SG2014012587A - Process for preparation of methacrylic acid and methacrylic acid esters - Google Patents

Process for preparation of methacrylic acid and methacrylic acid esters

Info

Publication number
SG2014012587A
SG2014012587A SG2014012587A SG2014012587A SG2014012587A SG 2014012587 A SG2014012587 A SG 2014012587A SG 2014012587 A SG2014012587 A SG 2014012587A SG 2014012587 A SG2014012587 A SG 2014012587A SG 2014012587 A SG2014012587 A SG 2014012587A
Authority
SG
Singapore
Prior art keywords
methacrylic acid
preparation
acid esters
esters
methacrylic
Prior art date
Application number
SG2014012587A
Inventor
Henning Schaefer
Torsten Balduf
Original Assignee
Evonik Roehm Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm Gmbh filed Critical Evonik Roehm Gmbh
Publication of SG2014012587A publication Critical patent/SG2014012587A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0013Crystallisation cooling by heat exchange by indirect heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0036Crystallisation on to a bed of product crystals; Seeding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/004Fractional crystallisation; Fractionating or rectifying columns
    • B01D9/0045Washing of crystals, e.g. in wash columns
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/10Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/58Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
SG2014012587A 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid esters SG2014012587A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2011/079774 WO2013037134A1 (en) 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid esters

Publications (1)

Publication Number Publication Date
SG2014012587A true SG2014012587A (en) 2014-06-27

Family

ID=47882553

Family Applications (1)

Application Number Title Priority Date Filing Date
SG2014012587A SG2014012587A (en) 2011-09-16 2011-09-16 Process for preparation of methacrylic acid and methacrylic acid esters

Country Status (8)

Country Link
JP (1) JP6008969B2 (en)
KR (1) KR101877597B1 (en)
CN (2) CN108373409A (en)
MY (1) MY161504A (en)
SA (1) SA112330845B1 (en)
SG (1) SG2014012587A (en)
TW (1) TWI627161B (en)
WO (1) WO2013037134A1 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG2014012561A (en) * 2011-09-16 2014-09-26 Evonik Roehm Gmbh Process for preparation of methacrylic acid and methacrylic acid esters
JP6092221B2 (en) * 2011-09-16 2017-03-08 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツングEvonik Roehm GmbH Method for producing methacrylic acid and methacrylic acid ester
KR101628287B1 (en) * 2013-07-22 2016-06-08 주식회사 엘지화학 Process for continuous recovering (meth)acrylic acid and apparatus for the process
WO2015012551A1 (en) * 2013-07-22 2015-01-29 주식회사 엘지화학 Method and apparatus for continuously recovering (meth)acrylic acid
US9718756B2 (en) 2013-07-23 2017-08-01 Lg Chem, Ltd. Method for continuously recovering (meth)acrylic acid and apparatus for the method
KR101601938B1 (en) * 2013-08-30 2016-03-09 주식회사 엘지화학 Process for continuous recovering (meth)acrylic acid and apparatus for the process
WO2024049105A1 (en) * 2022-08-30 2024-03-07 주식회사 엘지화학 Method for preparing high-purity (meth)acrylic acid

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5148614A (en) * 1974-10-22 1976-04-26 Japan Synthetic Rubber Co Ltd METAKURIRUSANNOBUNRIKAISHUHO
JPS54115318A (en) * 1978-02-28 1979-09-07 Sumitomo Chem Co Ltd Recovery of methacrylic acid
JPS54119412A (en) * 1978-03-06 1979-09-17 Mitsubishi Chem Ind Ltd Purification of methacrylic acid
JPH03279344A (en) * 1990-03-27 1991-12-10 Tosoh Corp Method for reducing acetic acid concentration in acetic acid waste water
DE19709392A1 (en) * 1997-03-07 1998-09-10 Basf Ag Process for the extraction of (meth) acrylic acid
JP2002128728A (en) * 2000-10-19 2002-05-09 Mitsubishi Rayon Co Ltd Method for purifying methacrylic acid
JP2002193875A (en) * 2000-12-27 2002-07-10 Mitsubishi Rayon Co Ltd Method for recovering methacrylic acid
DE10242746B4 (en) * 2002-09-13 2010-07-01 Evonik Degussa Gmbh Washing device, a process for cleaning a laundry and the use of the washing device
SI1995231T1 (en) * 2007-05-25 2014-03-31 Evonik Roehm Gmbh Process for preparation of methyl methacrylate using recycled methanol
EP2085376B1 (en) * 2008-01-30 2012-09-05 Evonik Röhm GmbH Process for preparation of high purity methacrylic acid
SG2014012561A (en) * 2011-09-16 2014-09-26 Evonik Roehm Gmbh Process for preparation of methacrylic acid and methacrylic acid esters
JP6092221B2 (en) * 2011-09-16 2017-03-08 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツングEvonik Roehm GmbH Method for producing methacrylic acid and methacrylic acid ester

Also Published As

Publication number Publication date
MY161504A (en) 2017-04-14
JP6008969B2 (en) 2016-10-19
WO2013037134A1 (en) 2013-03-21
TWI627161B (en) 2018-06-21
SA112330845B1 (en) 2015-07-07
CN108373409A (en) 2018-08-07
CN103827071A (en) 2014-05-28
JP2014528935A (en) 2014-10-30
KR20140060528A (en) 2014-05-20
TW201329035A (en) 2013-07-16
KR101877597B1 (en) 2018-07-12

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