SU1590472A1 - Uneritted glaze - Google Patents

Uneritted glaze Download PDF

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Publication number
SU1590472A1
SU1590472A1 SU874328842A SU4328842A SU1590472A1 SU 1590472 A1 SU1590472 A1 SU 1590472A1 SU 874328842 A SU874328842 A SU 874328842A SU 4328842 A SU4328842 A SU 4328842A SU 1590472 A1 SU1590472 A1 SU 1590472A1
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SU
USSR - Soviet Union
Prior art keywords
glaze
cao
mgo
suspensions
variation
Prior art date
Application number
SU874328842A
Other languages
Russian (ru)
Inventor
Александр Александрович Пащенко
Валентин Анатольевич Свидерский
Михаил Юрьевич Чоп
Павел Сергеевич Борсук
Александр Степанович Волков
Людмила Юрьевна Чоп
Original Assignee
Киевский Политехнический Институт Им.50-Летия Великой Октябрьской Социалистической Революции
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Priority to SU874328842A priority Critical patent/SU1590472A1/en
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Publication of SU1590472A1 publication Critical patent/SU1590472A1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Abstract

Изобретение относитс  к составам глазурей, предназначенным дл  изготовлени  отделочных строительных материалов с температурой обжига до 1000°С. Целью изобретени   вл етс  повышение морозостойкости и микротвердости и расширение интервала варьировани  коэффициента линейного термического расширени . Дл  этого глазурь содержит, мас.%: SIO 2 40,54-51,07The invention relates to coating compositions intended for the manufacture of finishing building materials with a firing temperature of up to 1000 ° C. The aim of the invention is to increase the frost resistance and microhardness and to extend the range of variation of the linear thermal expansion coefficient. For this glaze contains, wt%: SIO 2 40.54-51.07

AL 2О 3 7,76-10,76AL 2O 3 7.76-10.76

В 2О 3 7,69-9,10B 2O 3 7.69-9.10

Fe 2О 3 3,44-3,85Fe 2 3 3,44-3,85

СаО 21,91-24,12CaO 21.91-24.12

MGO 0,83-3,63MGO 0.83-3.63

ZNO 0,18-1,45ZNO 0.18-1.45

Na 2О 0,42-0,76Na2O 0.42-0.76

К 2О 0,30-0,56K 2 0.30-0.56

TIO 2 0,02-0,80TIO 2 0.02-0.80

FeO 1,43-7,42FeO 1.43-7.42

РвО 0,08-0,69PvO 0.08-0.69

SO 3 0,20-1,64. Морозостойкость глазури составл ет 95-100 циклов, коэффициент линейного термического расширени  (3,95-7,63) .10 -6 град -1. 2 табл.SO 3 0.20-1.64. The frost resistance of the glaze is 95-100 cycles, the coefficient of linear thermal expansion (3.95-7.63) .10 -6 degrees -1. 2 tab.

Description

Изобретение относитс  к составам глазурей, предназначенным дл  изготовлени  отделочных строительных материалов , и может быть использовано в производстве керамических плиток различного назначени , а также других керамических изделий с температурой обжига до .The invention relates to glaze compositions for the manufacture of finishing building materials, and can be used in the manufacture of ceramic tiles for various purposes, as well as other ceramic products with a firing temperature up to.

Целью изобретени   вл етс  повышение морозостойкости, микротвердости и расширение интервала варьировани  коэффициента линейного термического расширени .The aim of the invention is to increase the frost resistance, microhardness and the expansion of the range of variation of the coefficient of linear thermal expansion.

Конкретные составы предлагаемой глазури приведены в табл.1, а свойства их - в табл.2.Specific compositions of the proposed glaze are given in table 1, and their properties in table 2.

Глазурь имеет следующий шихтовой состав, мас.%: олов нно-свинцовыйThe glaze has the following charge composition, wt.%: Tin tin-lead

шлак 4-33; глина 18-38; датолитовый концентрат 49-58.slag 4-33; clay 18-38; datolite concentrate 49-58.

Олов нно-свинцовый шлак - сильно остеклованное вещество коричневого цвета, представл ет собой техногенный отход, образуемый при отражательной плавке олов нно-свинцового концентрата и имеет следующий химический состав , мас.%: SiOj 23,04; 7,37; Ti07 0,44,- FeO 21,00; 5,40; CaO 19,15; MgO 10,20; 1,81; 0,13; SOa 4,98; ZnO 4,38; PbO 2,10.Tin-lead slag is a highly vitrified brown-colored substance, is a man-made waste formed in the reflective melting of tin-lead concentrate and has the following chemical composition, wt.%: SiOj 23.04; 7.37; Ti07 0.44, - FeO 21.00; 5.40; CaO 19.15; MgO 10.20; 1.81; 0.13; SOa 4.98; ZnO 4.38; PbO 2,10.

Датолитовый концентрат - борсодер- жащий мелкодисперсньш порошок белого цвета следующего химического состава, мас.%: ВгОа 15,5; СаО 35,75; SiOi 42,5; 2,5; FeO 1,0; 1,7; MgO 0,3; CO 2.5,25; KiO 5,5. .Datolite concentrate - boron-containing fine white powder of the following chemical composition, wt.%: BrOa 15.5; CaO 35.75; SiOi 42.5; 2.5; FeO 1.0; 1.7; MgO 0.3; CO 2.5.25; KiO 5.5. .

СЛSL

COCO

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4four

4j4j

toto

1590А721590A72

В качестве пластичного компонента используют каолинит - гидрослюдистую глину ДНПК-1 следующего химичзского состава, мас.%: Si02 62,0; 23,0 FesOs .1; СаО 0,38| MgO 0,52; NajO 0,85j KjO 1,25, органические примеси 0,34; п.п.п. 5,9.As a plastic component, kaolinite is used - hydromica clay DNPK-1 of the following chemical composition, wt%: SiO2 62.0; 23.0 FesOs .1; Cao 0.38 | MgO 0.52; NajO 0.85 j KjO 1.25, organic impurities 0.34; ppt 5.9.

Claims (1)

Глазурные суспензии готов т традиционным способом. Помол компонентов осуществл ют в шаровой мельнице до остатка на сите № ООбЗ 0,2%. Плотность готовых суспензий составл ет 1,47-1,62 г/см . Полученные смеси нанос т на высушенные сырые плитки мето дом пульверизации. Исследуемые образцы обжигают одновременно в промышленной роликовой печи в течение 60 мин при максимальной температуре . Формула изобретен и   Glaze suspensions are prepared in the conventional manner. The grinding of the components is carried out in a ball mill to a residue on a sieve of no. SSB 0.2%. The density of the finished suspensions is 1.47-1.62 g / cm. The resulting mixtures are applied to the dried, raw tiles by pulverization. The test samples are burned simultaneously in an industrial roller furnace for 60 minutes at maximum temperature. Formula invented and Нефриттованна  глазурь, включающа  Si02, АНОа. , FeaOg, СаО, MgO,Jade glaze, including Si02, ANOa. , FeaOg, CaO, MgO, 4four , отличающа - то, с целью повышении моро , микротпердоетт и расшивала варьировани  коэффийного термического расшидополнительно содержит PbO, SO при следующем компонентов, ыасД:, characterized in that, in order to increase moro, micropertoetes and bruising the variation of the thermal coefficient, it additionally contains PbO, SO for the following components, as follows: f f г- t f 4 ff f g- t f 4 f 40,54-51,07 7,76-10,76 7,69-9,10 3,44-3,8540.54-51.07 7.76-10.76 7.69-9.10 3.44-3.85 21.91-24,12 0,83-3,63 0,18-1,45 0,42-0,76 0,30-0,56 0,02-0,8.0 1.43-7,42 О ,08-0,69 0,20-1,6421.91-24.12 0.83-3.63 0.18-1.45 0.42-0.76 0.30-0.56 0.02-0.8.0 1.43-7.42 O, 08-0 , 69 0.20-1.64 СвойстваProperties 7„637 63 1000 1000 1000 С 250 350 3001000 1000 1000 С 250 350 300 ,95 J, 95 J 100100 100100 3,95 5,75 3.95 5.75 Т a б л и ц a 1T a b l and c a 1 ТаблицаTable Данные глазури составаData glaze composition --л Г- Г- l rg ИзвестныйFamous 3,95 5,75 4,3-4,93.95 5.75 4.3-4.9 1000 1000 350 3001000 1000 350 300 JJ 100100 100100 1000 2501000 250 7676 851 932851 932 37,88 31,17 34,8237.88 31.17 34.82 46 38 51 0,018 0,011 0,015 87646 38 51 0,018 0,011 0,015 876 50 0,02050 0.020 812 88-98812 88-98
SU874328842A 1987-11-16 1987-11-16 Uneritted glaze SU1590472A1 (en)

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Application Number Priority Date Filing Date Title
SU874328842A SU1590472A1 (en) 1987-11-16 1987-11-16 Uneritted glaze

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Application Number Priority Date Filing Date Title
SU874328842A SU1590472A1 (en) 1987-11-16 1987-11-16 Uneritted glaze

Publications (1)

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SU1590472A1 true SU1590472A1 (en) 1990-09-07

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010126581A1 (en) * 2009-05-01 2010-11-04 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8500933B2 (en) 2007-12-14 2013-08-06 Guardian Industries Corp. Localized heating of edge seals for a vacuum insulating glass unit, and/or unitized oven for accomplishing the same
US8506738B2 (en) 2007-12-17 2013-08-13 Guardian Industries Corp. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US8733128B2 (en) 2011-02-22 2014-05-27 Guardian Industries Corp. Materials and/or method of making vacuum insulating glass units including the same
US8802203B2 (en) 2011-02-22 2014-08-12 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US9290408B2 (en) 2011-02-22 2016-03-22 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US9309146B2 (en) 2011-02-22 2016-04-12 Guardian Industries Corp. Vanadium-based frit materials, binders, and/or solvents and methods of making the same
US9359247B2 (en) 2011-02-22 2016-06-07 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9458052B2 (en) 2011-02-22 2016-10-04 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9593527B2 (en) 2014-02-04 2017-03-14 Guardian Industries Corp. Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same
US9822580B2 (en) 2011-02-22 2017-11-21 Guardian Glass, LLC Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same
US9988302B2 (en) 2014-02-04 2018-06-05 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Авторское свидетельство СССР № 1263683, кл. С 04 В 41/86, 1985. : Авторское свидетельство СССР № 1270147, кл. С 04 В 41/86, 1984. *

Cited By (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8500933B2 (en) 2007-12-14 2013-08-06 Guardian Industries Corp. Localized heating of edge seals for a vacuum insulating glass unit, and/or unitized oven for accomplishing the same
US8506738B2 (en) 2007-12-17 2013-08-13 Guardian Industries Corp. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US10717668B2 (en) 2007-12-17 2020-07-21 Guardian Glass, Llc. Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
US10294140B2 (en) 2007-12-17 2019-05-21 Guardian Glass, LLC Localized heating via an infrared heat source array of edge seals for a vacuum insulating glass unit, and/or unitized oven with infrared heat source array for accomplishing the same
WO2010126581A1 (en) * 2009-05-01 2010-11-04 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8227055B2 (en) 2009-05-01 2012-07-24 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8590343B2 (en) 2009-05-01 2013-11-26 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US8763427B2 (en) 2009-05-01 2014-07-01 Guardian Industries Corp. Vacuum insulating glass unit including infrared meltable glass frit, and/or method of making the same
US9822580B2 (en) 2011-02-22 2017-11-21 Guardian Glass, LLC Localized heating techniques incorporating tunable infrared element(s) for vacuum insulating glass units, and/or apparatuses for same
US10196299B2 (en) 2011-02-22 2019-02-05 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US9359247B2 (en) 2011-02-22 2016-06-07 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9458052B2 (en) 2011-02-22 2016-10-04 Guardian Industries Corp. Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US11028009B2 (en) 2011-02-22 2021-06-08 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9776910B2 (en) 2011-02-22 2017-10-03 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US9290408B2 (en) 2011-02-22 2016-03-22 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US11014847B2 (en) 2011-02-22 2021-05-25 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US10087676B2 (en) 2011-02-22 2018-10-02 Guardian Glass, LLC Vanadium-based frit materials, and/or methods of making the same
US10107028B2 (en) 2011-02-22 2018-10-23 Guardian Glass, LLC Method of making vacuum insulated glass (VIG) window unit
US10125045B2 (en) 2011-02-22 2018-11-13 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US9309146B2 (en) 2011-02-22 2016-04-12 Guardian Industries Corp. Vanadium-based frit materials, binders, and/or solvents and methods of making the same
US8802203B2 (en) 2011-02-22 2014-08-12 Guardian Industries Corp. Vanadium-based frit materials, and/or methods of making the same
US10329187B2 (en) 2011-02-22 2019-06-25 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US10858880B2 (en) 2011-02-22 2020-12-08 Guardian Glass, LLC Vanadium-based frit materials, binders, and/or solvents and/or methods of making the same
US10752535B2 (en) 2011-02-22 2020-08-25 Guardian Glass, LLC Coefficient of thermal expansion filler for vanadium-based frit materials and/or methods of making and/or using the same
US8733128B2 (en) 2011-02-22 2014-05-27 Guardian Industries Corp. Materials and/or method of making vacuum insulating glass units including the same
US10465433B2 (en) 2014-02-04 2019-11-05 Guardian Glass, Llc. Vacuum insulating glass (VIG) unit with lead-free dual-frit seals and/or methods of making the same
US10421684B2 (en) 2014-02-04 2019-09-24 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods
US9988302B2 (en) 2014-02-04 2018-06-05 Guardian Glass, LLC Frits for use in vacuum insulating glass (VIG) units, and/or associated methods
US9593527B2 (en) 2014-02-04 2017-03-14 Guardian Industries Corp. Vacuum insulating glass (VIG) unit with lead-free dual-frit edge seals and/or methods of making the same

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