SU372202A1 - - Google Patents

Info

Publication number

SU372202A1

SU372202A1 SU1677696A SU1677696A SU372202A1 SU 372202 A1 SU372202 A1 SU 372202A1 SU 1677696 A SU1677696 A SU 1677696A SU 1677696 A SU1677696 A SU 1677696A SU 372202 A1 SU372202 A1 SU 372202A1

Authority

SU

USSR - Soviet Union

Prior art keywords

monochlorohydrin

methanol

mol

esters

excess

Prior art date

1971-06-29

Links

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• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 11
• 238000000034 method Methods 0.000 claims description 11
• -1 glyceryl chlorohydrin esters Chemical class 0.000 claims description 7
• SSZWWUDQMAHNAQ-UHFFFAOYSA-N 3-chloropropane-1,2-diol Chemical compound OCC(O)CCl SSZWWUDQMAHNAQ-UHFFFAOYSA-N 0.000 claims description 6
• 235000011187 glycerol Nutrition 0.000 claims description 5
• 238000004821 distillation Methods 0.000 claims description 4
• 150000004702 methyl esters Chemical class 0.000 claims description 2
• 229920005862 polyol Polymers 0.000 claims description 2
• 150000003077 polyols Chemical class 0.000 claims description 2
• WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims 1
• 238000002955 isolation Methods 0.000 claims 1
• 239000011541 reaction mixture Substances 0.000 claims 1
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
• ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
• 229910052801 chlorine Inorganic materials 0.000 description 4
• 239000000460 chlorine Substances 0.000 description 4
• 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
• 239000007788 liquid Substances 0.000 description 3
• 239000007795 chemical reaction product Substances 0.000 description 2
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
• AIQDCMRYEJQBHT-UHFFFAOYSA-N (2,2-dimethoxy-3-phenylpropyl)benzene Chemical compound C=1C=CC=CC=1CC(OC)(OC)CC1=CC=CC=C1 AIQDCMRYEJQBHT-UHFFFAOYSA-N 0.000 description 1
• DAJPMKAQEUGECW-UHFFFAOYSA-N 1,4-bis(methoxymethyl)benzene Chemical compound COCC1=CC=C(COC)C=C1 DAJPMKAQEUGECW-UHFFFAOYSA-N 0.000 description 1
• HULQTTBWCGSJCT-UHFFFAOYSA-N 1,5-bis(methoxymethyl)-2,4-dimethylbenzene Chemical compound COCC1=CC(COC)=C(C)C=C1C HULQTTBWCGSJCT-UHFFFAOYSA-N 0.000 description 1
• LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
• 239000004593 Epoxy Substances 0.000 description 1
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
• 150000001500 aryl chlorides Chemical class 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 238000007033 dehydrochlorination reaction Methods 0.000 description 1
• 150000002118 epoxides Chemical class 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 239000012530 fluid Substances 0.000 description 1
• 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• GQKZBCPTCWJTAS-UHFFFAOYSA-N methoxymethylbenzene Chemical compound COCC1=CC=CC=C1 GQKZBCPTCWJTAS-UHFFFAOYSA-N 0.000 description 1
• 229940095674 pellet product Drugs 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 239000007787 solid Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 238000003786 synthesis reaction Methods 0.000 description 1