SG11201408036QA - Method of making polymers, polymer compositions and articles containing such polymers - Google Patents
Method of making polymers, polymer compositions and articles containing such polymersInfo
- Publication number
- SG11201408036QA SG11201408036QA SG11201408036QA SG11201408036QA SG11201408036QA SG 11201408036Q A SG11201408036Q A SG 11201408036QA SG 11201408036Q A SG11201408036Q A SG 11201408036QA SG 11201408036Q A SG11201408036Q A SG 11201408036QA SG 11201408036Q A SG11201408036Q A SG 11201408036QA
- Authority
- SG
- Singapore
- Prior art keywords
- polymer
- international
- lllll
- ohio
- polymers
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 title abstract 13
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 239000000203 mixture Substances 0.000 title abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 abstract 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 1
- 208000025370 Middle East respiratory syndrome Diseases 0.000 abstract 1
- 230000032683 aging Effects 0.000 abstract 1
- -1 alkoxy silane Chemical compound 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 1
- 150000001993 dienes Chemical class 0.000 abstract 1
- 125000005842 heteroatom Chemical group 0.000 abstract 1
- 239000003999 initiator Substances 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 230000008520 organization Effects 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 229960003903 oxygen Drugs 0.000 abstract 1
- 229910000077 silane Inorganic materials 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
- C08K5/541—Silicon-containing compounds containing oxygen
- C08K5/5415—Silicon-containing compounds containing oxygen containing at least one Si—O bond
- C08K5/5419—Silicon-containing compounds containing oxygen containing at least one Si—O bond containing at least one Si—C bond
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C19/00—Chemical modification of rubber
- C08C19/25—Incorporating silicon atoms into the molecule
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C19/00—Chemical modification of rubber
- C08C19/30—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule
- C08C19/42—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule reacting with metals or metal-containing groups
- C08C19/44—Addition of a reagent which reacts with a hetero atom or a group containing hetero atoms of the macromolecule reacting with metals or metal-containing groups of polymers containing metal atoms exclusively at one or both ends of the skeleton
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C2/00—Treatment of rubber solutions
- C08C2/06—Winning of rubber from solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F236/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
- C08F236/02—Copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
- C08F236/04—Copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
- C08F236/10—Copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated with vinyl-aromatic monomers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F36/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
- C08F36/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
- C08F36/04—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
- C08F36/06—Butadiene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/205—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase
- C08J3/21—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase the polymer being premixed with a liquid phase
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L15/00—Compositions of rubber derivatives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
- C08F2500/21—Rubbery or elastomeric properties
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2309/00—Characterised by the use of homopolymers or copolymers of conjugated diene hydrocarbons
- C08J2309/06—Copolymers with styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Materials Engineering (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Polyamides (AREA)
Abstract
(12) INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property Organization International Bureau (43) International Publication Date 12 December 2013 (12.12.2013) WIPOIPCT (10) International Publication Number WO 2013/184783 A3 (51) International Patent Classification: C08C19/25 (2006.01) C08L 15/00 (2006.01) C08F 36/06 (2006.01) B60C1/00 (2006.01) C08F 236/10 ( 2006.01) (21) International Application Number: PCT/US2013/044288 (22) International Filing Date: 5 June 2013 (05.06.2013) (25) Filing Language: English (26) Publication Language: English (30) Priority Data: 61/656,144 6 June 2012 (06.06.2012) US (71) Applicant: FIRESTONE POLYMERS, LLC [US/US]; 381 West Wilbeth Road, Akron, Ohio 44301 (US). (72) Inventors: NAKATANI, Kenji; 10-1, Kyobashi 1-Chome, Chuo-Ku, Tokyo 104-8340 (JP). DEDECKER, Mark N.; 8775 Leyland Avenue NW, North Canton, Ohio 44720 (US). PADOLEWSKI, Joseph P.; 165 Hunt Club Drive, Apt. 3C, Copley, Ohio 44321 (US). PAWLOW, James H.; 1984 Braewick Drive, Akron, Ohio 44313 (US). (74) Agents: HOOKER, Meredith E et al.; 10 East Firestone Blvd., Akron, Ohio 44317 (US). [Continued on next page] (54) Title: METHOD OF MAKING POLYMERS, POLYMER COMPOSITIONS AND ARTICLES CONTAINING SUCH POLY MERS (57) Abstract: A method of making a polymer with stable Mooney viscosity and molecular weight is de scribed. A conjugated diolefin reacted in is a hydrocar bon solvent in the presence of an initiator to form a polymer. After forming the polymer, alkoxy silane ter minal functionalizing groups are bonded to the poly mer. A stabilizing agent having the formula (R)4- „Si(OH)n wherein R is a Ci to Cis alkyl, Ci to Cis alkyl group containing heteroatom such a as nitrogen or oxy gen, C 4 to C cycloalkyl, 8 or C 6 to Cis aromatic group is then added to the polymer, optionally in the presence of hydrocarbon oil. The polymer is then desolvatizing, resulting in a polymer with stable Mooney viscosity and molecular weight, even over prolonged periods of time. Compositions and articles containing the polymer are also described. (81) Designated States (unless otherwise indicated, for every kind of national protection available)'. AE, AG, AL, AM, AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, CA, CH, CL, CN, CO, CR, CU, CZ, DE, DK, DM, DO, DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, HR, HU, ID, IL, IN, IS, JP, KE, KG, KN, KP, KR, KZ, LA, LC, LK, LR, LS, LT, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW. (84) Designated States (unless otherwise indicated, for every kind of regional protection available)'. ARIPO (BW, GH, GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, SZ, TZ, UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, TJ, TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, KM, ML, MR, NE, SN, TD, TG). Published: — with international search report (Art. 21(3)) FIG. 1 ML4 vs. Aging \ 120 WO 2013/184783 A3 I lllll llllllll II llllll III lllll lllll III III III lllll lllll lllll lllll lllll llll llll lllllll llll llll - before the expiration of the time limit for amending the (88 » Date of publication of the international search^report: claims and to be republished in the event of receipt of amendments (Rule 48.2(h))
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261656144P | 2012-06-06 | 2012-06-06 | |
| PCT/US2013/044288 WO2013184783A2 (en) | 2012-06-06 | 2013-06-05 | Method of making polymers, polymer compositions and articles containing such polymers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SG11201408036QA true SG11201408036QA (en) | 2015-01-29 |
Family
ID=49712830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SG11201408036QA SG11201408036QA (en) | 2012-06-06 | 2013-06-05 | Method of making polymers, polymer compositions and articles containing such polymers |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10400089B2 (en) |
| EP (1) | EP2859020B1 (en) |
| JP (1) | JP6239600B2 (en) |
| KR (1) | KR20150021550A (en) |
| CN (1) | CN104428321B (en) |
| BR (1) | BR112014030696A2 (en) |
| RU (1) | RU2649008C2 (en) |
| SG (1) | SG11201408036QA (en) |
| WO (1) | WO2013184783A2 (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3080167B1 (en) | 2013-12-12 | 2024-12-04 | Firestone Polymers, LLC | Method for producing polymeric compositions including functionalized polymers |
| EP3110749A1 (en) * | 2014-02-28 | 2017-01-04 | ExxonMobil Chemical Patents Inc. | Nanocomposite mooney viscosity stability |
| KR101918369B1 (en) * | 2015-12-18 | 2018-11-13 | 주식회사 엘지화학 | Method for preparing modified conjugated diene polymer |
| JP6679398B2 (en) * | 2016-04-25 | 2020-04-15 | 株式会社ブリヂストン | Method for producing modified polymer, modified polymer, rubber composition and tire |
| JP6752053B2 (en) * | 2016-05-24 | 2020-09-09 | 旭化成株式会社 | Method for producing conjugated diene polymer and method for producing rubber veil |
| WO2019122750A1 (en) | 2017-12-22 | 2019-06-27 | Compagnie Generale Des Etablissements Michelin | Compound comprising at least two trialcoxysilyl groups, use of same as a diene elastomer functionalisation agent, modified diene elastomer and composition containing same |
| KR102678859B1 (en) * | 2018-10-12 | 2024-06-28 | 브리지스톤 어메리카스 타이어 오퍼레이션스, 엘엘씨 | Modified diene copolymer with stabilized target viscosity |
| JP2022531495A (en) | 2019-05-07 | 2022-07-06 | ブリヂストン アメリカズ タイヤ オペレーションズ、 エルエルシー | Modified high cispolybutadiene polymer, related methods and rubber compositions |
| JP7334267B2 (en) | 2019-05-14 | 2023-08-28 | 株式会社ブリヂストン | Modified high-cis polybutadiene polymers, related methods and tire compositions |
| EP3907244B1 (en) | 2019-09-11 | 2025-07-09 | LG Chem, Ltd. | Modified conjugated diene-based polymer, method for preparing same, and rubber composition comprising same |
| BR112021022891A2 (en) | 2019-09-11 | 2022-03-29 | Lg Chemical Ltd | Modified conjugated diene based polymer and rubber composition including the same |
| TW202122426A (en) | 2019-09-11 | 2021-06-16 | 南韓商Ｌｇ化學股份有限公司 | Modified conjugated diene-based polymer,method for preparing the same and rubber composition including the same |
| WO2021049915A1 (en) | 2019-09-11 | 2021-03-18 | 주식회사 엘지화학 | Modified conjugated diene-based polymer and rubber composition comprising same |
| KR20210031407A (en) | 2019-09-11 | 2021-03-19 | 주식회사 엘지화학 | Modified conjugated diene-based polymer, preparing method thereof and rubber composition comprising the same |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2821232A (en) * | 1954-07-08 | 1958-01-28 | Columbia Southern Chem Corp | Rubber tire tread composition containing carbon black and silica and tire made from same |
| US3244664A (en) | 1960-10-24 | 1966-04-05 | Phillips Petroleum Co | Silicon-containing polymers |
| US3423385A (en) * | 1964-09-18 | 1969-01-21 | Firestone Tire & Rubber Co | Process for purifying butadiene stream |
| GB1597500A (en) | 1977-12-29 | 1981-09-09 | Shell Int Research | Polymers |
| US4429091A (en) | 1983-03-09 | 1984-01-31 | The Firestone Tire & Rubber Company | Oligomeric oxolanyl alkanes as modifiers for polymerization of dienes using lithium-based initiators |
| EP0169536B1 (en) * | 1984-07-26 | 1994-05-18 | Kanegafuchi Chemical Industry Co., Ltd. | Curable polymer composition |
| JPS6134066A (en) * | 1984-07-26 | 1986-02-18 | Kanegafuchi Chem Ind Co Ltd | Composition having improved tensile characteristics |
| US5659056A (en) | 1996-04-10 | 1997-08-19 | Bridgestone Corporation | Stabilization of siloxane terminated polymers |
| US6393167B1 (en) | 1998-07-31 | 2002-05-21 | Monica K. Davis | Fast, environmentally-stable fiber switches using a Sagnac interferometer |
| US6255404B1 (en) * | 1999-07-26 | 2001-07-03 | Bridgestone Corporation | Method to control increase in viscosity during aging of siloxane modified polymers |
| US6279632B1 (en) | 1999-11-24 | 2001-08-28 | Bridgestone Corporation | Method to control increase in viscosity during aging of siloxane modified polymers |
| DE69907230T2 (en) | 1999-12-02 | 2004-02-05 | Bridgestone Corp. | Polymer, process for making and using this polymer in a rubber composition |
| EP1326914B1 (en) | 2000-10-13 | 2006-06-21 | Société de Technologie Michelin | Rubber composition comprising as coupling agent a polyfunctional organosilane |
| KR100403089B1 (en) * | 2001-01-03 | 2003-10-30 | 금호석유화학 주식회사 | A manufacturing method of an end-modified diene copolymer |
| RU2266917C2 (en) * | 2001-02-15 | 2005-12-27 | Джей Эс Эр КОРПОРЕЙШН | Oil-filled 1,2-polybutadiene, method for its preparing, its composition and molded article |
| JP4139949B2 (en) | 2002-07-19 | 2008-08-27 | Ｊｓｒ株式会社 | Conjugated diolefin (co) polymer rubber and method for producing the same |
| CN100347208C (en) * | 2001-09-27 | 2007-11-07 | Jsr株式会社 | Conjugated diene homo-or copolymer rubber, method for producing homo-or copolymer rubber, rubber composition, composite, and tire |
| JP5576020B2 (en) | 2005-09-22 | 2014-08-20 | 旭化成ケミカルズ株式会社 | Conjugated diene polymer and process for producing the same |
| US9718931B2 (en) | 2012-06-06 | 2017-08-01 | Firestone Polymers, Llc | Method of making base stabilized polymers, polymer compositions and articles containing such polymers |
| WO2013184756A1 (en) | 2012-06-06 | 2013-12-12 | Firestone Polymers, Llc | Method of making iminosilane stabilized polymers, polymer compositions, and articles containing such polymers |
| US9611364B2 (en) | 2012-06-06 | 2017-04-04 | Firestone Polymers, Llc | Method of making alkoxysilane stabilized polymers, and polymer compositions |
-
2013
- 2013-06-05 EP EP13800495.7A patent/EP2859020B1/en active Active
- 2013-06-05 JP JP2015516168A patent/JP6239600B2/en active Active
- 2013-06-05 CN CN201380036977.2A patent/CN104428321B/en not_active Expired - Fee Related
- 2013-06-05 KR KR1020147036886A patent/KR20150021550A/en not_active Abandoned
- 2013-06-05 BR BR112014030696A patent/BR112014030696A2/en active Search and Examination
- 2013-06-05 SG SG11201408036QA patent/SG11201408036QA/en unknown
- 2013-06-05 US US14/405,624 patent/US10400089B2/en active Active
- 2013-06-05 RU RU2014153539A patent/RU2649008C2/en not_active IP Right Cessation
- 2013-06-05 WO PCT/US2013/044288 patent/WO2013184783A2/en active Application Filing
Also Published As
| Publication number | Publication date |
|---|---|
| US20150166738A1 (en) | 2015-06-18 |
| RU2014153539A (en) | 2016-08-10 |
| EP2859020A2 (en) | 2015-04-15 |
| JP2015520272A (en) | 2015-07-16 |
| CN104428321B (en) | 2019-01-29 |
| JP6239600B2 (en) | 2017-11-29 |
| WO2013184783A2 (en) | 2013-12-12 |
| EP2859020B1 (en) | 2020-02-12 |
| CN104428321A (en) | 2015-03-18 |
| EP2859020A4 (en) | 2016-02-24 |
| BR112014030696A2 (en) | 2017-06-27 |
| WO2013184783A3 (en) | 2014-03-20 |
| US10400089B2 (en) | 2019-09-03 |
| RU2649008C2 (en) | 2018-03-29 |
| KR20150021550A (en) | 2015-03-02 |
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