SU315359A1 - - Google Patents

Info

Publication number

SU315359A1

SU315359A1 SU1224808A SU1224808A SU315359A1 SU 315359 A1 SU315359 A1 SU 315359A1 SU 1224808 A SU1224808 A SU 1224808A SU 1224808 A SU1224808 A SU 1224808A SU 315359 A1 SU315359 A1 SU 315359A1

Authority

SU

USSR - Soviet Union

Prior art keywords

acid

mol

product

solution

water

Prior art date

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• HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
• VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 12
• 239000000047 product Substances 0.000 description 12
• 239000002253 acid Substances 0.000 description 10
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
• FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
• 239000011780 sodium chloride Substances 0.000 description 6
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
• 150000002903 organophosphorus compounds Chemical class 0.000 description 4
• 150000008044 alkali metal hydroxides Chemical class 0.000 description 3
• 150000001875 compounds Chemical class 0.000 description 3
• 238000001704 evaporation Methods 0.000 description 3
• 239000000706 filtrate Substances 0.000 description 3
• MFGCWSYRYXMYKY-UHFFFAOYSA-N methoxymethylphosphonic acid Chemical class COCP(O)(O)=O MFGCWSYRYXMYKY-UHFFFAOYSA-N 0.000 description 3
• 150000003839 salts Chemical class 0.000 description 3
• -1 sodium alkoxides Chemical class 0.000 description 3
• 239000002904 solvent Substances 0.000 description 3
• WEVYAHXRMPXWCK-UHFFFAOYSA-N acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 2
• 125000000217 alkyl group Chemical group 0.000 description 2
• 230000015572 biosynthetic process Effects 0.000 description 2
• UAYHQZXVMFBCIF-UHFFFAOYSA-N bis(chloromethyl)phosphinic acid Chemical class ClCP(=O)(O)CCl UAYHQZXVMFBCIF-UHFFFAOYSA-N 0.000 description 2
• 238000009835 boiling Methods 0.000 description 2
• 125000004432 carbon atoms Chemical group C* 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• 239000000460 chlorine Substances 0.000 description 2
• 229910052801 chlorine Inorganic materials 0.000 description 2
• RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
• RWSOTUBLDIXVET-UHFFFAOYSA-N dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
• 238000005755 formation reaction Methods 0.000 description 2
• 229910052739 hydrogen Inorganic materials 0.000 description 2
• 239000001257 hydrogen Substances 0.000 description 2
• 125000004435 hydrogen atoms Chemical group [H]* 0.000 description 2
• 238000002955 isolation Methods 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• 229910052751 metal Inorganic materials 0.000 description 2
• 239000002184 metal Substances 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
• 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• WYURNTSHIVDZCO-UHFFFAOYSA-N tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
• 238000005406 washing Methods 0.000 description 2
• RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
• VAYGXNSJCAHWJZ-UHFFFAOYSA-N Dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 1
• GQZXNSPRSGFJLY-UHFFFAOYSA-N Hypophosphorous acid Chemical class OP=O GQZXNSPRSGFJLY-UHFFFAOYSA-N 0.000 description 1
• XCAUINMIESBTBL-UHFFFAOYSA-N Lead(II) sulfide Chemical compound [Pb]=S XCAUINMIESBTBL-UHFFFAOYSA-N 0.000 description 1
• YACKEPLHDIMKIO-UHFFFAOYSA-N Methylphosphonic acid Chemical compound CP(O)(O)=O YACKEPLHDIMKIO-UHFFFAOYSA-N 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 125000004849 alkoxymethyl group Chemical group 0.000 description 1
• 230000000875 corresponding Effects 0.000 description 1
• YOTZYFSGUCFUKA-UHFFFAOYSA-N dimethylphosphine Chemical compound CPC YOTZYFSGUCFUKA-UHFFFAOYSA-N 0.000 description 1
• GOJNABIZVJCYFL-UHFFFAOYSA-N dimethylphosphinic acid Chemical class CP(C)(O)=O GOJNABIZVJCYFL-UHFFFAOYSA-N 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 230000000855 fungicidal Effects 0.000 description 1
• 239000000417 fungicide Substances 0.000 description 1
• 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
• 230000000749 insecticidal Effects 0.000 description 1
• 239000002917 insecticide Substances 0.000 description 1
• 230000003993 interaction Effects 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 230000020477 pH reduction Effects 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 229910052708 sodium Inorganic materials 0.000 description 1
• 239000011734 sodium Substances 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 239000006188 syrup Substances 0.000 description 1
• 235000020357 syrup Nutrition 0.000 description 1