SG2014012637A - Process for preparation of methacrylic acid and methacrylic acid ester - Google Patents

Process for preparation of methacrylic acid and methacrylic acid ester

Info

Publication number
SG2014012637A
SG2014012637A SG2014012637A SG2014012637A SG2014012637A SG 2014012637 A SG2014012637 A SG 2014012637A SG 2014012637 A SG2014012637 A SG 2014012637A SG 2014012637 A SG2014012637 A SG 2014012637A SG 2014012637 A SG2014012637 A SG 2014012637A
Authority
SG
Singapore
Prior art keywords
methacrylic acid
preparation
acid ester
ester
methacrylic
Prior art date
Application number
SG2014012637A
Inventor
Jerald A Jones
Torsten Balduf
Henning Schaefer
Original Assignee
Evonik Roehm Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm Gmbh filed Critical Evonik Roehm Gmbh
Publication of SG2014012637A publication Critical patent/SG2014012637A/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0013Crystallisation cooling by heat exchange by indirect heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/004Fractional crystallisation; Fractionating or rectifying columns
    • B01D9/0045Washing of crystals, e.g. in wash columns
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/58Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
SG2014012637A 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid ester SG2014012637A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2011/079764 WO2013037131A1 (en) 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid ester

Publications (1)

Publication Number Publication Date
SG2014012637A true SG2014012637A (en) 2014-06-27

Family

ID=47882550

Family Applications (1)

Application Number Title Priority Date Filing Date
SG2014012637A SG2014012637A (en) 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid ester

Country Status (8)

Country Link
JP (1) JP6092221B2 (en)
KR (1) KR20140060529A (en)
CN (1) CN103796982B (en)
MY (1) MY165642A (en)
SA (1) SA112330847B1 (en)
SG (1) SG2014012637A (en)
TW (1) TWI535696B (en)
WO (1) WO2013037131A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6008969B2 (en) * 2011-09-16 2016-10-19 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツングEvonik Roehm GmbH Method for producing methacrylic acid and methacrylic acid ester
EP3049385B1 (en) * 2013-09-26 2018-01-03 Evonik Röhm GmbH Process for producing methyl methacrylate
KR20220125361A (en) 2020-02-26 2022-09-14 미쯔비시 케미컬 주식회사 A method for separating a crystal containing water, a method for producing methacrylic acid, and a method for producing a methacrylic acid ester

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS54115318A (en) * 1978-02-28 1979-09-07 Sumitomo Chem Co Ltd Recovery of methacrylic acid
JPS5692831A (en) * 1979-12-27 1981-07-27 Sumitomo Chem Co Ltd Recovering method of by-product acetic acid in preparation of methacrylic acid
JPS57144237A (en) * 1981-03-04 1982-09-06 Japan Synthetic Rubber Co Ltd Preparation of methacrylic acid
JPH03279344A (en) * 1990-03-27 1991-12-10 Tosoh Corp Method for reducing acetic acid concentration in acetic acid waste water
DE19709392A1 (en) * 1997-03-07 1998-09-10 Basf Ag Process for the extraction of (meth) acrylic acid
BR0012007A (en) * 1999-06-29 2002-03-12 Shell International Res Mij B Process for the treatment of a waste water supply containing organic contaminants
JP2002128728A (en) * 2000-10-19 2002-05-09 Mitsubishi Rayon Co Ltd Method for purifying methacrylic acid
DE10242746B4 (en) * 2002-09-13 2010-07-01 Evonik Degussa Gmbh Washing device, a process for cleaning a laundry and the use of the washing device
SI1995231T1 (en) * 2007-05-25 2014-03-31 Evonik Roehm Gmbh Process for preparation of methyl methacrylate using recycled methanol
EP2085376B1 (en) * 2008-01-30 2012-09-05 Evonik Röhm GmbH Process for preparation of high purity methacrylic acid
JP6008969B2 (en) * 2011-09-16 2016-10-19 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツングEvonik Roehm GmbH Method for producing methacrylic acid and methacrylic acid ester

Also Published As

Publication number Publication date
MY165642A (en) 2018-04-18
JP2014528934A (en) 2014-10-30
TWI535696B (en) 2016-06-01
CN103796982A (en) 2014-05-14
JP6092221B2 (en) 2017-03-08
TW201326115A (en) 2013-07-01
SA112330847B1 (en) 2015-08-16
CN103796982B (en) 2015-10-14
KR20140060529A (en) 2014-05-20
WO2013037131A1 (en) 2013-03-21

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