RU99109172A - METHOD OF ISOLATION OF CERIUM (+4) FROM NITROGEN-SOLID SOLUTION OF RARE-EARTH ELEMENTS - Google Patents

METHOD OF ISOLATION OF CERIUM (+4) FROM NITROGEN-SOLID SOLUTION OF RARE-EARTH ELEMENTS

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Publication number
RU99109172A
RU99109172A RU99109172/12A RU99109172A RU99109172A RU 99109172 A RU99109172 A RU 99109172A RU 99109172/12 A RU99109172/12 A RU 99109172/12A RU 99109172 A RU99109172 A RU 99109172A RU 99109172 A RU99109172 A RU 99109172A
Authority
RU
Russia
Prior art keywords
cerium
rare
earth elements
isolation
nitrogen
Prior art date
Application number
RU99109172/12A
Other languages
Russian (ru)
Other versions
RU2162821C2 (en
Inventor
Валерий Дмитриевич Косынкин
Лидия Алексеевна Аржаткина
Рудольф Михайлович Щелков
Евгений Николаевич Иванов
Михаил Георгиевич Штуца
Владимир Викторович Соловьев
Александр Иванович Грабко
Александр Викторович Кардаполов
Original Assignee
Всероссийский научно-исследовательский институт химической технологии
ОАО "Чепецкий механический завод"
Filing date
Publication date
Application filed by Всероссийский научно-исследовательский институт химической технологии, ОАО "Чепецкий механический завод" filed Critical Всероссийский научно-исследовательский институт химической технологии
Priority to RU99109172/12A priority Critical patent/RU2162821C2/en
Priority claimed from RU99109172/12A external-priority patent/RU2162821C2/en
Application granted granted Critical
Publication of RU2162821C2 publication Critical patent/RU2162821C2/en
Publication of RU99109172A publication Critical patent/RU99109172A/en

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Claims (1)

Способ выделения церия (+4) из азотнокислого раствора редкоземельных элементов, включающий введение реагента, осаждение церийсодержащего соединения и его последующее отделение, отличающийся тем, что в качестве реагента используют воду, взятую в количестве, отвечающем соотношению:
Figure 00000001

где [Н] исх., [Ce(+4)]исх. - численные значения концентраций свободной азотной кислоты и церия в исходном растворе, выраженных в м/л; Vисх., Vдоб. - численные значения объемов исходного раствора и введенной воды, выраженных в л, причем осаждение проводят из полученного раствора при температуре 70-100oC в течение не менее 30 мин.
A method of extracting cerium (+4) from a nitrate solution of rare-earth elements, including the introduction of a reagent, the precipitation of a cerium-containing compound and its subsequent separation, characterized in that water is used as a reagent in an amount corresponding to
Figure 00000001

where [H] ref. , [Ce (+4)] ref. - the numerical values of the concentrations of free nitric acid and cerium in the initial solution, expressed in m / l; V out V ext - the numerical values of the volumes of the initial solution and the introduced water, expressed in liters, and the precipitation is carried out from the resulting solution at a temperature of 70-100 o C for at least 30 minutes.
RU99109172/12A 1999-05-05 1999-05-05 Method of recovery of cerium (+4) from nitrate solution of rare-earth elements RU2162821C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU99109172/12A RU2162821C2 (en) 1999-05-05 1999-05-05 Method of recovery of cerium (+4) from nitrate solution of rare-earth elements

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU99109172/12A RU2162821C2 (en) 1999-05-05 1999-05-05 Method of recovery of cerium (+4) from nitrate solution of rare-earth elements

Publications (2)

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RU2162821C2 RU2162821C2 (en) 2001-02-10
RU99109172A true RU99109172A (en) 2001-05-10

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2495147C9 (en) * 2012-09-13 2013-12-10 Открытое акционерное общество "Нижнекамскнефтехим" Cerium extraction method
RU2563015C2 (en) * 2014-01-30 2015-09-10 Общество с ограниченной ответственностью "Научно-производственная компания "Русредмет"(ООО НПК"Русредмет") Method of extraction of cerium from nitrate solutions containing sum of rare-earth elements
RU2646416C2 (en) * 2016-07-18 2018-03-05 Федеральное государственное унитарное предприятие "Институт химических реактивов и особо чистых химических веществ Национального исследовательского центра "Курчатовский институт" (НИЦ "Курчатовский институт"-ИРЕА) Method for obtaining of high-clean cerium (iii) nitrate solution

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