TR201902160T4 - Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. - Google Patents
Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. Download PDFInfo
- Publication number
- TR201902160T4 TR201902160T4 TR2019/02160T TR201902160T TR201902160T4 TR 201902160 T4 TR201902160 T4 TR 201902160T4 TR 2019/02160 T TR2019/02160 T TR 2019/02160T TR 201902160 T TR201902160 T TR 201902160T TR 201902160 T4 TR201902160 T4 TR 201902160T4
- Authority
- TR
- Turkey
- Prior art keywords
- glycerol
- fatty acid
- mixture
- aliphatic monoalcohol
- equal
- Prior art date
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title abstract 12
- 235000014113 dietary fatty acids Nutrition 0.000 title abstract 4
- 229930195729 fatty acid Natural products 0.000 title abstract 4
- 239000000194 fatty acid Substances 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- -1 fatty acid esters Chemical class 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 5
- 125000001931 aliphatic group Chemical group 0.000 abstract 4
- 235000019737 Animal fat Nutrition 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000011806 microball Substances 0.000 abstract 2
- 235000019871 vegetable fat Nutrition 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- 239000002638 heterogeneous catalyst Substances 0.000 abstract 1
- 239000002815 homogeneous catalyst Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 238000005809 transesterification reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
- B02C17/10—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with one or a few disintegrating members arranged in the container
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
- B02C17/16—Mills in which a fixed container houses stirring means tumbling the charge
- B02C17/163—Stirring means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
- B02C17/18—Details
- B02C17/20—Disintegrating members
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
- C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/002—Mixed oxides other than spinels, e.g. perovskite
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Food Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Abstract
Buluş en az bir bitkisel veya hayvansal yağ ve en az bir alifatik monoalkol arasında bir dizi transesterleşme reaksiyonu kullanan, yağ asidi alkilik esterleri ve gliserol üretimine yönelik bir yöntem ile ilgili olup, yöntem aşağıdaki aşamaları içermektedir: (A) bir başlangıç karışımının oluşturulması için, en az bir bitkisel ve/veya hayvansal yağ, en az bir alifatik monoalkol ve en az bir heterojen ve/veya homojen katalizörün ayrı olarak veya karışım halinde bir mikro bilyalı üç boyutlu öğütücü içine sokulması; (B) söz konusu başlangıç karışımının 50°C'ye eşit veya daha düşük olan, tercihen 25°C'ye eşit veya daha düşük olan bir sıcaklıkta, 5 dakikaya eşit veya daha düşük olan, tercihen 5 ila 30 saniye arasında değişen ve tipik olarak 5 ila 15 saniye arasında değişen bir kalma süresi boyunca bir mikro bilyalı üç boyutlu öğütücü içinde öğütülmesi; (C) en az yağ asidi alkilik esterleri, gliserol, katalizör ve reaksiyona girmeyen alifatik monoalkol içeren bir nihai karışımın üç boyutlu öğütücünün çıkışında geri kazanılması; ve (D) bu nihai karışımın, yağ asidi alkilik esterleri içeren bir birinci faza ve gliserol, reaksiyona girmeyen alifatik monoalkol ve katalizör içeren bir ikinci faza ayrılması.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1656335A FR3053335B1 (fr) | 2016-07-01 | 2016-07-01 | Procede de production d'esters d'acides gras et de glycerol a basse temperature |
Publications (1)
Publication Number | Publication Date |
---|---|
TR201902160T4 true TR201902160T4 (tr) | 2019-03-21 |
Family
ID=57539332
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TR2019/02160T TR201902160T4 (tr) | 2016-07-01 | 2017-06-30 | Düşük sıcaklıkta yağ asidi esterleri ve gliserolün üretilmesine yönelik yöntem. |
Country Status (10)
Country | Link |
---|---|
US (1) | US10533145B2 (tr) |
EP (1) | EP3322689B1 (tr) |
BR (1) | BR112018077522B1 (tr) |
CA (1) | CA3029073C (tr) |
ES (1) | ES2712130T3 (tr) |
FR (1) | FR3053335B1 (tr) |
PL (1) | PL3322689T3 (tr) |
PT (1) | PT3322689T (tr) |
TR (1) | TR201902160T4 (tr) |
WO (1) | WO2018002559A1 (tr) |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3442359A (en) | 1967-06-23 | 1969-05-06 | Edward J Atchison | Vehicle drive apparatus |
DE4123928A1 (de) | 1991-07-19 | 1993-01-21 | Metallgesellschaft Ag | Verfahren zum erzeugen von fettsaeure-methylester oder fettsaeure-aethylester und glycerin durch umesterung von oelen oder fetten |
FR2752242B1 (fr) | 1996-08-08 | 1998-10-16 | Inst Francais Du Petrole | Procede de fabrication d'esters a partir d'huiles vegetales ou animales et d'alcools |
FR2772756B1 (fr) | 1997-12-18 | 2000-02-11 | Inst Francais Du Petrole | Procede de fabrication d'esters de corps gras et les esters de haute purete obtenus |
FR2838433B1 (fr) | 2002-04-11 | 2005-08-19 | Inst Francais Du Petrole | Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique |
WO2003087279A2 (en) | 2002-04-12 | 2003-10-23 | Cornell Research Foundation, Inc. | Continuous transesterification process |
US7420072B2 (en) | 2006-05-05 | 2008-09-02 | Orbitek, Inc. | Apparatus and method for producing biodiesel fuel |
US8901330B2 (en) * | 2007-08-29 | 2014-12-02 | Sauber Llc | Method for production of biofuel |
FR2962727B1 (fr) | 2009-09-11 | 2012-08-10 | IFP Energies Nouvelles | Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee |
US8580119B1 (en) * | 2012-11-27 | 2013-11-12 | Menlo Energy Management, LLC | Transesterification of biodiesel feedstock with solid heterogeneous catalyst |
US9492806B2 (en) * | 2013-12-10 | 2016-11-15 | Heiko Ackermann | Cavitation generation mechanisms and their use in fermentation and wastewater and sand cleaning processes |
-
2016
- 2016-07-01 FR FR1656335A patent/FR3053335B1/fr not_active Expired - Fee Related
-
2017
- 2017-06-30 PL PL17745416T patent/PL3322689T3/pl unknown
- 2017-06-30 CA CA3029073A patent/CA3029073C/fr active Active
- 2017-06-30 WO PCT/FR2017/051778 patent/WO2018002559A1/fr active Application Filing
- 2017-06-30 TR TR2019/02160T patent/TR201902160T4/tr unknown
- 2017-06-30 BR BR112018077522-3A patent/BR112018077522B1/pt active IP Right Grant
- 2017-06-30 ES ES17745416T patent/ES2712130T3/es active Active
- 2017-06-30 US US16/314,506 patent/US10533145B2/en active Active
- 2017-06-30 PT PT17745416T patent/PT3322689T/pt unknown
- 2017-06-30 EP EP17745416.2A patent/EP3322689B1/fr active Active
Also Published As
Publication number | Publication date |
---|---|
BR112018077522B1 (pt) | 2022-10-11 |
EP3322689B1 (fr) | 2018-11-21 |
US10533145B2 (en) | 2020-01-14 |
BR112018077522A2 (pt) | 2019-04-02 |
PT3322689T (pt) | 2019-02-25 |
FR3053335A1 (fr) | 2018-01-05 |
CA3029073C (fr) | 2024-04-16 |
ES2712130T3 (es) | 2019-05-09 |
US20190345413A1 (en) | 2019-11-14 |
CA3029073A1 (fr) | 2018-01-04 |
EP3322689A1 (fr) | 2018-05-23 |
FR3053335B1 (fr) | 2019-07-05 |
PL3322689T3 (pl) | 2019-06-28 |
WO2018002559A1 (fr) | 2018-01-04 |
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