SU568264A1 - Method of obtaining phenolformaldehyde resins of novolak type - Google Patents

Method of obtaining phenolformaldehyde resins of novolak type

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Publication number
SU568264A1
SU568264A1 SU742085046A SU2085046A SU568264A1 SU 568264 A1 SU568264 A1 SU 568264A1 SU 742085046 A SU742085046 A SU 742085046A SU 2085046 A SU2085046 A SU 2085046A SU 568264 A1 SU568264 A1 SU 568264A1
Authority
SU
USSR - Soviet Union
Prior art keywords
obtaining
novolak type
phenolformaldehyde resins
phenolformaldehyde
resins
Prior art date
Application number
SU742085046A
Other languages
Russian (ru)
Inventor
С.Б. Макаров
Ю.А. Лейкин
О.Н. Власовская
А.В. Смирнов
Л.А. Тихонова
Original Assignee
Предприятие П/Я А-7815
Московский ордена Ленина и ордена Трудового Красного Знамени химико-технологический институт им. Д.И.Менделеева
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
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Application filed by Предприятие П/Я А-7815, Московский ордена Ленина и ордена Трудового Красного Знамени химико-технологический институт им. Д.И.Менделеева filed Critical Предприятие П/Я А-7815
Priority to SU742085046A priority Critical patent/SU568264A1/en
Application granted granted Critical
Publication of SU568264A1 publication Critical patent/SU568264A1/en

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  • Phenolic Resins Or Amino Resins (AREA)

Description

дистиллированной водой. Катионит отмывают дистиллированной водой до нейтральной реакции промывных вод, обрабатывают 4%-ным раствором едкого «атра и снова водой. Затем катионит перевод т в Н+-форму 6%-ным раствором сол ной кислоты , отмывают дистиллированной водой до отсутстви  ионов хлора в промывных водах и высушивают при 70°С в течение в-10 ч.distilled water. The cation exchanger is washed with distilled water until neutral wash water, treated with a 4% solution of caustic "atra and again with water. Then the cation exchanger is converted into H + -form with a 6% hydrochloric acid solution, washed with distilled water to the absence of chlorine ions in the wash water and dried at 70 ° C for-10 h.

Статическа  обменна  емкость полученного катионита по 0,1 н. раствору едкого натра 3,1 мГЭкв/г, удельный объем в Н+нформе 8,:1 мл/г, содержание азота и серы 4,5 и 9,5% соответственно.The static exchange capacity of the obtained cation exchanger is 0.1 n. a solution of caustic soda 3.1 mHEq / g, specific volume in H + form 8,: 1 ml / g, nitrogen and sulfur content of 4.5 and 9.5%, respectively.

Пример 2. 25 г сополимера стирола с 2% п-дивинилбензола обрабатывают по примеру 1 с той лишь разницей, что реакционна  смесь содержит 5 г нитрата кали  (0,2 моль на осново-моль сополимера) и процесс провод т При 70°С.Example 2. 25 g of a styrene copolymer with 2% p-divinylbenzene are treated as in Example 1 with the only difference that the reaction mixture contains 5 g of potassium nitrate (0.2 mol based on the mol-copolymer) and the process is carried out at 70 ° C.

Статическа  обменна  емкость полученного Катионита по 0,1 н. раствору едкогоThe static exchange capacity of the obtained Cation exchanger is 0.1 n. caustic solution

иатра Составл ет 4,0 мг-экв/г, удельный объем его в Н+-форме 9,8 мл/г, содержание азота и серы 1,6 и 12,6% соответственно .It is 4.0 mEq / g, its specific volume in the H + form is 9.8 ml / g, the nitrogen and sulfur contents are 1.6 and 12.6%, respectively.

Claims (3)

1.Патент США № 3256250, кл. 260-2.2, 1966.1. US patent number 3256250, class. 260-2.2, 1966. 2.Патент США № 3370021, кл. 260-2.2, 1968.2. US patent number 3370021, cl. 260-2.2, 1968. 3.J. Appl. Chem., 18, 2, 48, 1968.3.J. Appl. Chem., 18, 2, 48, 1968.
SU742085046A 1974-12-18 1974-12-18 Method of obtaining phenolformaldehyde resins of novolak type SU568264A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU742085046A SU568264A1 (en) 1974-12-18 1974-12-18 Method of obtaining phenolformaldehyde resins of novolak type

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU742085046A SU568264A1 (en) 1974-12-18 1974-12-18 Method of obtaining phenolformaldehyde resins of novolak type

Publications (1)

Publication Number Publication Date
SU568264A1 true SU568264A1 (en) 1979-01-30

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU742085046A SU568264A1 (en) 1974-12-18 1974-12-18 Method of obtaining phenolformaldehyde resins of novolak type

Country Status (1)

Country Link
SU (1) SU568264A1 (en)

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