FR2962727B1 - Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee - Google Patents

Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee

Info

Publication number
FR2962727B1
FR2962727B1 FR1002971A FR1002971A FR2962727B1 FR 2962727 B1 FR2962727 B1 FR 2962727B1 FR 1002971 A FR1002971 A FR 1002971A FR 1002971 A FR1002971 A FR 1002971A FR 2962727 B1 FR2962727 B1 FR 2962727B1
Authority
FR
France
Prior art keywords
triglycerides
glycerin
alcohols
preparation
heterogeneous catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1002971A
Other languages
English (en)
Other versions
FR2962727A1 (fr
Inventor
Vincent Coupard
Sylvie Maury
Veronique Pugnet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from FR0904349A external-priority patent/FR2962728A1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR1002971A priority Critical patent/FR2962727B1/fr
Priority to ES201031283A priority patent/ES2358663B1/es
Priority to BRPI1003366-1A priority patent/BRPI1003366A2/pt
Priority to MYPI2010004176A priority patent/MY166244A/en
Priority to SE1050927A priority patent/SE534664C2/sv
Priority to US12/879,528 priority patent/US8362288B2/en
Publication of FR2962727A1 publication Critical patent/FR2962727A1/fr
Publication of FR2962727B1 publication Critical patent/FR2962727B1/fr
Application granted granted Critical
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/005—Spinels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/005—Spinels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/06—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of zinc, cadmium or mercury
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0036—Grinding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1018—Biomass of animal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80—Additives
    • C10G2300/805—Water
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
FR1002971A 2009-09-11 2010-07-15 Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee Expired - Fee Related FR2962727B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1002971A FR2962727B1 (fr) 2009-09-11 2010-07-15 Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee
ES201031283A ES2358663B1 (es) 2009-09-11 2010-08-25 Procedimiento de preparación de ésteres alcohólicos y de glicerina a partir de triglicéridos y de alcoholes por medio de un catalizador heterogéneo en presencia de agua en un contenido controlado.
BRPI1003366-1A BRPI1003366A2 (pt) 2009-09-11 2010-09-03 processo de preparação de ésteres alcoólicos e de glicerina a partir de triglicerìdeos e de alcoóis com o auxìlio de um catalisador heterogêneo na presença de água em teor controlado
MYPI2010004176A MY166244A (en) 2009-09-11 2010-09-06 Process for preparing esters of alcohols and glycerin from triglycerides and alcohols using a heterogeneous catalyst in the presence of a controlled quantity of water
SE1050927A SE534664C2 (sv) 2009-09-11 2010-09-08 Förfarande för framställning av estrar av alkoholer och glycerin från triglycerider och alkoholer genom användning av en heterogen katalysator i närvaro av en kontrollerad mängd vatten.
US12/879,528 US8362288B2 (en) 2009-09-11 2010-09-10 Process for preparing esters of alcohols and glycerin from triglycerides and alcohols using a heterogeneous catalyst in the presence of a controlled quantity of water

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0904349A FR2962728A1 (fr) 2009-09-11 2009-09-11 Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee
FR1002971A FR2962727B1 (fr) 2009-09-11 2010-07-15 Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee

Publications (2)

Publication Number Publication Date
FR2962727A1 FR2962727A1 (fr) 2012-01-20
FR2962727B1 true FR2962727B1 (fr) 2012-08-10

Family

ID=43731209

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1002971A Expired - Fee Related FR2962727B1 (fr) 2009-09-11 2010-07-15 Procede de preparation d'esters alcooliques et de glycerine a partir de triglycerides et d'alcools au moyen d'un catalyseur heterogene en presence d'eau en teneur controlee

Country Status (6)

Country Link
US (1) US8362288B2 (fr)
BR (1) BRPI1003366A2 (fr)
ES (1) ES2358663B1 (fr)
FR (1) FR2962727B1 (fr)
MY (1) MY166244A (fr)
SE (1) SE534664C2 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017119007A1 (fr) 2016-01-07 2017-07-13 Institute Of Chemical Technology Procédé de purification et de raffinage du glycérol
FR3053335B1 (fr) 2016-07-01 2019-07-05 Easyl Procede de production d'esters d'acides gras et de glycerol a basse temperature

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2752242B1 (fr) * 1996-08-08 1998-10-16 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huiles vegetales ou animales et d'alcools
FR2794768B1 (fr) * 1999-06-11 2006-07-07 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huile de ricin et d'alcools utilisant un catalyseur heterogene
FR2838433B1 (fr) * 2002-04-11 2005-08-19 Inst Francais Du Petrole Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique
WO2004026465A1 (fr) * 2002-09-23 2004-04-01 Shell Internationale Research Maatschappij B.V. Particules de catalyseur et utilisation dans la désulfuration
FR2852531B1 (fr) * 2003-03-17 2007-06-01 Procede de preparation d'un catalyseur a base d'aluminate de zinc et catalyseur obtenu
FR2852602B1 (fr) * 2003-03-17 2007-08-10 Inst Francais Du Petrole Procede d'alcoolyse d'huiles acides d'origine vegetale ou animale
FR2890963A1 (fr) * 2005-09-16 2007-03-23 Inst Francais Du Petrole Procede de fabrication d'esters ethyliques d'acides gras a partir de triglycerides et d'alcools
WO2008129226A1 (fr) * 2007-04-18 2008-10-30 Petroleo Brasileiro S.A. - Petrobras Procédé d'augmentation de l'indice de cétane et additif pour carburant diesel

Also Published As

Publication number Publication date
US8362288B2 (en) 2013-01-29
SE534664C2 (sv) 2011-11-08
BRPI1003366A2 (pt) 2012-05-29
FR2962727A1 (fr) 2012-01-20
ES2358663B1 (es) 2012-03-23
ES2358663A1 (es) 2011-05-12
SE1050927A1 (sv) 2011-03-12
MY166244A (en) 2018-06-22
US20110065942A1 (en) 2011-03-17

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Effective date: 20150331