SE7513307L - DIVISION PROCEDURE AND ASSOCIATIONS - Google Patents

DIVISION PROCEDURE AND ASSOCIATIONS

Info

Publication number
SE7513307L
SE7513307L SE7513307A SE7513307A SE7513307L SE 7513307 L SE7513307 L SE 7513307L SE 7513307 A SE7513307 A SE 7513307A SE 7513307 A SE7513307 A SE 7513307A SE 7513307 L SE7513307 L SE 7513307L
Authority
SE
Sweden
Prior art keywords
dihydroxypropane
butylamino
diastereoisomer
solution
enantiomers
Prior art date
Application number
SE7513307A
Other languages
Swedish (sv)
Other versions
SE435499B (en
Inventor
D F Reinhold
Original Assignee
Merck & Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Merck & Co Inc filed Critical Merck & Co Inc
Publication of SE7513307L publication Critical patent/SE7513307L/en
Publication of SE435499B publication Critical patent/SE435499B/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/10—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic with one amino group and at least two hydroxy groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B53/00—Asymmetric syntheses
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B57/00—Separation of optically-active compounds

Abstract

1470030 Optical resolution of 1-t-butylamino- 2,3-dihydroxypropane MERCK & CO Inc 10 Dec 1975 [13 Dec 1974 25 Sept 1975] 50632/75 Heading C2C Mixtures of enantiomers of 1-t-butylamino- 2,3-dihydroxypropane are optically resolved by (1) treating a solution of the mixture with a resolving agent selected from S-pyroglutamic acid, R-pyroglutamic acid, L-tartaric acid and D-tartaric acid (2) separating from the solution the solid diastereoisomer which forms and (3) recovering from the diastereoisomer a single enantiomer of 1-t-butylamino-2,3-dihydroxypropane, e.g. by treating it with a base or running a solution of the diastereoisomer through an ion-exchange resin. The initial mixture of enantiomers of 1-t-butylamino-2,3-dihydroxypropane may be made by reacting t-butylamine with glycidol.
SE7513307A 1974-12-13 1975-11-26 DIASTEREOMERED SALT OF S-1-T-BUTYLAMINO-2,3-DIHYDROXIPROPAN SE435499B (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US53254774A 1974-12-13 1974-12-13
US61594175A 1975-09-25 1975-09-25

Publications (2)

Publication Number Publication Date
SE7513307L true SE7513307L (en) 1976-06-14
SE435499B SE435499B (en) 1984-10-01

Family

ID=27063872

Family Applications (1)

Application Number Title Priority Date Filing Date
SE7513307A SE435499B (en) 1974-12-13 1975-11-26 DIASTEREOMERED SALT OF S-1-T-BUTYLAMINO-2,3-DIHYDROXIPROPAN

Country Status (10)

Country Link
JP (1) JPS51118711A (en)
AU (1) AU510799B2 (en)
CA (1) CA1064943A (en)
DE (1) DE2556040C2 (en)
DK (1) DK532575A (en)
FR (2) FR2294151A1 (en)
GB (1) GB1470030A (en)
IE (1) IE42206B1 (en)
NL (1) NL7513818A (en)
SE (1) SE435499B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5931693A (en) * 1982-08-13 1984-02-20 Kanegafuchi Chem Ind Co Ltd Preparation of optical active oxazolidinone derivative
JPH01149775A (en) * 1987-12-07 1989-06-12 Kawaken Fine Chem Co Ltd Production of optically active 2-methylpiperazine
US5684159A (en) * 1995-05-30 1997-11-04 Rhone-Poulenc Rorer S.A. L-tartaric acid salt of a (1R) diastereomer of a 2-azadihydroxybicyclo 2.2.1!heptane compound and the preparation of 2-azabicyclo 2.2.1!heptane compounds
IN187238B (en) * 1995-06-30 2002-03-09 Astra Ab
WO2017165878A1 (en) * 2016-03-25 2017-09-28 The United States Of America, As Represented By The Secretary, Department Of Health And Human Services Crystal forms and methods of synthesis of (2r, 6r)-hydroxynorketamine and (2s, 6s)-hydroxynorketamine

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2528267A (en) * 1950-10-31 Eobeet j
US3116332A (en) * 1958-10-17 1963-12-31 Du Pont Resolution of racemic aminoisopropanol

Also Published As

Publication number Publication date
JPS51118711A (en) 1976-10-18
GB1470030A (en) 1977-04-14
FR2303790B1 (en) 1980-07-18
FR2303790A1 (en) 1976-10-08
NL7513818A (en) 1976-06-15
SE435499B (en) 1984-10-01
DE2556040A1 (en) 1976-06-16
AU510799B2 (en) 1980-07-17
FR2294151B1 (en) 1979-04-06
DE2556040C2 (en) 1986-05-07
DK532575A (en) 1976-06-14
CA1064943A (en) 1979-10-23
FR2294151A1 (en) 1976-07-09
IE42206L (en) 1976-06-13
IE42206B1 (en) 1980-06-18
AU8722075A (en) 1977-06-09

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