TR201902160T4 - Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. - Google Patents

Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. Download PDF

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Publication number
TR201902160T4
TR201902160T4 TR2019/02160T TR201902160T TR201902160T4 TR 201902160 T4 TR201902160 T4 TR 201902160T4 TR 2019/02160 T TR2019/02160 T TR 2019/02160T TR 201902160 T TR201902160 T TR 201902160T TR 201902160 T4 TR201902160 T4 TR 201902160T4
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TR
Turkey
Prior art keywords
glycerol
fatty acid
mixture
aliphatic monoalcohol
equal
Prior art date
Application number
TR2019/02160T
Other languages
English (en)
Inventor
Lacoste François
Thiel Julien
Lair Valentin
Halloumi Samy
Original Assignee
Easyl
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Easyl filed Critical Easyl
Publication of TR201902160T4 publication Critical patent/TR201902160T4/tr

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/10—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with one or a few disintegrating members arranged in the container
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16—Mills in which a fixed container houses stirring means tumbling the charge
    • B02C17/163—Stirring means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/18—Details
    • B02C17/20—Disintegrating members
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Food Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)

Abstract

Buluş en az bir bitkisel veya hayvansal yağ ve en az bir alifatik monoalkol arasında bir dizi transesterleşme reaksiyonu kullanan, yağ asidi alkilik esterleri ve gliserol üretimine yönelik bir yöntem ile ilgili olup, yöntem aşağıdaki aşamaları içermektedir: (A) bir başlangıç karışımının oluşturulması için, en az bir bitkisel ve/veya hayvansal yağ, en az bir alifatik monoalkol ve en az bir heterojen ve/veya homojen katalizörün ayrı olarak veya karışım halinde bir mikro bilyalı üç boyutlu öğütücü içine sokulması; (B) söz konusu başlangıç karışımının 50°C'ye eşit veya daha düşük olan, tercihen 25°C'ye eşit veya daha düşük olan bir sıcaklıkta, 5 dakikaya eşit veya daha düşük olan, tercihen 5 ila 30 saniye arasında değişen ve tipik olarak 5 ila 15 saniye arasında değişen bir kalma süresi boyunca bir mikro bilyalı üç boyutlu öğütücü içinde öğütülmesi; (C) en az yağ asidi alkilik esterleri, gliserol, katalizör ve reaksiyona girmeyen alifatik monoalkol içeren bir nihai karışımın üç boyutlu öğütücünün çıkışında geri kazanılması; ve (D) bu nihai karışımın, yağ asidi alkilik esterleri içeren bir birinci faza ve gliserol, reaksiyona girmeyen alifatik monoalkol ve katalizör içeren bir ikinci faza ayrılması.
TR2019/02160T 2016-07-01 2017-06-30 Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. TR201902160T4 (tr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1656335A FR3053335B1 (fr) 2016-07-01 2016-07-01 Procede de production d'esters d'acides gras et de glycerol a basse temperature

Publications (1)

Publication Number Publication Date
TR201902160T4 true TR201902160T4 (tr) 2019-03-21

Family

ID=57539332

Family Applications (1)

Application Number Title Priority Date Filing Date
TR2019/02160T TR201902160T4 (tr) 2016-07-01 2017-06-30 Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem.

Country Status (10)

Country Link
US (1) US10533145B2 (tr)
EP (1) EP3322689B1 (tr)
BR (1) BR112018077522B1 (tr)
CA (1) CA3029073C (tr)
ES (1) ES2712130T3 (tr)
FR (1) FR3053335B1 (tr)
PL (1) PL3322689T3 (tr)
PT (1) PT3322689T (tr)
TR (1) TR201902160T4 (tr)
WO (1) WO2018002559A1 (tr)

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3442359A (en) 1967-06-23 1969-05-06 Edward J Atchison Vehicle drive apparatus
DE4123928A1 (de) 1991-07-19 1993-01-21 Metallgesellschaft Ag Verfahren zum erzeugen von fettsaeure-methylester oder fettsaeure-aethylester und glycerin durch umesterung von oelen oder fetten
FR2752242B1 (fr) 1996-08-08 1998-10-16 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huiles vegetales ou animales et d'alcools
FR2772756B1 (fr) 1997-12-18 2000-02-11 Inst Francais Du Petrole Procede de fabrication d'esters de corps gras et les esters de haute purete obtenus
FR2838433B1 (fr) 2002-04-11 2005-08-19 Inst Francais Du Petrole Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique
AU2003224942A1 (en) 2002-04-12 2003-10-27 Alfred Center Continuous transesterification process
US7420072B2 (en) 2006-05-05 2008-09-02 Orbitek, Inc. Apparatus and method for producing biodiesel fuel
US8901330B2 (en) * 2007-08-29 2014-12-02 Sauber Llc Method for production of biofuel
FR2962727B1 (fr) 2009-09-11 2012-08-10 IFP Energies Nouvelles Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee
US8580119B1 (en) * 2012-11-27 2013-11-12 Menlo Energy Management, LLC Transesterification of biodiesel feedstock with solid heterogeneous catalyst
US9492806B2 (en) * 2013-12-10 2016-11-15 Heiko Ackermann Cavitation generation mechanisms and their use in fermentation and wastewater and sand cleaning processes

Also Published As

Publication number Publication date
FR3053335A1 (fr) 2018-01-05
FR3053335B1 (fr) 2019-07-05
CA3029073A1 (fr) 2018-01-04
BR112018077522A2 (pt) 2019-04-02
EP3322689B1 (fr) 2018-11-21
PT3322689T (pt) 2019-02-25
BR112018077522B1 (pt) 2022-10-11
CA3029073C (fr) 2024-04-16
PL3322689T3 (pl) 2019-06-28
ES2712130T3 (es) 2019-05-09
US20190345413A1 (en) 2019-11-14
EP3322689A1 (fr) 2018-05-23
US10533145B2 (en) 2020-01-14
WO2018002559A1 (fr) 2018-01-04

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