SG11201806430TA - A process for the preparation of propylene oxide - Google Patents
A process for the preparation of propylene oxideInfo
- Publication number
- SG11201806430TA SG11201806430TA SG11201806430TA SG11201806430TA SG11201806430TA SG 11201806430T A SG11201806430T A SG 11201806430TA SG 11201806430T A SG11201806430T A SG 11201806430TA SG 11201806430T A SG11201806430T A SG 11201806430TA SG 11201806430T A SG11201806430T A SG 11201806430TA
- Authority
- SG
- Singapore
- Prior art keywords
- international
- propylene oxide
- str
- liquid feed
- feed stream
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
- B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/36—Use of additives, e.g. for stabilisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/00033—Continuous processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00164—Controlling or regulating processes controlling the flow
- B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Epoxy Compounds (AREA)
Abstract
INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property Organization International Bureau (10) International Publication Number (43) International Publication Date WO 2017/140774 Al 24 August 2017 (24.08.2017) WIPO I PCT 1111111111111101110111111111110101111101110101111111111111011101111111111111110111111 International Patent Classification: C07D 301/12 (2006.01) C07D 301/36 (2006.01) International Application Number: PCT/EP2017/053492 International Filing Date: (25) Filing Language: (26) Publication Language: (30) Priority Data: 16156112.1 17 February 2016 (17.02.2016) EP (71) Applicant: BASF SE [DE/DE]; Ludwigshafen, 67056 Ludwigshafen (DE). (72) Inventors: RIEDEL, Dominic; Richard-Weber-StraBe 20, 68623 Lampertheim (DE). TELES, Joaquim H.; Philipp- Hirsch-Str. 4, 67165 Waldsee (DE). SCHELLING, Hein- er; Am Bilschel 9a, 67273 Bobenheim am Berg (DE). WEGERLE, Ulrike; St.-Bonifatius-Str. 11, 67550 Worms (DE). MULLER, Ulrich; Am Stecken 14a, 67435 Neustadt (DE). PARVULESCU, Andrei-Nicolae; HauptstraBe 74, 67152 Ruppertsberg (DE). MANN- WEILER, Jochen; MittelstraBe 6, 67547 Worms (DE). HENN, Timo; Wassergasse 26, 67294 Staten (DE). LU- DERITZ, Thomas; RingstraBe 30b, 67141 Neuhofen berger Str. 7, 67117 Limburgerhof (DE). URBANCZYK, Daniel; Darmstadter Str. 86, 64347 Griesheim (DE). (74) Agent: HERZOG FIESSER & PARTNER PAT- ENTANWALTE PARTG MBB; ALTMANN, Andreas, DudenstraBe 46, 68167 Mannheim (DE). (81) Designated States (unless otherwise indicated, for every kind of national protection available): AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IR, IS, JP, KE, KG, KH, KN, KP, KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW. (84) Designated States (unless otherwise indicated, for every kind of regional protection available): ARIPO (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, TJ, TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG). Published: 16 February 2017 (16.02.2017) English English DE ORZ laiT ik i 1 1 64293 ( ). W , N co on o; V tor aatz p , Darmstadt (DE). MULLER, Christian; Neckarpromenade 25, 68167 Mannheim (DE). WEBER, Markus; Rupperts- - with international search report (Art. 2 1 (3)) W O 20 1714077 / 4 Al (54) Title: A PROCESS FOR THE PREPARATION OF PROPYLENE OXIDE (57) : A continuous process for the preparation of propylene oxide, comprising a start-up stage and normal run stage, wherein the normal run stage comprises (i) continuously providing a liquid feed stream comprising propene, hydrogen peroxide, acetonitrile, a formate salt, water and optionally propane, wherein in the liquid feed stream, the molar amount of the formate salt Tel - ative to the molar amount of hydrogen peroxide at a given point of time during the normal run stage is a N (Fo/H202); (ii) continuously passing the liquid feed stream provided in (i) into an epoxidation zone comprising a catalyst comprising a titanium zeolite having framework type MWW, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising propylene oxide, acetonitrile, water, the formate salt, optionally propene, and optionally propane; (iii) continuously removing an effluent stream from the epoxidation zone, the effluent stream comprising propylene oxide, acetonitrile, water, at least a portion of the formate salt, optionally propene, and optionally propane; wherein the normal run stage is character - ized in an average rate of change of a N (Fo/H 2 0 2 ) of less than 0 h-1.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP16156112 | 2016-02-17 | ||
PCT/EP2017/053492 WO2017140774A1 (en) | 2016-02-17 | 2017-02-16 | A process for the preparation of propylene oxide |
Publications (1)
Publication Number | Publication Date |
---|---|
SG11201806430TA true SG11201806430TA (en) | 2018-09-27 |
Family
ID=55409729
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SG11201806430TA SG11201806430TA (en) | 2016-02-17 | 2017-02-16 | A process for the preparation of propylene oxide |
Country Status (13)
Country | Link |
---|---|
US (1) | US10544115B2 (en) |
EP (1) | EP3416954B1 (en) |
KR (1) | KR20180112856A (en) |
CN (1) | CN109071475B (en) |
BR (1) | BR112018016770B1 (en) |
ES (1) | ES2831762T3 (en) |
HU (1) | HUE051214T2 (en) |
MX (1) | MX2018010016A (en) |
PL (1) | PL3416954T3 (en) |
RU (1) | RU2734823C2 (en) |
SG (1) | SG11201806430TA (en) |
WO (1) | WO2017140774A1 (en) |
ZA (1) | ZA201806073B (en) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2867052T3 (en) | 2016-06-29 | 2021-10-20 | Basf Se | Process for preparing alpha and beta unsaturated aldehydes by oxidation of alcohols in the presence of a liquid phase |
WO2018096171A1 (en) | 2016-11-28 | 2018-05-31 | Basf Se | Catalyst composite comprising an alkaline earth metal containing cha zeolite and use thereof in a process for the conversion of oxygenates to olefins |
US11091425B2 (en) | 2016-11-30 | 2021-08-17 | Basf Se | Process for the conversion of ethylene glycol to ethylenediamine employing a zeolite catalyst |
JP2019536774A (en) | 2016-11-30 | 2019-12-19 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Method for converting monoethanolamine to ethylenediamine using copper-modified zeolite having a MOR skeleton structure |
MX2019010265A (en) | 2017-02-28 | 2019-10-14 | Basf Se | Process for preparing an unsaturated alcohol. |
US10961177B2 (en) | 2017-03-21 | 2021-03-30 | Basf Se | Process for preparing an anticorrosion component for an antifreeze |
US10774034B2 (en) | 2017-05-03 | 2020-09-15 | Basf Se | Process for the conversion of ethylene oxide to monoethanolamine and ethylenediamine employing a zeolite |
JP7266577B2 (en) | 2017-08-04 | 2023-04-28 | ビーエーエスエフ ソシエタス・ヨーロピア | A zeolitic material having a framework type CHA and containing a transition metal and one or more of potassium and cesium |
US20230030960A1 (en) * | 2019-12-20 | 2023-02-02 | Basf Se | A molding comprising a ti-mww zeolite and having a specific lewis acidity |
CN113387907B (en) * | 2021-06-30 | 2022-08-02 | 中国石油化工股份有限公司 | System and method for continuously producing propylene oxide by industrial propane |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3936854A1 (en) | 1989-11-06 | 1991-05-08 | Basf Ag | METHOD FOR PRODUCING METHYL FORMATE |
EP1122249A1 (en) | 2000-02-02 | 2001-08-08 | SOLVAY (Société Anonyme) | Process for producing oxiranes |
RU2537296C2 (en) * | 2009-07-16 | 2014-12-27 | Басф Се | Method of separating acetonitrile from water |
EP3024578B1 (en) | 2013-07-24 | 2018-05-30 | Basf Se | A process for preparing propylene oxide |
-
2017
- 2017-02-16 MX MX2018010016A patent/MX2018010016A/en unknown
- 2017-02-16 RU RU2018132763A patent/RU2734823C2/en active
- 2017-02-16 CN CN201780024060.9A patent/CN109071475B/en active Active
- 2017-02-16 KR KR1020187026838A patent/KR20180112856A/en active IP Right Grant
- 2017-02-16 ES ES17705863T patent/ES2831762T3/en active Active
- 2017-02-16 BR BR112018016770-3A patent/BR112018016770B1/en active IP Right Grant
- 2017-02-16 PL PL17705863T patent/PL3416954T3/en unknown
- 2017-02-16 HU HUE17705863A patent/HUE051214T2/en unknown
- 2017-02-16 EP EP17705863.3A patent/EP3416954B1/en active Active
- 2017-02-16 US US16/076,600 patent/US10544115B2/en active Active
- 2017-02-16 WO PCT/EP2017/053492 patent/WO2017140774A1/en active Application Filing
- 2017-02-16 SG SG11201806430TA patent/SG11201806430TA/en unknown
-
2018
- 2018-09-11 ZA ZA2018/06073A patent/ZA201806073B/en unknown
Also Published As
Publication number | Publication date |
---|---|
ZA201806073B (en) | 2021-04-28 |
RU2018132763A3 (en) | 2020-05-14 |
RU2734823C2 (en) | 2020-10-23 |
MX2018010016A (en) | 2018-11-09 |
US10544115B2 (en) | 2020-01-28 |
US20190077779A1 (en) | 2019-03-14 |
BR112018016770A2 (en) | 2018-12-26 |
EP3416954B1 (en) | 2020-08-19 |
ES2831762T3 (en) | 2021-06-09 |
EP3416954A1 (en) | 2018-12-26 |
RU2018132763A (en) | 2020-03-18 |
PL3416954T3 (en) | 2021-01-25 |
BR112018016770B1 (en) | 2022-11-01 |
WO2017140774A1 (en) | 2017-08-24 |
KR20180112856A (en) | 2018-10-12 |
CN109071475B (en) | 2022-12-27 |
CN109071475A (en) | 2018-12-21 |
HUE051214T2 (en) | 2021-03-01 |
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