TW201236581A - Preparation method of gel state water-soluble essence for tobacco - Google Patents

Preparation method of gel state water-soluble essence for tobacco Download PDF

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Publication number
TW201236581A
TW201236581A TW100113242A TW100113242A TW201236581A TW 201236581 A TW201236581 A TW 201236581A TW 100113242 A TW100113242 A TW 100113242A TW 100113242 A TW100113242 A TW 100113242A TW 201236581 A TW201236581 A TW 201236581A
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Taiwan
Prior art keywords
tobacco
temperature
gel state
essence
soluble
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TW100113242A
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Chinese (zh)
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TWI423769B (en
Inventor
Jian Hua
xing-hui Chang
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Shenzhen Smoke Biolog Technology Ltd Company
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Publication of TWI423769B publication Critical patent/TWI423769B/zh

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  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses a preparation method of gel state water-soluble essence for tobacco. The method comprises the following steps of: mixing glycerol and food thickener in an adding mass ratio of the food thickener to the glycerol of 1:50-1:5, stirring the mixture uniformly, heating the mixture to the temperature of between 80 and 100 DEG C, stirring and dissolving completely, homogenizing, cooling the solution to the temperature of between 30 and 50 DEG C, adding water-soluble essence for tobacco, and standing for not less than 12 hours at the temperature of between 1 and 30 DEG C to obtain a finished product. The finished product prepared by adopting the method has the advantages that the volatilization of the essence is inhibited to a large extent, the fragrance is kept completely, loss caused by certain volatile components is reduced, and transportation and preservation are convenient.

Description

201236581 六、發明說明: 【發明所屬之技術領域】 成凝’尤其是將水溶性煙用香精製造 【先前技術】 煙用香精的香氣類型和錢風格在 煙的檔次和品位,通常_在燃燒的過程中會 道的有機物,如果在香煙中加入一此悉產生二辛辣味 燒過程中產生的辛辣味,目前所採用 精油形式,_起香_揮=失 在香煙的氣造過程中,為了改善香 蝴 μ 礙 缺點β二此、㈣醇甘'由、丙—醇等溶劑的煙用香精香料,其 劑中疋均勻的溶解於上述溶 發2彳Π 態的’也餘料成香味的揮 少。貝失把煙用香精製造成凝膠態在目前的相關技射報導很 【發明内容】 精製歧供把水雜煙用香 將由以下技術方案實現的: 比例為1 : 依照食品增_與甘油的添加品質 拌溶解完全,均質^ ’、擾拌均勻’加熱到断:〜WC攪 凡王謂5〜15分鐘,冷卻心〇t〜耽加 201236581 性煙用香精攪拌均勻,rc〜30°c放置至少12小時即得成品, 其中該食品增稠劑較佳為聚丙稀酸鈉。 本發明把水溶性煙用香精做成凝膠態,具有以下明顯的效 果: (1) 本發明把水溶性煙用香精做成凝膠態,使用更加方 便,包裝運輸儲存更加靈活。 (2) 本發明把水溶性煙用香精做成凝膠態,大大提高了 煙用香精耐熱'耐光、耐氧的能力,避免因為直接受光、熱 外界影響引起的變色變味。 ^ 本發明把水溶性煙用香精做成凝膠態,香精的揮發 得到很大程度的抑制,香味保留完整,減少了一些揮發成分弓X 起的損失。 (4) 本發明把水溶性煙用香精做成凝膠態,可提高產品 的品質,增加留香性。 (5) 本發明把水溶性煙用香精做成凝膠態,不含水,可 以保持在-20°C低溫下不結冰。 (6) 本發明生產成本較低,原料容易取得,生產工藝比 較簡單’便於實際生產。 κ 另外,聚丙烯酸納能溶於甘油中形成極黏稠的透明液體, 其黏性是由於分子内許多陰離子基團的離子現象使分子鏈增 長’表現黏度增大而形成高粘性溶液’久存黏度變化極小。曰 【實施方式】 實施例1,凝膠態草莓香味煙用香精的製造: 依次稱取甘油85克、聚丙稀酸鈉5克,混合並攪拌均勺’ 加熱到8(TC溶解完全’並均質5分鐘使體系更加均勻。在擾 拌的同時冷卻到30°C ’加入煙用草莓香精1〇克,擾掉均句, 在溫度是181的環境中放置13小時後即為成品。 實施例2,凝膠態草莓香味煙用香精的製造: 依次稱取甘油25克、聚丙稀酸納5克,混合並攪拌均勻, 201236581 加熱到9(TC溶解完全,並均質5分鐘使體系更加 到Ϊ 入煙用草每香精1〇克,擾拌均勾見 在値度疋18 C的環境中放置18小時後即為成品。 實施例3,凝膠態草莓香味煙用香精的製造: 依次稱取甘油25G克、聚㈣賴5克,混合 if二Γ㈣完全’並均質5分鐘使體系更加均句。在擾 拌的同時冷卻到50C,加入煙用草莓香精1〇克,擾拌 在溫度是18Ϊ的環境中放置24小時後即為成品。=二’ 實施例4,凝膠態轉檬香味煙用香精的製造: 依次稱取甘油40克、聚丙稀酸納8克,混合並攪拌 =熱到%。c溶解完全,並均質10分鐘使體系更加均句;在 拌的同時冷卻到30。〇,加入煙用檸檬香精15克, 在溫度是15。(:的環境中放置13小時後即為成品。_二, 實施例5 ’凝谬態棒檬香味煙用香精的製造: 依次稱取甘油80克、聚丙稀酸納8克,混合並攪拌均句, 加熱到8(TC溶解完全,並均質10分鐘使體系更加均勻。-在浐 拌的同時冷卻到饥,加入煙用檸檬香精ls克,攪拌 i 在溫度是15°C的環境中放置18小時後即為成品。 一, 實知例6 ’凝膠態棒樣香味煙用香精的製造: 依次稱取甘油400克、聚丙稀酸鈉8克,混合並攪拌均句, 加熱到10(TC溶解完全,並均質10分鐘使體系更加均句。一在 攪拌的同時冷卻到5〇。(:,加入煙用檸檬香精15克,攪拌均勻, 在溫度是15°C的環境中放置24小時後即為成品。 一’ 【圖式簡單說明】 益 «、、、 【主要元件符號說明】201236581 VI. Description of the invention: [Technical field of invention] Cheng Ning', especially the manufacture of water-soluble tobacco flavors [Prior Art] The aroma type and the money style of the tobacco flavor are in the grade and grade of the smoke, usually _ burning In the process, the organic matter in the process, if added to the cigarette, the spicy taste produced during the process of producing the two spicy flavors, the current form of essential oil, _ fragrant _ wave = lost in the gas production process of cigarettes, in order to improve Fragrance of the scent of scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scented scent less. Beibei's use of refined scent to cause gelation is reported in the current related technical report. [Inventive content] The refined qi supply will be realized by the following technical solutions: The ratio is 1: According to food increase _ and glycerin Add quality mix and dissolve completely, homogenize ^ ', disturb evenly mixed' heating to break: ~ WC stir the king said 5 to 15 minutes, cool heart 〇 t ~ 耽 plus 201236581 smoky tobacco with aroma stir evenly, rc ~ 30 ° c placed The finished product is obtained in at least 12 hours, wherein the food thickener is preferably sodium polyacrylate. The present invention has the following effects in the gel state of the water-soluble tobacco flavor: (1) The present invention makes the water-soluble tobacco flavor into a gel state, which is more convenient to use, and is more flexible in packaging transportation and storage. (2) The present invention makes the water-soluble tobacco flavor into a gel state, which greatly improves the ability of the tobacco flavor to resist heat and light, and avoids discoloration and odor caused by direct external light and heat. The invention adopts the water-soluble tobacco flavor into a gel state, and the volatilization of the essence is suppressed to a large extent, the flavor remains intact, and the loss of some volatile components is reduced. (4) The present invention makes the water-soluble tobacco flavor into a gel state, which can improve the quality of the product and increase the fragrance retention. (5) The present invention makes the water-soluble tobacco flavor into a gel state, and does not contain water, and can be kept frozen at a low temperature of -20 °C. (6) The invention has low production cost, easy access to raw materials, and simple production process, which is convenient for actual production. κ In addition, polyacrylic acid can dissolve in glycerin to form a very viscous transparent liquid. Its viscosity is due to the ionic phenomenon of many anionic groups in the molecule, which causes the molecular chain to grow, and the viscosity is increased to form a highly viscous solution. The change is minimal.曰【Embodiment】 Example 1, the manufacture of gelatinized strawberry flavored tobacco flavor: Weighed 85 grams of glycerin and 5 grams of sodium polyacrylate, mixed and stirred, and heated to 8 (TC dissolved completely) and homogenized 5 minutes to make the system more uniform. Cooled to 30 ° C while disturbing. 'Adding strawberry flavor 1 gram of tobacco, disturbing the average sentence, and placing it in the environment with temperature of 181 for 13 hours is the finished product. Manufacture of gelatinized strawberry flavored tobacco flavor: Weigh 25 grams of glycerin and 5 grams of sodium polyacrylate, mix and stir evenly, heat it to 9 at 201236581 (TC dissolves completely, and homogenizes for 5 minutes to make the system more entangled) The tobacco grass is 1 gram per fragrance, and the scrambled mixture is placed in the environment of 18 ° C for 18 hours, which is the finished product. Example 3: Gelatinized strawberry flavored tobacco flavor: glycerin is weighed in order 25G grams, poly (four) Lai 5 grams, mixed if two (four) completely 'and homogenization for 5 minutes to make the system more uniform. Cooled to 50C while disturbing, add tobacco strawberry flavor 1 gram, disturbed at a temperature of 18 Ϊ After being placed in the environment for 24 hours, it is the finished product. = two ' real Example 4: Manufacture of gelatinous flavored tobacco flavor: 40 grams of glycerin and 8 grams of sodium polyacrylate were weighed, mixed and stirred = heat to %. c dissolved completely, and homogenized for 10 minutes to make the system more uniform Sentence; cool to 30 while mixing. 〇, add 15 grams of tobacco with lemon essence, the temperature is 15. (13: after the environment is placed in the finished product. _ 2, Example 5 'condensed state lemon Manufacture of flavored tobacco flavor: Weigh 80 grams of glycerin and 8 grams of sodium polyacrylate, mix and stir, and heat to 8 (TC dissolves completely, and homogenizes for 10 minutes to make the system more uniform. - While mixing Cooling to hunger, adding 7.5 grams of lemon flavor, stirring i is placed in an environment where the temperature is 15 ° C for 18 hours, which is the finished product. I, Example 6 The manufacture of gel-like aroma-like flavors: Weigh 400 g of glycerin and 8 g of sodium polyacrylate in sequence, mix and stir, and heat to 10 (TC dissolves completely, and homogenizes for 10 minutes to make the system more uniform. One is cooled to 5 搅拌 while stirring. Add 15 grams of tobacco with lemon flavor, stir evenly, at a temperature of 15 ° C ring In 24 hours after products A '[Yi] Brief Description of the drawings «,,, Main reference numerals DESCRIPTION

Claims (1)

201236581 七、申請專利範圍: 食^增補賴該食品增綱與甘油的添加品 .50〜〗· s混合,擾拌均勻加熱到8〇它〜1〇〇七搜拌 卜-種,職水溶性賴香精 方法, 將甘油與一▲ 例為1 : 50〜1 溶解完全’均質5〜15分鐘,冷卻到3(rC〜耽加入— 煙用香精攪拌均勻,在1°C〜30〇C下放置至少12小時而^^該 凝膠態水溶性煙用香精。 f s 2、如申請專利範圍第1項所述之凝膠態水溶性煙用香精製造方 法,其中該食品增稍劑為聚丙稀酸納。 & s 201236581 四、指定代表圖: (一) 本案指定代表圖為:第(無)圖。 (二) 本代表圖之元件符號簡單說明: 無 五、本案若有化學式時,請揭示最能顯示發明特徵的化學式: 無201236581 VII, the scope of application for patents: food ^ supplements the food supplement and glycerin additives. 50 ~ 〗 s mix, disturbed evenly heated to 8 〇 it ~ 1 〇〇 搜 拌 - 种 种 种 种 种Laixiangjing method, dissolve glycerin with a ▲ case 1: 50~1 completely 'homogeneous 5~15 minutes, cool to 3 (rC~耽 add - mix with tobacco flavor, place at 1 °C~30〇C The method for producing a gelatinous water-soluble tobacco flavor according to the first aspect of the invention, wherein the food-increasing agent is polyacrylic acid, at least 12 hours. & s 201236581 IV. Designated representative map: (1) The representative representative of the case is: (No). (2) The symbol of the representative figure is simple: No. 5. If there is a chemical formula in this case, please reveal The chemical formula that best shows the characteristics of the invention: None
TW100113242A 2011-03-02 2011-04-15 Preparation method of gel state water-soluble essence for tobacco TW201236581A (en)

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CN103535851B (en) * 2013-10-22 2015-11-18 深圳市凯神科技股份有限公司 solid tobacco tar and processing method thereof
CN107365628A (en) * 2017-06-29 2017-11-21 云南中烟新材料科技有限公司 A kind of cigarette fragrance sustained release agent and its preparation method and application
JP2023507455A (en) * 2019-12-18 2023-02-22 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Formulations for use in aerosol-generating systems

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CN1153667A (en) * 1996-01-02 1997-07-09 崔京怡 Ultrasonic coupling agent
CN1135860A (en) * 1996-05-09 1996-11-20 徐度 Atomized cigarette
US7575697B2 (en) * 2004-08-04 2009-08-18 Intematix Corporation Silicate-based green phosphors
CN101461566B (en) * 2009-01-08 2012-01-18 华健 Atomized liquid of electronic smoke
CN101869657A (en) * 2010-06-29 2010-10-27 吴轲 Plaster used together with cigarettes, method for preparing same and ring containing same
CN101926505A (en) * 2010-08-09 2010-12-29 深圳市如烟生物科技有限公司 Caffeine electronic cigarette liquid

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