯/α-烯烴/非共軛二烯共聚物橡膠 之實例爲乙烯/丙烯/亞乙基降莰烯共聚物橡膠及乙烯/丙烯 /二環戊二烯共聚物橡膠。這些橡膠中之一者可被單獨使 用、或將它們其中之二或更多者摻合使用。此外，只要橡 膠性質不會被破壞，則可加入上述橡膠以外之橡膠、樹脂 及例如穩定劑之添加劑。 關於上述聚合物橡膠中任一者的製造方法，可利用包 括溶液聚合、嵌段聚合、懸浮聚合及乳化聚合之任何已知 方法。 將橡膠饋入配有擠壓機模具之擠壓機，以將橡膠熔化 及混合。待饋入擠壓機之橡膠可爲粉末、九粒或屑粒（ crumb )形式。或者，在橡膠爲溶液聚合所製造的情況中 ’仍含有溶劑之橡膠可被饋入擠壓機，以執行除氣同時熔 化及混合。更或者，可將仍含有水分組分之橡膠饋入擠壓 機，以執行脫水同時熔化及混合。 至於擠壓機，較佳的是使用雙螺桿擠壓機，以改善混 合效能。當使用該雙螺桿擠壓機時，螺桿的轉動方向可爲 相同或相異。或者，可使用串列式擠壓機（tandem extruder )。在饋入仍溶在溶劑中之橡膠的情況中，該擠 壓機則配有通氣孔’經此進行除氣。此外，必要時可提供 齒輪泵。 在以擠壓機將橡膠熔化及混合後，將熔化態之橡膠擠 壓通過該擠壓機模具，並將該擠壓出之橡膠切割以產生九 粒’該九粒於冷卻水中冷卻。至於製造及冷卻九粒之方法 201236841 ，較佳的是利用稱爲「水下切割法（under water cut method)」，即，將經擠壓通過擠壓機模具之熔化態橡膠 切割，並立即於冷卻水中冷卻的方法。 爲了藉由設定於製造包期間的九粒表面溫度高於指定 溫度，增加九粒之間的融合強度，以改善包的形狀之穩定 性，則正在被擠壓通過擠壓機模具之橡膠的溫度較佳的是 1〇〇 °C或更高、更佳的是110 °C或更高、且進一步更佳的是 1 2(TC或更高。此外，爲了藉由降低儲存包之間的黏附， 以改善在將包從包儲存盒取出時的包取用之容易度，或爲 了於乾燥程序或稱重程序期間減少例如因九粒互相黏附而 堵塞管子程序問題，則正在被擠壓通過擠壓機模具之橡膠 的溫度較佳的是160°C或更低 '更佳的是15(TC或更低、且 進一步更佳的是140 °C或更低。 此外，爲了藉由設定於製造包期間的九粒表面溫度高 於指定溫度，增加九粒之間的融合強度，以改善包的形狀 之穩定性，則所要製造之各九粒質量較佳的是0.3 g或更 多，且更佳的是〇.4 g或更多。此外，爲了藉由降低儲存 包之間的黏附，以改善在將包從包儲存盒取出時的包取用 之容易度，或爲了減少於乾燥程序或稱重程序期間例如因 九粒互相黏附而堵塞管子的程序問題，則各九粒質量較佳 的是0.7 g或更少，且更佳的是0.6 g或更少。至於各九 粒之質量的調整方法，舉例而言，可改變旋轉刀的旋轉速 度》 將該因此製造之九粒於冷卻水中冷卻，並於之後將九-6- S 201236841 Glue and polychlorinated rubber. Examples of the ethylene/α-olefin/non-conjugated diene copolymer rubber are ethylene/propylene/ethylene decene copolymer rubber and ethylene/propylene/dicyclopentadiene copolymer rubber. One of these rubbers may be used singly or in combination of two or more of them. Further, as long as the rubber property is not broken, a rubber other than the above rubber, a resin, and an additive such as a stabilizer may be added. Regarding the production method of any of the above polymer rubbers, any known method including solution polymerization, block polymerization, suspension polymerization, and emulsion polymerization can be utilized. The rubber is fed into an extruder equipped with an extruder die to melt and mix the rubber. The rubber to be fed into the extruder may be in the form of powder, nine or crumb. Alternatively, in the case where the rubber is produced by solution polymerization, the rubber which still contains the solvent can be fed into the extruder to perform degassing while melting and mixing. Alternatively, the rubber still containing the moisture component can be fed into the extruder to perform dehydration while melting and mixing. As for the extruder, it is preferred to use a twin-screw extruder to improve the mixing efficiency. When the twin-screw extruder is used, the directions of rotation of the screws may be the same or different. Alternatively, a tandem extruder can be used. In the case of feeding a rubber which is still dissolved in a solvent, the extruder is equipped with a venting port' to degas. In addition, gear pumps are available if necessary. After the rubber is melted and mixed by an extruder, the molten rubber is extruded through the extruder die, and the extruded rubber is cut to produce nine particles which are cooled in cooling water. As for the method of manufacturing and cooling nine pieces 201236841, it is preferable to use an "under water cut method", that is, to cut a molten rubber which is extruded through an extruder die, and immediately Cooling method in cooling water. In order to increase the fusion strength between the nine particles by setting the surface temperature of the nine particles during the manufacturing package to be higher than the specified temperature to improve the stability of the shape of the package, the temperature of the rubber being extruded through the die of the extruder It is preferably 1 ° C or higher, more preferably 110 ° C or higher, and still more preferably 1 2 (TC or higher. In addition, in order to reduce adhesion between the storage bags In order to improve the ease of taking the bag when the bag is taken out of the bag storage case, or to reduce the blockage process, for example, due to the adhesion of nine pieces of each other during the drying process or the weighing process, it is being squeezed through the squeeze The temperature of the rubber of the press mold is preferably 160 ° C or lower, more preferably 15 (TC or lower, and still more preferably 140 ° C or lower. In addition, in order to be manufactured by setting The surface temperature of the nine particles during the bag is higher than the specified temperature, and the fusion strength between the nine particles is increased to improve the stability of the shape of the bag. The mass of each of the nine particles to be manufactured is preferably 0.3 g or more, and more The best is 〇.4 g or more. In addition, in order to reduce Adhesion between the packages to improve the ease of taking the bag when the bag is removed from the bag, or to reduce the procedural problems of clogging the tube during the drying process or weighing procedure, for example, due to the adhesion of nine particles to each other, Then, the mass of each of the nine particles is preferably 0.7 g or less, and more preferably 0.6 g or less. As for the adjustment method of the mass of each of the nine grains, for example, the rotation speed of the rotary knife can be changed. Therefore, the nine pieces produced are cooled in cooling water and will be nine afterwards.
-8- S 201236841 粒與該冷卻水分開。從切割九粒至與該冷 時.間爲2 0秒或更少。當該冷卻時間過長 過度冷卻，且因此在製造包後所達到的九 度會過低，以致包的形狀之穩定性被降低 善包的形狀之穩定性，該冷卻時間較佳的 ，且更佳的是1 5秒或更少。此外，爲藉 間的黏附，以改善在將包從包儲存盒取出 易度，或爲了減少於乾燥程序或稱重程序 互相黏附而堵塞管子程序問題，該冷卻時 或更多、更佳的是7秒或更多、且進一步 或更多。 爲了藉由設定於製造包期間的九粒表 溫度，增加九粒之間的融合強度，以改善 性，則冷卻水的溫度較佳的是1 o°c或更 2 0°C或更高。此外，爲了藉由降低儲存包 改善在將包從包儲存盒取出時的包取用之 減少於乾燥程序或稱重程序期間例如因九 塞管子程序問題，則該冷卻水溫度較佳的 且更佳的是3 5 °C或更低。 雖然該九粒係於冷卻水中冷卻，但可 移動。可靜置該九粒之狀態實例爲該九粒 中之狀態。或者，移動該九粒之狀態實例 中流動冷卻水運送之狀態。 至於將該九粒與該冷卻水分開之方法 卻水分開的冷卻 時，則九粒會被 粒之間的融合強 。此外，爲更改 是1 8秒或更少 由降低儲存包之 時的包取用之容 期間例如因九粒 間較佳的是5秒 •更佳的是1 0秒 面溫度高於指定 包的形狀之穩定 高，且更佳的是 之間的黏附，以 容易度，或爲了 粒互相黏附而堵 是40°C或更低， 將該九粒靜置或 係容納於冷卻浴 爲該九粒係與管 ，可利用包括以 -9 - 201236841 篩網分開及離心分開之任何已知方法。 2 1分開後，將該九粒於氣流中接受乾燥處理。該氣流 溫度爲5°C或更高且爲40°C或更低。當該氣流溫度過低時 ，該九粒會被過度冷卻，且因此在製造包後所達到的該九 粒之間的融合強度被降低，以致包的形狀之穩定性被降低 。爲進一步改善包的形狀之穩定性，該氣流溫度較佳的是 1 〇°c或更高。又，當該氣流溫度過高時，該九粒冷卻不足 ，且因此將包從包儲存盒取出時的包取用之容易度被降低 ，或於乾燥程序或稱重程序期間例如因九粒互相黏附而堵 塞管子程序問題的發生可能性會提高。此外，爲改善在將 包從包儲存盒取出時的包取用之容易度，或爲了進一步減 少於乾燥程序或稱重程序期間例如因九粒互相黏附而堵塞 管子程序問題，則該氣流溫度較佳的是3 5 °c或更低。 至於用於進行乾燥處理之方法，可利用以鼓風乾燥機 中的空氣吹氣九粒之方法，或可利用讓空氣於管中流動並 讓該九粒於管中與通過管中的空氣一起流動之方法。 在於氣流中乾燥該九粒後，稱重取得所需量之九粒， 並將該稱重取得之九粒加以壓縮成型一段時間，其中將稱 重取得之九粒分離後的平均經過時間爲3 0秒或更多且爲 1 〇 〇秒或更少，藉此獲得橡膠包。當該平均經過時間過長 時，該九粒會被過度冷卻，且因此在製造包後所達到的該 九粒之間的融合強度被降低，以致包的形狀之穩定性被降 低。該平均經過時間較佳的是90秒或更少，且更佳的是 8 0秒或更少。或者，當該平均經過時間過短時，該九粒內-8- S 201236841 The pellet is separated from the cooling water. From cutting nine grains to the cold time, it is 20 seconds or less. When the cooling time is too long and excessively cooled, and thus the nine degrees reached after the package is manufactured, the stability of the shape of the package is lowered, and the cooling time is better, and The best is 15 seconds or less. In addition, for the adhesion of the borrowing, to improve the ease of taking the bag from the bag storage box, or to reduce the problem of clogging the pipe program in order to reduce the drying procedure or the weighing procedure sticking to each other, the cooling is more or better. 7 seconds or more, and further or more. In order to increase the fusion strength between the nine particles by setting the nine-sheet temperature during the production of the package to improve the temperature, the temperature of the cooling water is preferably 1 °C or 20 °C or higher. In addition, in order to reduce the bag take-up when the bag is taken out of the bag storage case by reducing the storage bag, the cooling water temperature is better and more, for example, due to a nine-plug process problem during the drying process or the weighing process. The best is 3 5 ° C or lower. Although the nine-grain line is cooled in cooling water, it can be moved. An example of a state in which the nine particles can be left to stand is the state in the nine grains. Alternatively, move the state of the flow of cooling water in the nine-state instance. As for the method of separating the nine particles from the cooling water while cooling, the nine particles are strongly fused by the particles. In addition, the change period is 18 seconds or less. The period during which the package is taken down is, for example, because the nine-part is preferably 5 seconds. More preferably, the 10-second surface temperature is higher than the specified package. The shape is stable, and it is better that the adhesion between them is easy, or for the particles to adhere to each other and the plug is 40 ° C or lower, the nine particles are allowed to stand or are contained in the cooling bath for the nine particles. The system and tube can be any known method including separation and centrifugation separated by a sieve of -9 - 201236841. After the separation of 2 1 , the nine pellets were subjected to a drying treatment in a gas stream. The gas flow temperature is 5 ° C or higher and 40 ° C or lower. When the temperature of the gas stream is too low, the nine particles are excessively cooled, and thus the fusion strength between the nine particles obtained after the package is produced is lowered, so that the stability of the shape of the bag is lowered. In order to further improve the stability of the shape of the bag, the temperature of the gas stream is preferably 1 〇 ° C or higher. Moreover, when the temperature of the air stream is too high, the nine particles are insufficiently cooled, and thus the ease of taking the bag when the bag is taken out of the bag storage case is lowered, or during the drying process or the weighing process, for example, due to nine mutual The possibility of sticking and blocking the tube program is likely to increase. In addition, in order to improve the ease of taking the bag when the bag is taken out of the bag storage case, or to further reduce the problem of clogging the pipe program during the drying process or the weighing process, for example, due to the adhesion of nine particles to each other, the air flow temperature is higher. The best is 3 5 °c or lower. As for the method for performing the drying treatment, a method of blowing nine particles with air in a blast dryer may be utilized, or the air may be allowed to flow in the tube and the nine particles may be used in the tube together with the air passing through the tube. The method of flow. After drying the nine particles in the air stream, weighed to obtain the required amount of nine particles, and the nine particles obtained by the weighing were compression-molded for a period of time, wherein the average elapsed time after the separation of the nine particles obtained by the weighing was 3 0 seconds or more and 1 〇〇 second or less, thereby obtaining a rubber bag. When the average elapsed time is too long, the nine particles are excessively cooled, and thus the fusion strength between the nine particles obtained after the package is manufactured is lowered, so that the stability of the shape of the package is lowered. The average elapsed time is preferably 90 seconds or less, and more preferably 80 seconds or less. Or, when the average elapsed time is too short, the nine grains
-10- S 201236841 的熱不足以擴散至該九粒表面，且因此在製造包中所獲得 之該九粒表面溫度未增加，以致該九粒之間的融合強度被 降低以及包的形狀之穩定性被降低。該平均經過時間較佳 的是45秒或更多，且更佳的是60或更多。模製壓力較佳 的是50 kg/cm2至150 kg/cm2 ’且模製時間較佳的是5秒 至20秒。 這時，將經稱重取得之九粒分離後的平均經過時間（ 由待加以壓縮成型之全部九粒間取得），爲藉由分離裝置 將該九粒與該冷卻水分開至經過壓縮成型製造包的經過時 間之平均。在介於九粒分離與壓縮成型之間有複數個程序 的情況中，該平均經過時間係藉由取得在各個程序中各九 粒的貯留時間並加總貯留時間來計算。舉例而言，運輸程 序中的貯留時間係以各九粒移動速度爲基礎而取得。又， 在稱重程序中的貯留時間係以成型循環時間及九粒饋入速 度爲基礎而取得。 在成型中，大於所需包的包可藉由切割該較大的包而 成型，以獲得所需包。此外，爲保護該包的表面，可將經 成型包的表面以膜包覆。 根據本發明所製造之橡膠包可適於應用在包括車輛輪 胎及密封材料之各種用途。 根據本發明所製造之橡膠包的形狀穩定性佳。此外， 在乾燥程序中及稱重程序中極少造成程序問題。利用於本 發明之適用方法不包括將九粒壓縮成型前加熱九粒之步驟 ，且此方法在成本上有極佳優勢。 -11 - 201236841 圖1顯示本發明中利用之方法實施例的實例槪要。將 相當於原料的橡膠饋入擠壓機（1)、經過具有孔洞之模 具擠壓出、並於製粒機（2)中切割及冷卻，藉此獲得九 粒。將所獲得之九粒立即自製粒機排出並經由管（9 )與 冷卻水一起被運至分離裝置（3)。將在分離裝置中與冷 卻水分開之九粒通過鼓風乾燥機（4)並於壓縮成型機（5 )中成型爲包。 圖2顯示本發明中利用之方法實施例的另一實例槪要 。此實例從原料饋入至擠壓機（1)達至運送該九粒至分 離裝置（3)與圖1中所示相同。自該分離裝置（3)排出 之九粒掉入垂直管（12)，同時暴露於空氣、於管（13) 中與藉由鼓風機（6)所發送之空氣一起被運送至經過旋 風器（7)及垂直管（14)，至壓縮成型機（5)，它們在 此成型爲包。 實例1 將苯乙烯丁二烯聚合物橡膠饋入擠壓機、以旋轉切割 刀片切割、並將該生成物以冷卻水冷卻’由此獲得九粒。 調整擠壓機圓筒的溫度’以使在模具中已熔融橡膠的溫度 爲1 3 0 °C。該冷卻水的溫度約爲3 0 °C。取出經此獲得之十 個九粒，且結果每一個九粒的平均質量爲〇·43 g。 將所獲得之九粒立即自製粒機排出並與管中流動冷卻 水運至分離裝置。自切割橡膠至輸入九粒至分離裝置中的 冷卻時間約爲1 4秒。The heat of -10-S 201236841 is not sufficient to diffuse to the nine surface, and thus the nine surface temperatures obtained in the manufacturing package are not increased, so that the fusion strength between the nine particles is lowered and the shape of the package is stabilized. Sex is reduced. The average elapsed time is preferably 45 seconds or more, and more preferably 60 or more. The molding pressure is preferably from 50 kg/cm2 to 150 kg/cm2' and the molding time is preferably from 5 seconds to 20 seconds. At this time, the average elapsed time after separation of the nine particles obtained by weighing (taken from all nine particles to be compression-molded) is to separate the nine particles from the cooling water to a compression-molded manufacturing package by a separating device. The average of the elapsed time. In the case where there are a plurality of procedures between the nine separation and the compression molding, the average elapsed time is calculated by taking the storage time of each of the nine particles in each program and adding the storage time. For example, the storage time in the transportation process is based on nine movement speeds. Further, the storage time in the weighing procedure was obtained based on the molding cycle time and the nine-feed speed. In forming, a package larger than the desired package can be formed by cutting the larger package to obtain the desired package. Further, to protect the surface of the bag, the surface of the formed bag may be coated with a film. The rubber bag manufactured in accordance with the present invention can be suitably used in a variety of applications including vehicle tires and sealing materials. The rubber bag manufactured according to the present invention has a good shape stability. In addition, there are very few procedural problems in the drying process and in the weighing procedure. The method applicable to the present invention does not include the step of heating nine particles before compression molding, and this method has an excellent cost advantage. -11 - 201236841 Figure 1 shows an example of an embodiment of a method utilized in the present invention. The rubber equivalent to the raw material was fed into the extruder (1), extruded through a mold having a hole, and cut and cooled in a granulator (2), thereby obtaining nine particles. The obtained nine instant granules were discharged and transported to the separation device (3) via a tube (9) together with cooling water. The nine particles separated from the cooling water in the separating device were passed through a blast dryer (4) and molded into a bag in a compression molding machine (5). Fig. 2 shows another example of an embodiment of the method utilized in the present invention. This example is fed from the feedstock to the extruder (1) until the transport of the nine pellets to the separation device (3) is the same as that shown in Figure 1. The nine particles discharged from the separating device (3) fall into the vertical tube (12) while being exposed to the air, and are transported in the tube (13) together with the air sent by the blower (6) to the cyclone (7). And vertical tubes (14) to compression molding machines (5) where they are formed into a package. Example 1 A styrene butadiene polymer rubber was fed into an extruder, cut with a rotary cutting blade, and the resultant was cooled with cooling water. Thus, nine particles were obtained. The temperature of the extruder cylinder was adjusted so that the temperature of the molten rubber in the mold was 130 °C. The temperature of the cooling water is about 30 °C. Ten nine particles obtained by this were taken out, and the average mass of each of the nine particles was 〇·43 g. The nine instant granules obtained were discharged and transported to the separation device with flowing cooling water in the tubes. The cooling time from cutting the rubber to inputting nine to the separation device is about 14 seconds.
S -12- 201236841 將已輸入至分離裝置中的九粒立即與冷卻水分開、以 30°C的空氣於管中移動、並接著稱重取得所指定量。在經 稱重取得之九粒分開後的67秒平均經過時間，將該經稱 重取得之九粒壓縮成型成橡膠包。該成型壓力係150 kg/cm2，且該成型時間爲10秒。該由此成型之包的形狀 穩定性佳。此外，在乾燥程序及九粒稱量程序中不會造成 例如堵塞管子之程序問題。 【圖式簡單說明】 圖1爲說明本發明中利用之方法實施例的實例示意圖 〇 圖2爲說明本發明中利用之該方法實施例的另一實例 7K意圖。 【主要元件符號說明】 1 :擠壓機 2 :製粒機 3 :分離裝置 4 :鼓風乾燥機 5 :壓縮成型機 6 :鼓風機 7 :旋風器 9 :管 12 :垂直管 -13- 201236841 1 3 :管 1 4 :垂直管 -14-S -12- 201236841 The nine particles that have been input into the separation device are immediately separated from the cooling water, moved in a tube at 30 ° C, and then weighed to obtain the specified amount. The weighed nine pieces were compression-molded into a rubber bag after an average elapsed time of 67 seconds after the separation of the nine particles obtained by weighing. The molding pressure was 150 kg/cm2, and the molding time was 10 seconds. The shape of the thus formed bag is excellent in stability. In addition, there is no procedural problem such as clogging the tube in the drying procedure and the nine weighing procedure. BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a schematic view showing an example of an embodiment of a method utilized in the present invention. Fig. 2 is a view showing another example of the embodiment of the method utilized in the present invention. [Explanation of main component symbols] 1 : Extruder 2 : Granulator 3 : Separation device 4 : Blast dryer 5 : Compression molding machine 6 : Blower 7 : Cyclone 9 : Tube 12 : Vertical tube - 13 - 201236841 1 3: tube 1 4: vertical tube-14-
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