TR201902111T4 - Çökeltilen silikaların hazırlanmasına yönelik yeni proses, çökeltilen yeni silikalar ve bunların özellikle polimerlerin takviyelendirilmesine yönelik kullanımları. - Google Patents

Çökeltilen silikaların hazırlanmasına yönelik yeni proses, çökeltilen yeni silikalar ve bunların özellikle polimerlerin takviyelendirilmesine yönelik kullanımları. Download PDF

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Publication number
TR201902111T4
TR201902111T4 TR2019/02111T TR201902111T TR201902111T4 TR 201902111 T4 TR201902111 T4 TR 201902111T4 TR 2019/02111 T TR2019/02111 T TR 2019/02111T TR 201902111 T TR201902111 T TR 201902111T TR 201902111 T4 TR201902111 T4 TR 201902111T4
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TR
Turkey
Prior art keywords
new
precipitated silicas
preparation
reinforcement
polymers
Prior art date
Application number
TR2019/02111T
Other languages
English (en)
Inventor
Boivin Cédric
Guy Laurent
Perin Eric
Lamiri Kilani
Original Assignee
Rhodia Operations
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Rhodia Operations filed Critical Rhodia Operations
Publication of TR201902111T4 publication Critical patent/TR201902111T4/tr

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
    • C08K5/092—Polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C08K3/36—Silica
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/02—Ingredients treated with inorganic substances
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3045—Treatment with inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3063—Treatment with low-molecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/06—Treatment with inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2227—Oxides; Hydroxides of metals of aluminium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

Buluş, bir çökeltilen silikanın hazırlanmasına yönelik yeni bir proses ile ilgilidir, burada: - çökeltilen silikanın bir süspansiyonunun elde edileceği şekilde, en az bir asitleştirme ajanı ile bir silika reakte ettirilir, - bir filtrasyon kekinin elde edileceği şekilde çökeltilen silikanın söz konusu süspansiyonu filtrelenir, - söz konusu filtrasyon keki, bir alüminyum bileşiğinin eklenmesini içeren bir parçalanma işlemine tabi tutulur, - parçalama işleminden sonra, bir kurutma adımına devam edilir, filtrasyon kekine, parçalama işlemi esnasında veya bundan sonra, metilglutarik asidin eklenmesi ile karakterize edilir. Bu aynı zamanda çökeltilen yeni silikalar ve bunların kullanımları ile ilgilidir.
TR2019/02111T 2012-08-31 2013-09-02 Çökeltilen silikaların hazırlanmasına yönelik yeni proses, çökeltilen yeni silikalar ve bunların özellikle polimerlerin takviyelendirilmesine yönelik kullanımları. TR201902111T4 (tr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1202349A FR2994962B1 (fr) 2012-08-31 2012-08-31 Nouveau procede de preparation de silices precitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres

Publications (1)

Publication Number Publication Date
TR201902111T4 true TR201902111T4 (tr) 2019-03-21

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Application Number Title Priority Date Filing Date
TR2019/02111T TR201902111T4 (tr) 2012-08-31 2013-09-02 Çökeltilen silikaların hazırlanmasına yönelik yeni proses, çökeltilen yeni silikalar ve bunların özellikle polimerlerin takviyelendirilmesine yönelik kullanımları.

Country Status (15)

Country Link
US (1) US9862810B2 (tr)
EP (1) EP2890638B1 (tr)
JP (1) JP5996807B2 (tr)
KR (1) KR101804877B1 (tr)
CN (1) CN104603055B (tr)
BR (1) BR112015004241B1 (tr)
CA (1) CA2881281C (tr)
ES (1) ES2711573T3 (tr)
FR (1) FR2994962B1 (tr)
MX (1) MX360563B (tr)
PL (1) PL2890638T3 (tr)
RU (1) RU2673521C2 (tr)
TR (1) TR201902111T4 (tr)
TW (1) TWI508919B (tr)
WO (1) WO2014033301A1 (tr)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2681845T3 (es) * 2014-02-14 2018-09-17 Rhodia Operations Proceso para la preparación de sílice precipitada, sílice precipitada y sus usos, en particular para el refuerzo de polímeros
KR102398812B1 (ko) * 2014-02-14 2022-05-17 로디아 오퍼레이션스 침강 실리카의 제조 방법, 침강 실리카, 및 특히 중합체 보강을 위한 이의 용도
FR3018070B1 (fr) 2014-02-28 2017-09-15 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR3018072B1 (fr) * 2014-02-28 2019-10-25 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
EP3114083A1 (en) * 2014-03-05 2017-01-11 Rhodia Operations Process for the preparation of precipitated silicas, precipitated silicas and their uses, in particular for the reinforcement of polymers
WO2016199429A1 (ja) * 2015-06-12 2016-12-15 株式会社ブリヂストン ゴム組成物及びタイヤ
WO2019106562A1 (en) * 2017-11-29 2019-06-06 Pirelli Tyre S.P.A. Microbeads comprising silicate fibres with needle-shaped morphology of nanometric size, preparation thereof, elastomeric compositions and tyres for vehicles comprising them
EP3820816A1 (en) * 2018-07-13 2021-05-19 Rhodia Operations Precipitated silica with improved processing properties
WO2021186210A1 (en) * 2020-03-16 2021-09-23 Bridgestone Europe Nv/Sa Rubber composition, rubber product and tyre

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SU1420000A1 (ru) * 1986-01-02 1988-08-30 Предприятие П/Я В-2609 Полимерна композици
FR2627176B1 (fr) 1988-02-11 1990-06-15 Rhone Poulenc Chimie Suspension aqueuse stable de silice de precipitation
FR2732331B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant du zinc et leur utilisation au renforcement des elastomeres
FR2732328B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant de l'aluminium et leur utilisation au renforcement des elastomeres
KR100244062B1 (ko) * 1994-06-07 2000-02-01 로디아 쉬미 침강 실리카의 제조 방법, 알루미늄을 함유하는침강 실리카 및 이의 엘라스토머 강화용 용도
FR2732329B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant de l'aluminium et leur utilisation au renforcement des elastomeres
FR2732351B1 (fr) * 1995-03-29 1998-08-21 Michelin & Cie Composition de caoutchouc pour enveloppe de pneumatique renfermant de la silice dopee aluminium a titre de charge renforcante
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FR2994963B1 (fr) 2012-08-31 2014-10-03 Rhodia Operations Nouveau procede de preparation de silices precipitees, nouvelles silices precipitees et leurs utilisations, notamment pour le renforcement de polymeres
FR2994961B1 (fr) * 2012-08-31 2014-10-03 Rhodia Operations Nouveau procede de preparation de silices precipitee, nouvelles silices precipitees et leur utilisations, notamment pour le renforcement de polymeres

Also Published As

Publication number Publication date
JP2015529625A (ja) 2015-10-08
TW201425225A (zh) 2014-07-01
EP2890638A1 (fr) 2015-07-08
MX360563B (es) 2018-11-07
TWI508919B (zh) 2015-11-21
RU2673521C2 (ru) 2018-11-27
JP5996807B2 (ja) 2016-09-21
KR20150046289A (ko) 2015-04-29
PL2890638T3 (pl) 2019-05-31
FR2994962A1 (fr) 2014-03-07
CN104603055B (zh) 2016-10-26
ES2711573T3 (es) 2019-05-06
CA2881281A1 (fr) 2014-03-06
US9862810B2 (en) 2018-01-09
CA2881281C (fr) 2020-10-27
FR2994962B1 (fr) 2014-12-26
BR112015004241A2 (pt) 2017-07-04
CN104603055A (zh) 2015-05-06
KR101804877B1 (ko) 2017-12-06
EP2890638B1 (fr) 2018-11-14
RU2015111246A (ru) 2016-10-20
US20150247022A1 (en) 2015-09-03
MX2015002581A (es) 2015-06-22
WO2014033301A1 (fr) 2014-03-06
BR112015004241B1 (pt) 2021-09-21

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