SU280481A1 - - Google Patents

Info

Publication number

SU280481A1

SU280481A1 SU1277689A SU1277689A SU280481A1 SU 280481 A1 SU280481 A1 SU 280481A1 SU 1277689 A SU1277689 A SU 1277689A SU 1277689 A SU1277689 A SU 1277689A SU 280481 A1 SU280481 A1 SU 280481A1

Authority

SU

USSR - Soviet Union

Prior art keywords

bitartrate

raw materials

sulfuric acid

alkaloids

filtered

Prior art date

Links

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• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
• FEWJPZIEWOKRBE-UHFFFAOYSA-M 3-carboxy-2,3-dihydroxypropanoate Chemical compound OC(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-M 0.000 description 5
• 229930013930 alkaloid Natural products 0.000 description 5
• 235000019441 ethanol Nutrition 0.000 description 5
• 239000002994 raw material Substances 0.000 description 5
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
• 239000000284 extract Substances 0.000 description 4
• 238000000034 method Methods 0.000 description 4
• 239000000243 solution Substances 0.000 description 3
• SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 2
• 241000239290 Araneae Species 0.000 description 2
• HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
• 241000196324 Embryophyta Species 0.000 description 2
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
• 229910021529 ammonia Inorganic materials 0.000 description 2
• 238000009835 boiling Methods 0.000 description 2
• 239000002244 precipitate Substances 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• BTHCJHQOYFUIMG-REYNEDSXSA-N Platyphylline Chemical compound O1C(=O)C(=C/C)\C[C@@H](C)[C@@](C)(O)C(=O)OC[C@H]2CCN3[C@H]2[C@H]1CC3 BTHCJHQOYFUIMG-REYNEDSXSA-N 0.000 description 1
• 241000780602 Senecio Species 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
• FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• 150000003797 alkaloid derivatives Chemical class 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 239000002026 chloroform extract Substances 0.000 description 1
• 238000000605 extraction Methods 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• BTHCJHQOYFUIMG-UHFFFAOYSA-N platyphylline Natural products O1C(=O)C(=CC)CC(C)C(C)(O)C(=O)OCC2CCN3C2C1CC3 BTHCJHQOYFUIMG-UHFFFAOYSA-N 0.000 description 1
• AVLNKVCJJSEPHO-DJTRMNNZSA-N platyphylline, tartrate Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O.O1C(=O)C(=C/C)\C[C@@H](C)[C@@](C)(O)C(=O)OC[C@H]2CCN3[C@H]2[C@H]1CC3 AVLNKVCJJSEPHO-DJTRMNNZSA-N 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 235000002906 tartaric acid Nutrition 0.000 description 1
• 239000011975 tartaric acid Substances 0.000 description 1
• 239000011787 zinc oxide Substances 0.000 description 1