SU474535A1 - The method of obtaining 4-iminothiazolidinone-2 - Google Patents
The method of obtaining 4-iminothiazolidinone-2Info
- Publication number
- SU474535A1 SU474535A1 SU1966745A SU1966745A SU474535A1 SU 474535 A1 SU474535 A1 SU 474535A1 SU 1966745 A SU1966745 A SU 1966745A SU 1966745 A SU1966745 A SU 1966745A SU 474535 A1 SU474535 A1 SU 474535A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- iminothiazolidinone
- obtaining
- thiazolidinedione
- calculated
- found
- Prior art date
Links
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Description
Найдено, %: N 12,80; S 14,40.Found,%: N 12.80; S 14.40.
CioHioOaNsS.CioHioOaNsS.
Вычислено, %: NCalculated,%: N
12,60; S 14,43.12.60; S 14.43.
n p и M e p 3. 4 n p and M e p 3. 4
- n - толилиминотиазолидин2-OH .- n - tolylimothiazolidin2-OH.
Продукт получают из тиазолидин-2,4-диона хлорокиси фосфора и п-толуидина, как описа но в примере I. Бесцветные кристаллы раство римы в спиртах, диоксане, дихлорэтане. Вы ход 74%, т. ол. 236°С из пропанола (с разложением ).The product is obtained from thiazolidine-2,4-dione phosphorus oxychloride and p-toluidine, as described in Example I. Colorless crystals of the solvent in alcohols, dioxane, and dichloroethane. You move 74%, t. Ol. 236 ° C from propanol (with decomposition).
Найдено, %: N 13,87; S 15,8.Found,%: N 13.87; S 15.8.
CioHioONsS.CioHioONsS.
Вычислено, %: N 13,86; S 15,55.Calculated,%: N 13.86; S 15.55.
Предмет изобретени Subject invention
Способ получени 4-иминотиазолидинонов-2 из тиазолидиндиона-2,4, отличающийс тем, что, с целью упрощени процесса, тиазолидиндион-2 ,4 (Подвергают взаимодействию с хлорокисью фосфора с последующей обработкой реакционной массы спиртовым раствором амина.A method for preparing 4-iminothiazolidinone-2 from thiazolidinedione-2.4, characterized in that, in order to simplify the process, thiazolidinedione-2, 4 (Exposed to phosphorus oxychloride followed by treating the reaction mass with an alcoholic solution of amine.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1966745A SU474535A1 (en) | 1973-10-22 | 1973-10-22 | The method of obtaining 4-iminothiazolidinone-2 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU1966745A SU474535A1 (en) | 1973-10-22 | 1973-10-22 | The method of obtaining 4-iminothiazolidinone-2 |
Publications (1)
Publication Number | Publication Date |
---|---|
SU474535A1 true SU474535A1 (en) | 1975-06-25 |
Family
ID=20566681
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU1966745A SU474535A1 (en) | 1973-10-22 | 1973-10-22 | The method of obtaining 4-iminothiazolidinone-2 |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU474535A1 (en) |
-
1973
- 1973-10-22 SU SU1966745A patent/SU474535A1/en active
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