SU862823A3 - Способ получени 5-(4-аминобутил)-гидантоина или их смеси 5-(4-аминобутил)гидантоина с 1-уреидо-5-аминокапронамидом - Google Patents
Способ получени 5-(4-аминобутил)-гидантоина или их смеси 5-(4-аминобутил)гидантоина с 1-уреидо-5-аминокапронамидом Download PDFInfo
- Publication number
- SU862823A3 SU862823A3 SU782564302A SU2564302A SU862823A3 SU 862823 A3 SU862823 A3 SU 862823A3 SU 782564302 A SU782564302 A SU 782564302A SU 2564302 A SU2564302 A SU 2564302A SU 862823 A3 SU862823 A3 SU 862823A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- aminobutyl
- hydantoin
- ureido
- catalyst
- carried out
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims 4
- VQEWBNPYMIPJQY-UHFFFAOYSA-N 5-(4-aminobutyl)imidazolidine-2,4-dione Chemical compound NCCCCC1NC(=O)NC1=O VQEWBNPYMIPJQY-UHFFFAOYSA-N 0.000 title abstract 3
- 239000003054 catalyst Substances 0.000 claims abstract description 11
- 238000005984 hydrogenation reaction Methods 0.000 claims abstract 3
- 229910017052 cobalt Inorganic materials 0.000 claims description 5
- 239000010941 cobalt Substances 0.000 claims description 5
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 125000004042 4-aminobutyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])N([H])[H] 0.000 claims 1
- 239000007791 liquid phase Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 6
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 abstract description 2
- 239000004472 Lysine Substances 0.000 abstract description 2
- WJRBRSLFGCUECM-UHFFFAOYSA-N hydantoin Chemical compound O=C1CNC(=O)N1 WJRBRSLFGCUECM-UHFFFAOYSA-N 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 229940091173 hydantoin Drugs 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 229910052759 nickel Inorganic materials 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 238000004255 ion exchange chromatography Methods 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D233/72—Two oxygen atoms, e.g. hydantoin
- C07D233/76—Two oxygen atoms, e.g. hydantoin with substituted hydrocarbon radicals attached to the third ring carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7700046A NL7700046A (nl) | 1977-01-05 | 1977-01-05 | Werkwijze voor de bereiding van 5-(4-aminobutyl)- -hydantoine en/of 1-ureido-5-amino-capronamide. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU862823A3 true SU862823A3 (ru) | 1981-09-07 |
Family
ID=19827726
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU782564302A SU862823A3 (ru) | 1977-01-05 | 1978-01-05 | Способ получени 5-(4-аминобутил)-гидантоина или их смеси 5-(4-аминобутил)гидантоина с 1-уреидо-5-аминокапронамидом |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS5395918A (enrdf_load_stackoverflow) |
| DE (1) | DE2758953A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2376851A1 (enrdf_load_stackoverflow) |
| NL (1) | NL7700046A (enrdf_load_stackoverflow) |
| SU (1) | SU862823A3 (enrdf_load_stackoverflow) |
-
1977
- 1977-01-05 NL NL7700046A patent/NL7700046A/xx not_active Application Discontinuation
- 1977-12-27 JP JP15871577A patent/JPS5395918A/ja active Pending
- 1977-12-30 DE DE19772758953 patent/DE2758953A1/de not_active Withdrawn
-
1978
- 1978-01-03 FR FR7800036A patent/FR2376851A1/fr active Granted
- 1978-01-05 SU SU782564302A patent/SU862823A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5395918A (en) | 1978-08-22 |
| NL7700046A (nl) | 1978-07-07 |
| DE2758953A1 (de) | 1978-07-06 |
| FR2376851B1 (enrdf_load_stackoverflow) | 1983-01-28 |
| FR2376851A1 (fr) | 1978-08-04 |
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