SG11201802071XA - Processes for purifying acetic acid and hydrating anhydride - Google Patents

Processes for purifying acetic acid and hydrating anhydride

Info

Publication number
SG11201802071XA
SG11201802071XA SG11201802071XA SG11201802071XA SG11201802071XA SG 11201802071X A SG11201802071X A SG 11201802071XA SG 11201802071X A SG11201802071X A SG 11201802071XA SG 11201802071X A SG11201802071X A SG 11201802071XA SG 11201802071X A SG11201802071X A SG 11201802071XA
Authority
SG
Singapore
Prior art keywords
hydrating
anhydride
processes
acetic acid
purifying acetic
Prior art date
Application number
SG11201802071XA
Inventor
Ronald D Shaver
Yaw-Hwa Liu
Mark O Scates
Original Assignee
Celanese Int Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Int Corp filed Critical Celanese Int Corp
Publication of SG11201802071XA publication Critical patent/SG11201802071XA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/083Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid anhydrides
    • C07C51/087Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid anhydrides by hydrolysis
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/47Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/54Preparation of carboxylic acid anhydrides
    • C07C51/56Preparation of carboxylic acid anhydrides from organic acids, their salts, their esters or their halides, e.g. by carboxylation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/12Acetic anhydride

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SG11201802071XA 2015-11-13 2016-11-11 Processes for purifying acetic acid and hydrating anhydride SG11201802071XA (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562255060P 2015-11-13 2015-11-13
US15/348,466 US9908835B2 (en) 2015-11-13 2016-11-10 Processes for purifying acetic and hydrating anhydride
PCT/US2016/061570 WO2017083677A1 (en) 2015-11-13 2016-11-11 Processes for purifying acetic acid and hydrating anhydride

Publications (1)

Publication Number Publication Date
SG11201802071XA true SG11201802071XA (en) 2018-05-30

Family

ID=58692007

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201802071XA SG11201802071XA (en) 2015-11-13 2016-11-11 Processes for purifying acetic acid and hydrating anhydride

Country Status (11)

Country Link
US (4) US9908835B2 (en)
EP (1) EP3374341B1 (en)
JP (1) JP6821672B2 (en)
KR (2) KR102669186B1 (en)
CN (1) CN108349864B (en)
MX (2) MX2018005281A (en)
MY (1) MY183686A (en)
RS (1) RS60055B1 (en)
SA (1) SA518391324B1 (en)
SG (1) SG11201802071XA (en)
WO (1) WO2017083677A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9908835B2 (en) * 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
CN114307252B (en) * 2021-12-30 2022-09-20 南京工业大学 Process for separating sugar and acid by using quasi-two-dimensional chromatography
CN116606204B (en) * 2023-07-17 2023-10-20 成都普什医药塑料包装有限公司 Recovered acetic acid for low-chroma acetic anhydride and cellulose acetate, and recovery method and application thereof

Family Cites Families (78)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB721301A (en) * 1952-03-19 1955-01-05 Anglo Iranian Oil Co Ltd Improvements in or relating to the separation of acetic acid from aqueous mixtures of organic compounds by distillation
US2770585A (en) * 1952-07-02 1956-11-13 Celanese Corp Purification of acids containing 2 to 6 carbon atoms
US3576870A (en) * 1967-07-05 1971-04-27 Du Pont Process for purifying n,n-dimethylacetamide
US3560560A (en) 1968-05-08 1971-02-02 Union Carbide Corp Purification of acetic acid
US3769329A (en) 1970-03-12 1973-10-30 Monsanto Co Production of carboxylic acids and esters
US4110372A (en) * 1972-11-29 1978-08-29 Hoechst Aktiengesellschaft Process for the purification of carboxylic acids
DE2450965C2 (en) 1974-10-26 1983-06-09 Hoechst Ag, 6230 Frankfurt Process for the production of acetic anhydride
US4115444A (en) 1975-03-10 1978-09-19 Halcon International, Inc. Process for preparing carboxylic acid anhydrides
SU798089A1 (en) * 1978-04-06 1981-01-23 Предприятие П/Я А-7372 Method of acetic acid purification from acetic anhydride
US4374070A (en) 1980-11-21 1983-02-15 Eastman Kodak Company Preparation of acetic anhydride
NL8204901A (en) 1981-12-30 1983-07-18 Halcon Sd Group Inc PURIFICATION OF CARBONYLATION PRODUCTS.
US5144068A (en) 1984-05-03 1992-09-01 Hoechst Celanese Corporation Methanol carbonylation process
US5001259A (en) 1984-05-03 1991-03-19 Hoechst Celanese Corporation Methanol carbonylation process
CA1228867A (en) 1984-05-03 1987-11-03 G. Paull Torrence Methanol carbonylation process
US5026908A (en) 1984-05-03 1991-06-25 Hoechst Celanese Corporation Methanol carbonylation process
US4615806B1 (en) 1985-03-07 1994-05-03 Hoechst Co American Removal of iodide compounds from non-aqueous organic media
GB9023634D0 (en) 1990-10-31 1990-12-12 British Petroleum Co Plc Process for purifying acetic acid and/or acetic anhydride
EP0563124B1 (en) 1990-12-20 1995-03-29 Eastman Chemical Company Continuous process for the preparation of acetic anhydride or mixtures of acetic anhydride and acetic acid
US5220058A (en) 1991-09-30 1993-06-15 Union Carbide Chemicals & Plastics Technology Corporation Iodide removal process
GB9122168D0 (en) 1991-10-18 1991-11-27 Bp Chem Int Ltd Process
US5672743A (en) 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
JP3377555B2 (en) 1993-05-31 2003-02-17 ダイセル化学工業株式会社 Method for removing iodine compound contained in carbonylation reaction product
EP0665210B2 (en) 1993-08-18 2005-11-23 Daicel Chemical Industries, Ltd. Process for producing acetic anhydride alone or both of acetic anhydride and acetic acid
JP3244385B2 (en) 1994-06-15 2002-01-07 ダイセル化学工業株式会社 Method for producing high-purity acetic acid
US5625095A (en) 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
US5696284A (en) 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof
CA2234853C (en) 1995-10-27 2005-01-11 Hoechst Celanese Corporation Process for improving productivity of a carbonylation catalyst solution by removing corrosion metals
JP3281258B2 (en) 1996-04-26 2002-05-13 ダイセル化学工業株式会社 Operating method for removing iodine compounds contained in organic medium
IN192600B (en) 1996-10-18 2004-05-08 Hoechst Celanese Corp
US6339171B1 (en) 1996-10-18 2002-01-15 Celanese International Corporation Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream
US5831120A (en) 1996-11-19 1998-11-03 Watson; Derrick John Process for the production of acetic acid
GB9625335D0 (en) 1996-12-05 1997-01-22 Bp Chem Int Ltd Process
GB9626428D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626429D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9626317D0 (en) 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
JPH10231267A (en) 1997-02-19 1998-09-02 Chiyoda Corp Production of organic carboxylic acid
US6066762A (en) 1996-12-30 2000-05-23 Chiyoda Corporation Process for the production of carbonyl compound
GB9802027D0 (en) 1998-01-31 1998-03-25 Bp Chem Int Ltd Chemical process
US5962735A (en) 1998-03-06 1999-10-05 Uop Llc Method for treating an organic liquid contaminated with an iodide compound
CN1199981C (en) 1998-04-28 2005-05-04 蔡传英 Zinc scutellarin as a new medicine
US6552221B1 (en) * 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US6225498B1 (en) * 2000-03-24 2001-05-01 Celanese International Corporation Method of removing organic iodides from organic media
US6657078B2 (en) 2001-02-07 2003-12-02 Celanese International Corporation Low energy carbonylation process
US6677480B2 (en) 2002-01-28 2004-01-13 Celanese International Corporation Process control in production of acetic acid via use of heavy phase density measurement
JP2004131389A (en) 2002-10-08 2004-04-30 Daicel Chem Ind Ltd Method for producing carboxylic acid and system for its production
US7005541B2 (en) 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
JP4526381B2 (en) 2004-12-27 2010-08-18 ダイセル化学工業株式会社 Method for producing acetic acid
US7855306B2 (en) 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
CN101223124B (en) 2005-07-14 2011-05-04 大赛璐化学工业株式会社 Process for producing carboxylic acid
US7737298B2 (en) 2006-06-09 2010-06-15 Eastman Chemical Company Production of acetic acid and mixtures of acetic acid and acetic anhydride
US8017802B2 (en) 2007-05-21 2011-09-13 Celanese International Corporation Control of impurities in reaction product of rhodium-catalyzed methanol carbonylation
GB2455282A (en) 2007-10-31 2009-06-10 Hewlett Packard Development Co Error correction in data communication system using iterative belief propagation with syndrome sent over a separate channel
US8729301B2 (en) * 2008-04-03 2014-05-20 Dow Corning Corporation Method of dehydrating acetic acid
US7884237B2 (en) 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8168822B2 (en) 2009-07-07 2012-05-01 Celanese International Corporation Acetic acid production by way of carbonylation with enhanced reaction and flashing
US9261929B2 (en) 2009-08-20 2016-02-16 Hewlett-Packard Development Company, L.P. Cooling device control
US8519181B2 (en) * 2010-04-07 2013-08-27 Lyondell Chemical Technology, L.P. Preparation of acetic acid
WO2011146446A1 (en) 2010-05-18 2011-11-24 Celanese International Corporation Process for purifying acetic acid streams by removing permanganate reducing compounds
KR101747484B1 (en) 2010-07-26 2017-06-14 주식회사 다이셀 Process for producing acetic acid
US8378141B2 (en) 2010-08-16 2013-02-19 Celanese International Corporation Process and system for supplying vapor from drying column to light ends column
CN103249705B (en) 2010-10-06 2015-11-25 株式会社大赛璐 The manufacture method of acetic acid
CN102442907B (en) * 2010-10-12 2015-04-08 上海华谊工程技术有限公司 Method for removing organic amine catalyst and acetic anhydride in acetoacetic ester reaction solution
US9416086B2 (en) 2010-11-12 2016-08-16 Eastman Chemical Company Processes for purification of acid solutions
KR101851035B1 (en) 2010-12-15 2018-04-20 주식회사 다이셀 Acetic acid production method
CN103402964B (en) 2010-12-15 2015-09-02 株式会社大赛璐 The preparation method of acetic acid
WO2012081416A1 (en) 2010-12-15 2012-06-21 株式会社ダイセル Acetic acid production method
EP2657220B1 (en) 2010-12-24 2016-08-31 Daicel Corporation Acetic acid production method
CN103121934B (en) * 2011-11-18 2014-07-23 中国石油化工股份有限公司 Method for reducing iodide impurity content in acetic acid
TWI547477B (en) 2012-03-14 2016-09-01 大賽璐股份有限公司 Process for producing acetic acid
US8759576B2 (en) 2012-09-06 2014-06-24 Celanese International Corporation Processes for purifying acetic anhydride
MX356188B (en) 2012-12-21 2018-05-16 Daicel Corp Method for producing acetic acid.
US9415366B2 (en) 2012-12-31 2016-08-16 Eastman Chemical Company Systems and methods for processing variable acetyl streams
AR094541A1 (en) 2013-01-25 2015-08-12 Daicel Corp PROCEDURE TO PRODUCE CARBOXYL ACID
WO2017057085A1 (en) 2015-09-29 2017-04-06 株式会社ダイセル Method of producing acetic acid
US9908835B2 (en) * 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
MX2018005994A (en) 2016-03-01 2018-08-29 Daicel Corp Acetic acid production method.

Also Published As

Publication number Publication date
EP3374341B1 (en) 2020-01-01
KR20180081708A (en) 2018-07-17
RS60055B1 (en) 2020-04-30
US20200247743A1 (en) 2020-08-06
KR20240074922A (en) 2024-05-28
US10160714B2 (en) 2018-12-25
US20190055184A1 (en) 2019-02-21
US20170137364A1 (en) 2017-05-18
JP2018533555A (en) 2018-11-15
MY183686A (en) 2021-03-08
US20180141890A1 (en) 2018-05-24
KR102669186B1 (en) 2024-05-23
MX2023004496A (en) 2023-05-10
EP3374341A1 (en) 2018-09-19
US10689319B2 (en) 2020-06-23
CN108349864B (en) 2021-04-13
US10899696B2 (en) 2021-01-26
WO2017083677A1 (en) 2017-05-18
CN108349864A (en) 2018-07-31
JP6821672B2 (en) 2021-01-27
US9908835B2 (en) 2018-03-06
SA518391324B1 (en) 2022-04-24
MX2018005281A (en) 2018-06-22

Similar Documents

Publication Publication Date Title
EP3232781A4 (en) Methods for forming peroxyformic acid and uses thereof
EP3221267A4 (en) System and method for water purification
ZA201902338B (en) Method and system for producing ethylene and acetic acid
SG11201800858SA (en) Method and apparatus for producing acetic acid
SG11201606743PA (en) Process and system for producing acrylic acid
SG11201703427QA (en) Processes for producing an acetic acid product having low butyl acetate content
PL3148661T3 (en) Method for purification of benzoic acid
EP3364960C0 (en) Agent for supportive immunomodulation containing propionic acid and fumaric acid ester
SG11201706506YA (en) Acetic acid process
SG11201609909SA (en) Improved catalytic performance in processes for preparing acetic acid
IL254836A0 (en) Process for isolating and purifying ambrox
SG11201609779YA (en) Process for the co-production of acetic acid and dimethyl ether
SG11201706008YA (en) Processes for producing acetic acid
ZA201708157B (en) Cyclopropane carboxylic acid derivatives and pharmaceutical uses thereof
SG11201608513WA (en) Novel purification process of gonadotropin
SG11201702183RA (en) Improved catalyst stability and corrosion prevention in acetic acid production process
EP3162788A4 (en) Method for purifying ferulic acid and/or salts thereof
SG11201802071XA (en) Processes for purifying acetic acid and hydrating anhydride
PL3271322T3 (en) Process for the purification of monochloroacetic acid
GB2539990B (en) Catalyst system and process
SG11201707217TA (en) Processes for producing acetic acid
RS62896B1 (en) Process for producing acetic acid
EP2987818A4 (en) Novel polycarboxylic acid anhydride and use thereof
EP3936499C0 (en) Process to produce acetic acid
EP3256455C0 (en) Method for the reduction of carboxylic acids or carbonic acid and their derivatives