SU303825A1 - Device for continuous crystallization purification of organic substances - Google Patents
Device for continuous crystallization purification of organic substancesInfo
- Publication number
- SU303825A1 SU303825A1 SU1369778A SU1369778A SU303825A1 SU 303825 A1 SU303825 A1 SU 303825A1 SU 1369778 A SU1369778 A SU 1369778A SU 1369778 A SU1369778 A SU 1369778A SU 303825 A1 SU303825 A1 SU 303825A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- organic substances
- continuous crystallization
- crystallization purification
- purification
- cone
- Prior art date
Links
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- Detergent Compositions (AREA)
- Cosmetics (AREA)
- Physical Water Treatments (AREA)
Description
Известны устройства пернодаческой крнсгаллизациоиной очистки органических веществ, в которых расплавпепмуто часть отдел ют после установлени равновеси между жидкой и твердой фазами.Devices for the percolation of gallisation purification of organic substances are known, in which the melt-fused portion is separated after establishing an equilibrium between the liquid and solid phases.
С целью непрерывной кристаллизациопной ошстки органических иещестц предагагаемое устройство вынол11е(о в виде обращетюго вершиной вниз конуса со нггунером вьшода расплавлеп юго очищенного продукта.For the purpose of continuous crystallization of organic fossils, the predestined device was taken out (in the form of a reversible apex downward cone with a ngguerometer that melted the south of the purified product.
На чертеже схематически изображено предлагаемое устройство.The drawing schematically shows the proposed device.
Оно СОСГОИ7 из корнуса i, вынолненного в форме конуса, теплообменника 2, охватывающего боковую поверхность корпуса 1, и нпуцоров 3-6.It is a SOSGOI7 from Cornus i, made in the form of a cone, a heat exchanger 2, which covers the lateral surface of the housing 1, and a tool 3-6.
Устройство работает следующим образом.The device works as follows.
В пусковой иериод через нггуцер 3 корпус зат1олн ог охлажденным очище)ным BcaiecTBONi. Тенлообмепник 2 включают на работы холодальника , внос т при необходимосш кристаллическую затравку и кр стал Изук Т, получа конусообразный криста;1.)И1(1;ский CJISITOK. которр-.т имеет новерхиоси крисгаллизин и и ((.In the start-up period through the ngguzer 3, the case is sealed with the cooled BcaiecTBONi cleaner. Tenlome articulum 2 includes the work of a cold box, introducing a crystalline seed when necessary, and cr. Became Izuk T, obtaining a cone-shaped crista; 1.) I1 (1; sky CJISITOK. Who-t has a verhiosy crisgallisin and and ((.
ienj oo6Memnii : иереключают на режим работы иагревагел . Ошщаемое нещестио пропускают тенлообмеи {ик и niTyuep 5 F-copnyca 1. Яоток его направл ют по поверхности криолшпизанки слитка, где он н крис1ал;и1зуетс . Поток циркулирующего вещества подхиаплваот примеси, вытесн емые в процессе кристаллиза1и1и, и через пгтуиер 4 отводит их от поверхности кристаллизации слигка. Теплообменник 2 нагревает боковую поверхность Ш1ав.пен11 ienj oo6Memnii: they switch to iagrevagel mode of operation. The cranky missed tenlomes {ik and niTyuep 5 F-copnyca 1). Its hole is directed along the surface of the cryol sponge of the ingot, where it is n crystal; The flow of the circulating substance under the impurity displaced during the crystallization process, and through the Ptuiuer 4 separates them from the surface of the crystallization of light. The heat exchanger 2 heats the side surface
слитка до телшературы. при которой скорость отвода очище {1 ого распларлениого aeniecTna равна скорости jXiCTa кристаллической фазы.ingot to telesheratura. at which the rate of removal is cleared {1 th melting aeniecTna equal to the speed jXiCTa of the crystalline phase.
По мере подтаивани поверхности плавлени слнлок под л.ейстпием собствопюго веса меллениоAs the melting surface is melted, the slnok under the l.
оссдаег, пыгесн и з зазора между слитком и cicnKoii oiHiiiieiiiiuc paciijsaBMejHioe вещество, которос через штуцер 6 са.мотском стекает в сборник.Ossdagh, pygesn and z the gap between the ingot and cicnKoii oiHiiiieiiiiuc paciijsaBMejHioe substance, which through fitting 6 ca. Motsky flows into the collection.
Одновременпо с отводом очищенного раснлавлс1нк1 (о BeiHecTna вс система непрерь вн | пополн етс исходным очищаемым )eн tcтнoSimultaneously with the removal of the purified moltenite 1 (about the BeiHecTna, the entire system is uninterrupted | is replenished with the original cleaned)
Ф о р м у л а и 3 о б р е т е н и Устройство дл непрерывной кристаллизчпионloii очистки opt пиических вепичШ. в том числе нереох.и1ж;1пи111Л с , Ol |iaci .i примесей.Fo rumula and 3 obre n e Device for continuous crystallization and purification of opt pytic veins. including irreducible; 1pi111 with, Ol | iaci .i impurities.
о I л ч а н) tu е е с тем, что оно выполнено в виде обращенного вершиной вниз неподвижною конуса, Jaiiojineiiupro очищенным вешестном. бокова поверхность которого снабнсена теплообмегт ком, а основание конусообразного слитка очищенного вещесгйа вл етс поверхностью кцисга.чпизаиин, причем аттупер дл вывода очищенного вещества расположен в вершине к-онуса, а штуцера нвод;| очи|т(аемото В14чесгва и вывода очи цаемого вещества , обпгаишнного примес ми, - у ею основани About I h a n) tu e e so that it is made in the form of a downward-facing fixed cone, Jaiiojineiiupro cleared by a spring. the lateral surface of which is provided with a heat exchanger, and the base of the cone-shaped ingot of the purified material is the surface of the cycouschpizayin, with an atuper for outputting the purified substance located at the top of the onus, and the union nvod; | cleaners (t amoto b14 chesgva and the removal of the substance to be purified, contaminated with impurities,
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1369778A SU303825A1 (en) | 1969-10-06 | 1969-10-06 | Device for continuous crystallization purification of organic substances |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1369778A SU303825A1 (en) | 1969-10-06 | 1969-10-06 | Device for continuous crystallization purification of organic substances |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU303825A1 true SU303825A1 (en) | 1976-09-25 |
Family
ID=20447789
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1369778A SU303825A1 (en) | 1969-10-06 | 1969-10-06 | Device for continuous crystallization purification of organic substances |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU303825A1 (en) |
-
1969
- 1969-10-06 SU SU1369778A patent/SU303825A1/en active
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