SU649325A3 - Способ получени полифениленоксида - Google Patents
Способ получени полифениленоксидаInfo
- Publication number
- SU649325A3 SU649325A3 SU762364051A SU2364051A SU649325A3 SU 649325 A3 SU649325 A3 SU 649325A3 SU 762364051 A SU762364051 A SU 762364051A SU 2364051 A SU2364051 A SU 2364051A SU 649325 A3 SU649325 A3 SU 649325A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- reaction
- polyphenylene oxide
- amount
- phenol
- nitrogen
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 9
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 16
- 229920006380 polyphenylene oxide Polymers 0.000 claims description 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 13
- 229920000642 polymer Polymers 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- 150000005619 secondary aliphatic amines Chemical class 0.000 claims description 6
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 claims description 5
- 150000001412 amines Chemical class 0.000 claims description 4
- 238000006068 polycondensation reaction Methods 0.000 claims description 4
- 150000003335 secondary amines Chemical class 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 11
- 239000000203 mixture Substances 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- NXXYKOUNUYWIHA-UHFFFAOYSA-N 2,6-di-methyl phenol Natural products CC1=CC=CC(C)=C1O NXXYKOUNUYWIHA-UHFFFAOYSA-N 0.000 description 7
- 229920005989 resin Polymers 0.000 description 7
- 239000011347 resin Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 239000003054 catalyst Substances 0.000 description 6
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 5
- -1 for example Chemical compound 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 3
- WAEMQWOKJMHJLA-UHFFFAOYSA-N Manganese(2+) Chemical compound [Mn+2] WAEMQWOKJMHJLA-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 150000001340 alkali metals Chemical class 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000013522 chelant Substances 0.000 description 3
- 229910052748 manganese Inorganic materials 0.000 description 3
- 239000011572 manganese Substances 0.000 description 3
- WAKHLWOJMHVUJC-FYWRMAATSA-N (2e)-2-hydroxyimino-1,2-diphenylethanol Chemical compound C=1C=CC=CC=1C(=N/O)\C(O)C1=CC=CC=C1 WAKHLWOJMHVUJC-FYWRMAATSA-N 0.000 description 2
- TYTPPOBYRKMHAV-UHFFFAOYSA-N 2,6-dimethylphenol Chemical compound CC1=CC=CC(C)=C1O.CC1=CC=CC(C)=C1O TYTPPOBYRKMHAV-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- WAKHLWOJMHVUJC-UHFFFAOYSA-N benzoin alpha-oxime Natural products C=1C=CC=CC=1C(=NO)C(O)C1=CC=CC=C1 WAKHLWOJMHVUJC-UHFFFAOYSA-N 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 2
- WEHWNAOGRSTTBQ-UHFFFAOYSA-N dipropylamine Chemical class CCCNCCC WEHWNAOGRSTTBQ-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- QOJQBWSZHCKOLL-UHFFFAOYSA-N 2,6-dimethylbenzaldehyde Chemical compound CC1=CC=CC(C)=C1C=O QOJQBWSZHCKOLL-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 229920000265 Polyparaphenylene Polymers 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 125000002015 acyclic group Chemical group 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 125000004350 aryl cycloalkyl group Chemical group 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 125000001316 cycloalkyl alkyl group Chemical group 0.000 description 1
- 125000000753 cycloalkyl group Chemical group 0.000 description 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
- LAWOZCWGWDVVSG-UHFFFAOYSA-N dioctylamine Chemical class CCCCCCCCNCCCCCCCC LAWOZCWGWDVVSG-UHFFFAOYSA-N 0.000 description 1
- WWRCTCWJBIULBY-UHFFFAOYSA-N disodium oxygen(2-) hydrate Chemical compound O.[O-2].[Na+].[Na+] WWRCTCWJBIULBY-UHFFFAOYSA-N 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- PXSXRABJBXYMFT-UHFFFAOYSA-N n-hexylhexan-1-amine Chemical class CCCCCCNCCCCCC PXSXRABJBXYMFT-UHFFFAOYSA-N 0.000 description 1
- CATWEXRJGNBIJD-UHFFFAOYSA-N n-tert-butyl-2-methylpropan-2-amine Chemical compound CC(C)(C)NC(C)(C)C CATWEXRJGNBIJD-UHFFFAOYSA-N 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229920000412 polyarylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920005990 polystyrene resin Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003462 sulfoxides Chemical class 0.000 description 1
- 150000003510 tertiary aliphatic amines Chemical class 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
- C08G65/44—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols by oxidation of phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
- C08L71/08—Polyethers derived from hydroxy compounds or from their metallic derivatives
- C08L71/10—Polyethers derived from hydroxy compounds or from their metallic derivatives from phenols
- C08L71/12—Polyphenylene oxides
- C08L71/123—Polyphenylene oxides not modified by chemical after-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/582,910 US4054553A (en) | 1975-06-02 | 1975-06-02 | Polyphenylene oxide process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU649325A3 true SU649325A3 (ru) | 1979-02-25 |
Family
ID=24330945
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762364051A SU649325A3 (ru) | 1975-06-02 | 1976-06-02 | Способ получени полифениленоксида |
Country Status (10)
| Country | Link |
|---|---|
| US (2) | US4054553A (enExample) |
| JP (1) | JPS5925810B2 (enExample) |
| BE (1) | BE842436A (enExample) |
| DE (1) | DE2622700C2 (enExample) |
| DK (1) | DK242376A (enExample) |
| FR (1) | FR2313413A1 (enExample) |
| GB (1) | GB1544122A (enExample) |
| IT (1) | IT1060790B (enExample) |
| NL (1) | NL7605915A (enExample) |
| SU (1) | SU649325A3 (enExample) |
Families Citing this family (43)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4102865A (en) * | 1976-12-21 | 1978-07-25 | General Electric Company | Moderation of manganese chelate catalyzed polymerization of phenolic monomers with polyfunctional alkanolamines |
| US4075174A (en) * | 1976-12-21 | 1978-02-21 | General Electric Company | Promotion of manganese chelate catalyzed polyphenylene ether oxide polymerization reactions |
| US4154712A (en) * | 1977-09-30 | 1979-05-15 | General Electric Company | Low molecular weight polyphenylene ether compositions |
| US4207406A (en) * | 1978-05-09 | 1980-06-10 | General Electric Company | Process for preparing polyphenylene oxide copolymers |
| US4226951A (en) * | 1978-06-19 | 1980-10-07 | General Electric Company | Block polymers of polyphenylene oxide and polystyrene |
| US4223062A (en) * | 1978-11-15 | 1980-09-16 | Bell & Howell Company | Curl resistant photoplastic film |
| US4335234A (en) * | 1979-10-24 | 1982-06-15 | General Electric Company | Use of manganese chelate to oxidatively couple phenolic compound in a self-precipitating system |
| US4393152A (en) * | 1981-07-16 | 1983-07-12 | International Minerals & Chemicals Corp. | Oxidatively coupled cold-set binders |
| US4517341A (en) * | 1982-07-27 | 1985-05-14 | General Electric Company | Process for preparing polyphenylene oxide-rubber graft copolymers and products obtained thereby |
| US4477650A (en) * | 1983-03-25 | 1984-10-16 | General Electric Company | Process for polyphenylene oxide preparation including catalyst pre-mixing |
| US4477649A (en) * | 1983-03-25 | 1984-10-16 | General Electric Company | Two-stage continuous process for preparation of polyphenylene oxides |
| US4578449A (en) * | 1983-03-25 | 1986-03-25 | General Electric Company | Two-stage process for preparation of polyphenylene oxides |
| JPS608318A (ja) * | 1983-06-28 | 1985-01-17 | Asahi Chem Ind Co Ltd | ２，６−ジ置換フエノ−ルの重合方法 |
| DE3414237A1 (de) * | 1984-04-14 | 1985-10-24 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von polyphenylenethern und deren verwendung zur herstellung von formteilen |
| EP0225801B2 (en) * | 1985-12-06 | 1994-10-26 | Sumitomo Chemical Company, Limited | Optical devices |
| US5159027A (en) * | 1989-01-27 | 1992-10-27 | Asahi Kasei Kogyo Kabushiki Kaisha | Stabilized polyphenylene ether resin and process for the preparation of the same |
| US5001214A (en) * | 1989-06-23 | 1991-03-19 | General Electric Company | Low odor polyphenylene ether produced in the absence of odor causing amine, in presence of manganese chelate complex catalyst |
| US5089343A (en) * | 1989-08-03 | 1992-02-18 | General Electric Company | Curable dielectric polyphenylene ether-polyepoxide compositions |
| US5384360A (en) * | 1990-12-17 | 1995-01-24 | General Electric Company | Thermally stable blends of pre-extruded polyphenylene ether, diene based rubber and dialkylamines |
| US5037943A (en) * | 1990-12-18 | 1991-08-06 | General Electric Co. | Polyphenylene ether process and resin composition |
| US5250486A (en) * | 1990-12-18 | 1993-10-05 | General Electric Company | Polyphenylene ether process and resin composition |
| DE4129350A1 (de) * | 1991-09-04 | 1993-03-11 | Basf Ag | Verfahren zur herstellung von pentan-1,5-diaminen |
| EP0614927A4 (en) * | 1992-07-29 | 1995-02-01 | Sumitomo Chemical Co | MODIFIED POLYPHENYLENE ETHERS, THEIR PRODUCTION AND THERMOPLASTIC RESIN COMPOSITION. |
| WO1994003524A1 (fr) * | 1992-07-29 | 1994-02-17 | Sumitomo Chemical Company, Limited | Ether de polyphenylene modifie, sa production et composition de resine thermoplastique |
| US6518362B1 (en) | 1998-02-18 | 2003-02-11 | 3M Innovative Properties Company | Melt blending polyphenylene ether, polystyrene and curable epoxy |
| US6294270B1 (en) | 1998-12-23 | 2001-09-25 | 3M Innovative Properties Company | Electronic circuit device comprising an epoxy-modified aromatic vinyl-conjugated diene block copolymer |
| US6906120B1 (en) * | 2000-06-20 | 2005-06-14 | General Electric | Poly(arylene ether) adhesive compositions |
| US7022777B2 (en) * | 2001-06-28 | 2006-04-04 | General Electric | Moldable poly(arylene ether) thermosetting compositions, methods, and articles |
| US20030078347A1 (en) | 2001-08-28 | 2003-04-24 | General Electric Company | Triazine compounds, polymers comprising triazine structural units, and method |
| US6437084B1 (en) * | 2001-11-12 | 2002-08-20 | General Electric Company | Method of preparing a poly (arylene ether) and a poly (arylene ether) prepared thereby |
| US7214739B2 (en) * | 2003-04-22 | 2007-05-08 | General Electric Company | Composition and method for improving the surface adhesion of resin compositions to polyurethane foam |
| US7167148B2 (en) * | 2003-08-25 | 2007-01-23 | Texas Instruments Incorporated | Data processing methods and apparatus in digital display systems |
| US7041780B2 (en) * | 2003-08-26 | 2006-05-09 | General Electric | Methods of preparing a polymeric material composite |
| US7244813B2 (en) | 2003-08-26 | 2007-07-17 | General Electric Company | Methods of purifying polymeric material |
| US7354990B2 (en) * | 2003-08-26 | 2008-04-08 | General Electric Company | Purified polymeric materials and methods of purifying polymeric materials |
| US7256225B2 (en) * | 2003-08-26 | 2007-08-14 | General Electric Company | Methods of preparing a polymeric material |
| US20050048252A1 (en) * | 2003-08-26 | 2005-03-03 | Irene Dris | Substrate and storage media for data prepared therefrom |
| US6924350B2 (en) * | 2003-08-26 | 2005-08-02 | General Electric Company | Method of separating a polymer from a solvent |
| US20080076884A1 (en) * | 2006-09-21 | 2008-03-27 | Gary William Yeager | Poly(arylene ether) composition and method |
| US8595220B2 (en) | 2010-06-16 | 2013-11-26 | Microsoft Corporation | Community authoring content generation and navigation |
| US20130142979A1 (en) | 2010-07-01 | 2013-06-06 | Lubrizol Advanced Materials, Inc. | Thermoformed IC Trays Of Poly(Phenylene Ether) Compositions |
| WO2020079544A1 (en) | 2018-10-18 | 2020-04-23 | Sabic Global Technologies B.V. | Method of preparing a poly(phenylene ether), poly(phenylene ether) made thereby, and article comprising the poly(phenylene ether) |
| US11472920B2 (en) | 2019-01-22 | 2022-10-18 | Shpp Global Technologies B.V. | Method for preparing a poly(phenylene ether) and poly(phenylene ether) prepared thereby |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL295699A (enExample) * | 1962-07-24 | |||
| GB1125620A (en) * | 1965-01-06 | 1968-08-28 | Gen Electric | Improvements in polymeric blends |
| DE1570458A1 (de) * | 1965-07-14 | 1969-09-18 | Dynamit Nobel Ag | Verfahren zur Herstellung von Polyphenylenoxyden |
| JPS4826395B1 (enExample) * | 1970-12-01 | 1973-08-09 | ||
| US3825521A (en) * | 1971-07-31 | 1974-07-23 | Asahi Dow Ltd | Manganese amine chelate catalyzed aromatic polyether formation |
| US3956242A (en) * | 1974-07-24 | 1976-05-11 | General Electric Company | Preparation of polyphenylene oxide using a manganese (II) ω-hydroxyoxime chelate reaction promoter |
| US3972851A (en) * | 1974-07-24 | 1976-08-03 | General Electric Company | Preparation of polyphenylene oxide using a manganese(II) ortho-hydroxyarene-oxime chelate reaction promoter |
-
1975
- 1975-06-02 US US05/582,910 patent/US4054553A/en not_active Expired - Lifetime
-
1976
- 1976-05-21 DE DE2622700A patent/DE2622700C2/de not_active Expired
- 1976-05-26 FR FR7615897A patent/FR2313413A1/fr active Granted
- 1976-05-28 GB GB22315/76A patent/GB1544122A/en not_active Expired
- 1976-06-01 NL NL7605915A patent/NL7605915A/xx not_active Application Discontinuation
- 1976-06-01 IT IT23868/76A patent/IT1060790B/it active
- 1976-06-01 BE BE167512A patent/BE842436A/xx unknown
- 1976-06-02 DK DK242376A patent/DK242376A/da not_active Application Discontinuation
- 1976-06-02 SU SU762364051A patent/SU649325A3/ru active
- 1976-06-02 JP JP51063644A patent/JPS5925810B2/ja not_active Expired
-
1977
- 1977-08-19 US US05/825,926 patent/US4098846A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| NL7605915A (nl) | 1976-12-06 |
| BE842436A (fr) | 1976-10-01 |
| GB1544122A (en) | 1979-04-11 |
| DE2622700A1 (de) | 1976-12-23 |
| FR2313413B1 (enExample) | 1979-09-07 |
| FR2313413A1 (fr) | 1976-12-31 |
| DE2622700C2 (de) | 1985-07-11 |
| JPS52897A (en) | 1977-01-06 |
| DK242376A (da) | 1976-12-03 |
| US4098846A (en) | 1978-07-04 |
| IT1060790B (it) | 1982-09-30 |
| JPS5925810B2 (ja) | 1984-06-21 |
| US4054553A (en) | 1977-10-18 |
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