SU403410A1 - METHOD FOR GETTING SAPONIN SUM, - Google Patents
METHOD FOR GETTING SAPONIN SUM,Info
- Publication number
- SU403410A1 SU403410A1 SU1734531A SU1734531A SU403410A1 SU 403410 A1 SU403410 A1 SU 403410A1 SU 1734531 A SU1734531 A SU 1734531A SU 1734531 A SU1734531 A SU 1734531A SU 403410 A1 SU403410 A1 SU 403410A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- sum
- extract
- saponin
- getting
- alcohol
- Prior art date
Links
Landscapes
- Steroid Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Description
ii
Изобрёте ие относитс к медицине, toMiiee к Ьолучёнию лекарственных препаратов.The invention relates to medicine, to Miiee to the acquisition of drugs.
Известен способ Получени су.м.мы сапонинов , обладаюпшх фибринолйтической активностью путем экстракции растительного сырь рода RLISCUS хлороформом, затем спиртом, очистки с последуюодим переосаждение.м из апетона, фильтрацией и высуШпвапием.The known method of obtaining sous.my saponins, having fibrinolysis activity by extracting plant materials of the genus RLISCUS with chloroform, then with alcohol, purification, followed by replanting m from apetone, filtration and discharging.
Однако этот способ имеет сложную технологию производства.However, this method has a complex production technology.
Целью изобретени вл етс упрощение технологического процесса и расширение сырьевой базы.The aim of the invention is to simplify the process and expand the raw material base.
Поставленна цель достигаетс тем, что экстракции подвер-гают корни и корневища Ruscus ponticus, экстракт обрабатывают раствором гидрата окиси аммони , растворитель отгон ют, остаток обрабатывают спиртом и далее процесс ведут известными приемами.The goal is achieved by extracting the roots and rhizomes of Ruscus ponticus, the extract is treated with ammonium hydroxide solution, the solvent is distilled off, the residue is treated with alcohol, and then the process is carried out using known methods.
Пример. Воздущносухие измельченные корни п корневища иглицы понтийской (1,5 кг) предварительно экстрагируют хлороформом в аппарате Сокслета, а затем сапонины извлекают при 80°С (5 лХ4) этанолом. Из экстракта спирт отгон ют, оставшуюс водную жидкость довод т до 5 л и экстрагируют бутанолом (3 лХ4). Объединенные бутанольные экстракты очищают 10-25%-ным гидра2Example. Blown shredded roots and rhizomes of the Pontian's needlefish (1.5 kg) are pre-extracted with chloroform in a Soxhlet apparatus, and then the saponins are extracted at 80 ° C (5 lH4) with ethanol. From the extract, the alcohol is distilled off, the remaining aqueous liquid is brought to 5 liters and extracted with butanol (3 LX4). The combined butanol extracts are purified by 10-25% hydra2
том окиси ам.мони дл удалени фенольМЫ.ч и крас щи. вен1,еств, промывают водой, и растворитель нолностью отгон ют под вакуумом . Полученный остаток 150 г раствор ютammonium monoxide to remove phenolmy. h and dye. The veins are washed with water and the solvent is completely stripped off under vacuum. The resulting residue is 150 g dissolved
в 1500 мл метанола и переосаждают из ацетона 7500 мл.in 1500 ml of methanol and 7500 ml of acetone is precipitated from acetone.
Выделившийс при этом осадок отдел ют от жидкости, промывают ацетоном, высушивают под вакуумом и превращают в порошок.The precipitate thus formed is separated from the liquid, washed with acetone, dried under vacuum and powdered.
Таким образом, получают сумму сапонинов в количестве 7% от вз того растительного сырь .Thus, the sum of saponins in the amount of 7% of bled vegetable raw material is obtained.
Предмет изобретени Subject invention
Способ нолуче1ш суммы сапонинов, обладающей фибринолйтической активиостью путем экстракции растительного сырь рода Rnscus хлороформом, затем спиртом, очистки с последующим переосаждением из ацетона, фильтрацией и высуни1ванием, отличающийс тем, что, с целью унрощени технологическогс процесса и расширени сырьевой базы, экстракции подвергают корпи и корневища Rnscus ponticus. экстракт обрабатывают расгвэром гидрата окиси аммони , растворитель отгон ют , осадок обрабатывают спиртом и далее процесс ведут известными приемами.The method of obtaining the sum of saponins with fibrinolytic activity by extracting plant material of the genus Rnscus with chloroform, then with alcohol, purification followed by reprecipitation from acetone, filtration and drying, characterized in that, in order to improve the technological process and expand the raw material base, extract the body, extract the theme, extract the theme, extract the body, extract the theme, extract and donate, and donate the body to the body. Rnscus ponticus. the extract is treated with an ammonium hydroxide solution, the solvent is distilled off, the residue is treated with alcohol, and then the process is carried out using known methods.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1734531A SU403410A1 (en) | 1972-01-06 | 1972-01-06 | METHOD FOR GETTING SAPONIN SUM, |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1734531A SU403410A1 (en) | 1972-01-06 | 1972-01-06 | METHOD FOR GETTING SAPONIN SUM, |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU403410A1 true SU403410A1 (en) | 1973-10-26 |
Family
ID=20499125
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1734531A SU403410A1 (en) | 1972-01-06 | 1972-01-06 | METHOD FOR GETTING SAPONIN SUM, |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU403410A1 (en) |
-
1972
- 1972-01-06 SU SU1734531A patent/SU403410A1/en active
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