SG11201807304UA - Benzoxazine based copolymer aerogels - Google Patents

Benzoxazine based copolymer aerogels

Info

Publication number
SG11201807304UA
SG11201807304UA SG11201807304UA SG11201807304UA SG11201807304UA SG 11201807304U A SG11201807304U A SG 11201807304UA SG 11201807304U A SG11201807304U A SG 11201807304UA SG 11201807304U A SG11201807304U A SG 11201807304UA SG 11201807304U A SG11201807304U A SG 11201807304UA
Authority
SG
Singapore
Prior art keywords
international
barcelona
based copolymer
benzoxazine
diisseldorf
Prior art date
Application number
SG11201807304UA
Inventor
Cano Elisabet Torres
Fouad Salhi
Ruiz Camilo Zuniga
Sanglas Joaquim Torres
Fernandez Maria Vega
Asta Sakalyte
Original Assignee
Henkel Ag & Co Kgaa
Henkel IP & Holding GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel Ag & Co Kgaa, Henkel IP & Holding GmbH filed Critical Henkel Ag & Co Kgaa
Publication of SG11201807304UA publication Critical patent/SG11201807304UA/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • C08J9/286Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum the liquid phase being a solvent for the monomers but not for the resulting macromolecular composition, i.e. macroporous or macroreticular polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/02Polyamines
    • C08G73/0233Polyamines derived from (poly)oxazolines, (poly)oxazines or having pendant acyl groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L79/00Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
    • C08L79/02Polyamines
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K11/00Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/16Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/162Selection of materials
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0091Aerogels; Xerogels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00Thermal insulation material
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2201/00Foams characterised by the foaming process
    • C08J2201/04Foams characterised by the foaming process characterised by the elimination of a liquid or solid component, e.g. precipitation, leaching out, evaporation
    • C08J2201/05Elimination by evaporation or heat degradation of a liquid phase
    • C08J2201/0502Elimination by evaporation or heat degradation of a liquid phase the liquid phase being organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00Foams characterised by their properties
    • C08J2205/02Foams characterised by their properties the finished foam itself being a gel or a gel being temporarily formed when processing the foamable composition
    • C08J2205/026Aerogel, i.e. a supercritically dried gel
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2379/00Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen, or carbon only, not provided for in groups C08J2361/00 - C08J2377/00
    • C08J2379/02Polyamines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Multimedia (AREA)
  • Acoustics & Sound (AREA)
  • Mechanical Engineering (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Epoxy Resins (AREA)
  • Polyethers (AREA)

Abstract

INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property -, Organization 111111110111101110101011111010111110111010111111111110011111101111101111011111 International Bureau 0.. .... .. ..... ...,/ (10) International Publication Number (43) International Publication Date WO 2017/178548 Al 19 October 2017(19.10.2017) WIPO I PCT (51) International Patent Classification: (74) Agent: HENKEL IP DEPARTMENT; Henkelstr. 67, C08G 73/02 (2006.01) 40589 Diisseldorf (DE). (21) International Application Number: (81) Designated States (unless otherwise indicated, for every PCT/EP2017/058836 kind of national protection available): AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, (22) International Filing Date: BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, 12 April 2017 (12.04.2017) DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, (25) Filing Language: English HN, HR, HU, ID, IL, IN, IR, IS, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, (26) Publication Language: English MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, (30) Priority Data: NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, 16165082.5 13 April 2016 (13.04.2016) EP RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, (71) Applicants: HENKEL AG & CO. KGAA [DE/DE]; Hen- ZA, ZM, ZW. kelstr. 67, 40589 Diisseldorf (DE). HENKEL IP & HOLDING GMBH [DE/DE]; 40589 Diisseldorf, Ger- (84) Designated States (unless otherwise indicated, for every many (DE). kind of regional protection available): ARIPO (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, (72) Inventors: TORRES CANO, Elisabet; Passeig Sant Ger- TZ, UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, vasio 87 1° 4a, 08022 Barcelona (ES). SALHI, Fouad; TJ, TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, 299 Colt Highway, Apt 428, Farmington, Connecticut DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, — 06032 (US). ZUNIGA RUIZ, Camilo; Edifici Eureka, 2nd LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, — floor, Campus UAB - Bellaterra, 08193 Barcelona (ES). SM, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, _ TORRES SANGLAS, Joaquim; Calle Arquitecte Adell GW, KM, ML, MR, NE, SN, TD, TG). Ferrer, 12, 2n la, Cornelia de Llo Barcelona (ES). VEGA . Published: FERNANDEZ, Maria; Calle Alfonso XIII, 42, 3r piso, 08202 Barcelona Asta; Es- — international 21(3)) Sabadell, (ES). SAKALYTE, with search report (Art. = calera 5, 5 0 2a, 43130 Sant Salvador (Tarragona) (ES). = = = = = = = = = = = 1-1 GC 7r 11 in cc IN ,—, (54) Title: BENZOXAZINE BASED COPOLYMER AEROGELS 1-1 C (57) : The present invention relates to a benzoxazine based copolymer aerogel obtained by reacting a benzoxazine ei monomer or oligomer and a comonomer selected from the group consisting of an isocyanate compound, a cyclic ether compound O and an acid anhydride compound in a presence of a catalyst and a solvent, wherein said catalyst is an optional ingredient when said ,-t comonomer is an acid anhydride compound or an isocyanate compound. Benzoxazine based copolymer aerogel according to the present invention provides high thermal insulation material, while good mechanical properties and performance is maintained.
SG11201807304UA 2016-04-13 2017-04-12 Benzoxazine based copolymer aerogels SG11201807304UA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16165082 2016-04-13
PCT/EP2017/058836 WO2017178548A1 (en) 2016-04-13 2017-04-12 Benzoxazine based copolymer aerogels

Publications (1)

Publication Number Publication Date
SG11201807304UA true SG11201807304UA (en) 2018-09-27

Family

ID=55755389

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201807304UA SG11201807304UA (en) 2016-04-13 2017-04-12 Benzoxazine based copolymer aerogels

Country Status (7)

Country Link
US (1) US20190048164A1 (en)
EP (1) EP3443023A1 (en)
JP (1) JP2019511620A (en)
KR (1) KR20180135904A (en)
CN (1) CN108884225A (en)
SG (1) SG11201807304UA (en)
WO (1) WO2017178548A1 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019121242A1 (en) * 2017-12-19 2019-06-27 Henkel Ag & Co. Kgaa Thiol-epoxy based aerogels
US10487077B1 (en) * 2018-06-14 2019-11-26 Sabic Global Technologies B.V. Bis(benzoxazinyl)phthalimidine and associated curable composition and composite
CN109225152B (en) * 2018-10-17 2020-07-28 华南理工大学 Ultrafast high-adsorption-performance cellulose elastic carbon aerogel and preparation method and application thereof
CN113272350A (en) * 2018-11-09 2021-08-17 亨茨曼国际有限公司 Benzoxazine-based polyurethane resin composition
WO2020173911A1 (en) 2019-02-25 2020-09-03 Henkel Ag & Co. Kgaa Composite aerogel material
CN112321783B (en) * 2020-10-14 2021-08-20 南京大学 Elastic aerogel material based on water-based benzoxazine emulsion and preparation method and application thereof
CN112980135B (en) * 2021-02-24 2022-06-10 西南石油大学 Flame-retardant and toughened benzoxazine/bio-based phosphide composite material and preparation method thereof
CN113278164B (en) * 2021-05-13 2023-03-24 电子科技大学 Preparation method of high-strength thermosetting resin hydrogel material
CN113416289B (en) * 2021-07-15 2022-10-11 中国科学院宁波材料技术与工程研究所 Bio-based benzoxazine organic phase change material and preparation method and application thereof
CN113603925A (en) * 2021-08-12 2021-11-05 石家庄铁道大学 Bisphenol F type ultrahigh-strength benzoxazine aerogel
CN114015194B (en) * 2021-10-19 2023-10-20 航天特种材料及工艺技术研究所 Polybenzoxazine aerogel and preparation method thereof
CN116622118B (en) * 2023-04-11 2024-01-30 山东大学 Tough polybenzoxazine aerogel and preparation method thereof
CN116396477B (en) * 2023-04-14 2024-05-28 中国人民解放军国防科技大学 High-temperature-resistant polybenzoxazine aerogel and preparation method thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101666098B1 (en) * 2010-04-01 2016-10-14 삼성전자 주식회사 Aerogel, composition for the aerogel and method of making the aerogel
EP2814802B1 (en) * 2012-02-17 2020-12-16 Huntsman Advanced Materials Americas LLC Mixture of benzoxazine, epoxy and anhydride
CN104744694B (en) * 2015-04-17 2017-11-21 苏州太湖电工新材料股份有限公司 A kind of preparation method of benzoxazine colophony

Also Published As

Publication number Publication date
CN108884225A (en) 2018-11-23
KR20180135904A (en) 2018-12-21
JP2019511620A (en) 2019-04-25
EP3443023A1 (en) 2019-02-20
US20190048164A1 (en) 2019-02-14
WO2017178548A1 (en) 2017-10-19

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