SU164279A1 - - Google Patents
Info
- Publication number
- SU164279A1 SU164279A1 SU865665A SU865665A SU164279A1 SU 164279 A1 SU164279 A1 SU 164279A1 SU 865665 A SU865665 A SU 865665A SU 865665 A SU865665 A SU 865665A SU 164279 A1 SU164279 A1 SU 164279A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- heated
- hydrocarbon residue
- triphenylphenacylphosphonium
- dry pyridine
- chloride
- Prior art date
Links
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 4
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 4
- OWTCGJRBQMOICX-UHFFFAOYSA-M phenacyl(triphenyl)phosphanium;chloride Chemical compound [Cl-].C=1C=CC=CC=1C(=O)C[P+](C=1C=CC=CC=1)(C=1C=CC=CC=1)C1=CC=CC=C1 OWTCGJRBQMOICX-UHFFFAOYSA-M 0.000 claims description 3
- 150000001299 aldehydes Chemical class 0.000 claims description 2
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 150000002430 hydrocarbons Chemical group 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Chemical compound C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 description 2
- GFCQYNBXLQEBEJ-UHFFFAOYSA-N 2-(diethoxymethyl)-1,1-diethoxybutane Chemical compound CCOC(OCC)C(CC)C(OCC)OCC GFCQYNBXLQEBEJ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000001235 sensitizing effect Effects 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU164279A1 true SU164279A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Cairns et al. | Cyanocarbon chemistry. I. Preparation and reactions of tetracyanoethylene | |
| JP2564462B2 (ja) | 新規アリールアルキル（チオ）アミド化合物 | |
| Silverstein et al. | 2-Pyrrolealdehyde, 3-hydroxymethylindole and 2-hydroxymethylpyrrole | |
| Skell et al. | Synthesis and Properties of Alkylpyrroles | |
| Young et al. | The Synthesis of the Isomeric 2-BUTENES1 | |
| SU164279A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| Franz et al. | The reactions of sulfonamides with oxalyl chloride | |
| Fuson et al. | Vinyl Alcohols. XVIII. 1 Increased Hindrance | |
| Hennion et al. | Reactions of Acetylenic Primary Amines1 | |
| Nenitzescu et al. | The polymerization of 1, 2-dihydronaphthalene and the dehydrogenating condensation of 1, 2, 3, 4-tetrahydronaphthalene | |
| FUSON et al. | 1, 4-Addition of the Grignard Reagent to Acetylenic Ketones | |
| Abaee et al. | Facile one-pot synthesis of novel dicyanoanilines fused to dithiane ring via a pseudo-four-component reaction | |
| Bergmann et al. | Investigations in the Acetylene Series. I. The Reactions of 3-Methyl-1-butyn-3-ol with Phosphorus Trichloride and of 3-Methyl-3-buten-1-yne with Hydrochloric Acid | |
| CH630054A5 (it) | Procedimento per la preparazione dell'acido m.benzoil-idratropico. | |
| US676862A (en) | Aromatic amido-aldehydes and process of making same. | |
| SU348569A1 (ru) | ВСГСОЮЗНАЯ Iг •--•<-;.л •• "Г^-'Т-'У^Я! (.' i^il.lty i ^..--1... •'• иЛП!ьиьлио :::КА { | |
| SU218151A1 (ru) | СПОСОБ ПОЛУЧЕНИЯ а.,а-ДИХЛОР-|5,у- И у,у-ДИФЕНИЛ- у-БУТИРОЛАКТОНОВ | |
| Mason | The Toxic Principles of Poison Ivy. II. Preparation and Properties of the Diphenylmethylene Ethers of Catechols1 | |
| US714931A (en) | Hydrobenzaldehyde and process of making same. | |
| Ulrich et al. | 4-Isocyanatophthalic anhydride. Novel difunctional monomer | |
| CH512440A (fr) | Procédé de préparation d'un mélange de composés aliphatiques w-carboxylés | |
| US2569114A (en) | Their hydkolytic products | |
| SU183731A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| SU242902A1 (ru) | Способ получения 2-метил-4,5-тиофено- | |
| SU348571A1 (ru) | СПОСОБ ПОЛУЧЬНИЯ ;j АРОИЛ-5-АРИЛИЗОКСЛЗОЛОВ |