SU642316A1 - Method of obtaining phospholipids from vegetable raw material - Google Patents

Method of obtaining phospholipids from vegetable raw material

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Publication number
SU642316A1
SU642316A1 SU762426094A SU2426094A SU642316A1 SU 642316 A1 SU642316 A1 SU 642316A1 SU 762426094 A SU762426094 A SU 762426094A SU 2426094 A SU2426094 A SU 2426094A SU 642316 A1 SU642316 A1 SU 642316A1
Authority
SU
USSR - Soviet Union
Prior art keywords
precipitate
liters
acetone
water
extractor
Prior art date
Application number
SU762426094A
Other languages
Russian (ru)
Inventor
Роберт Августович Бринкманис
Инара Кришьяновна Гозите
Ария Мартыновна Ирген
Original Assignee
Предприятие П/Я Г-4740
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Предприятие П/Я Г-4740 filed Critical Предприятие П/Я Г-4740
Priority to SU762426094A priority Critical patent/SU642316A1/en
Application granted granted Critical
Publication of SU642316A1 publication Critical patent/SU642316A1/en

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Claims (1)

в экстрактор с турбу енгной мешалкой   отбойниками. За нвают 4О л ацетона, добавл ют аитаоксидант, включают мешалку и провод т экстракцию при 1525°С в течение 2 q. После экстракции смесь фильтруют и осадок промывают н фильтре 5   акетона. Осадок (1,3 кг) загружают в экстрактор с турбулентной мешалкой, дс вл ют 6,5 л воды и перемешивают в течение i ч при 15-25 Затем полученную коллоидальную систему подвергают высушиванию во взвешен ном состо нии ар  9О-110 С. Выход порошкообразного целевого пр дукта 65%, содержание фосфо ипндов 92,5%. Пример 2. 2 кг сырого фосфати ного концентрата из сои помешают в реактор с мешалкой и отбойниками. Заливают 45 л ацетона, добавл ют антиок сидант, включают мешалку и провод т экстракцию njffl 15-25 С в течение 2 После экстракции смесь фильтруют и осадок промывают на фильтре 5 л ацетона . Осадок {l,l кг) снова загружают в реактор с турбинной мешалкой, добав л ют 4.4   воды и перемеишвают при 15-25 G в течение 1 ч. После гидрофилиаации полученную коллоидную систему подвергают высушиванию во взвешенном состо нии при 9О-11О С. Выход порошкообразного целевого продукта 55%, содег кание фосфопипидов 89%. Пример 3. 2 кг сырого фосфатидного концентрата из подсолнечника помешают в экстрактор с турбинной мешалкой , заливают 4О л aueiOHa; добав-л ют антноксидант, включают мешалку и провод т экстракцию при 15-25 С в течение 2 ч. После экстракции смесь фильтруют и осадок промывают на фильтре 5 л ацетона. Сырой осадок (l,3 кг) сразу загружают в экстрактор с турбинной мешалкой, добавл ют 4,5 л воды и перемешивают в течение 1,5 ч при 15-25 С, затем полученную коллоидную систему подвергают высушиванию во взвешенном состо нии при 99-1 ЮС. Выход целевого продукта 65%, содержа гае фосфолипидов 92,5%. Формула изобретени  Способ получени  фосфолипидов из растительного сырь , включающий обработку фосфатидных концентратов ацетоном , фильтрацию, отличаю шийс   тем, что, с целью упрощени  процесса , увеличени  выхода и улучшени  качества целевого продукта, осадок фосфолипидов, полученный после фильтрации , обрабатывают водой при весовом ссютношении фосфолштиды: вода 1:3,5- - 1:5,5 при 15-25 С с последуишим высушиванием во взвешенном состо нии при 90-11О°С. Источники игаформапии, пршн тые во внимание при экспертизе 1. Патент США № 3031478, кл. 260-403, 1962.into the extractor with a turbo with an energetic agitator with bump stops. Add a 4 L of acetone, add an antioxidant, turn on the stirrer, and extract at 1525 ° C for 2 q. After extraction, the mixture is filtered and the precipitate is washed with an aqetone filter. The precipitate (1.3 kg) is loaded into an extractor with a turbulent mixer, ds is 6.5 liters of water and stirred for i h at 15-25 Then the resulting colloidal system is subjected to drying in a suspended state ar 9O-110 C. Exit powdered target product 65%, phosphopend content 92.5%. Example 2. 2 kg of raw phosphate concentrate from soy is placed in a reactor with a stirrer and a bump stop. Pour 45 liters of acetone, add antioxidant, turn on the stirrer, and extract the njffl 15–25 ° C for 2 seconds. After extraction, the mixture is filtered and the precipitate is washed on the filter with 5 liters of acetone. The precipitate {l, l kg) is again loaded into the reactor with a turbine agitator, 4.4 water is added and stirred at 15-25 G for 1 hour. After hydrophilication, the resulting colloidal system is subjected to drying in a suspended state at 9 O-11 O C. powdered target product 55%; phosphoripid consumption, 89%. Example 3. 2 kg of crude phosphatide concentrate from sunflower will be placed in an extractor with a turbine mixer, pour 4O l of aueiOHa; Anthoxidant is added, the stirrer is turned on and extraction is carried out at 15-25 ° C for 2 hours. After extraction, the mixture is filtered and the precipitate is washed on the filter with 5 liters of acetone. The crude precipitate (l, 3 kg) is immediately loaded into the extractor with a turbine mixer, 4.5 liters of water are added and stirred for 1.5 hours at 15-25 ° C, then the resulting colloidal system is dried in a suspended state at 99- 1 JUS. The yield of the target product is 65%, containing a hedge of phospholipids of 92.5%. Claims A method for producing phospholipids from plant raw materials, including treating phosphatid concentrates with acetone, filtering, is distinguished by the fact that, in order to simplify the process, increase the yield and improve the quality of the target product, the phospholipid precipitate obtained after filtration is treated with water at a weight ratio of phospholystids: water 1: 3.5- - 1: 5.5 at 15-25 ° C, followed by drying in suspension at 90-11 ° C. Sources of agamaforma, taken into account during the examination 1. US patent No. 3031478, cl. 260-403, 1962.
SU762426094A 1976-12-02 1976-12-02 Method of obtaining phospholipids from vegetable raw material SU642316A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU762426094A SU642316A1 (en) 1976-12-02 1976-12-02 Method of obtaining phospholipids from vegetable raw material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU762426094A SU642316A1 (en) 1976-12-02 1976-12-02 Method of obtaining phospholipids from vegetable raw material

Publications (1)

Publication Number Publication Date
SU642316A1 true SU642316A1 (en) 1979-01-15

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU762426094A SU642316A1 (en) 1976-12-02 1976-12-02 Method of obtaining phospholipids from vegetable raw material

Country Status (1)

Country Link
SU (1) SU642316A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4524085A (en) * 1983-11-14 1985-06-18 The Procter & Gamble Company Lecithin containing cooking fats with reduced thermal discoloration
US4528201A (en) * 1983-06-20 1985-07-09 The Procter & Gamble Co. Alkali-treated lecithin in fats
US5145708A (en) * 1989-12-28 1992-09-08 Wm. Wrigley Jr. Company Method of preparing lecithin composition for chewing gum

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4528201A (en) * 1983-06-20 1985-07-09 The Procter & Gamble Co. Alkali-treated lecithin in fats
US4524085A (en) * 1983-11-14 1985-06-18 The Procter & Gamble Company Lecithin containing cooking fats with reduced thermal discoloration
US5145708A (en) * 1989-12-28 1992-09-08 Wm. Wrigley Jr. Company Method of preparing lecithin composition for chewing gum

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