RU94002793A - Method for extraction of dihydroquercitrol - Google Patents

Method for extraction of dihydroquercitrol

Info

Publication number
RU94002793A
RU94002793A RU94002793/14A RU94002793A RU94002793A RU 94002793 A RU94002793 A RU 94002793A RU 94002793/14 A RU94002793/14 A RU 94002793/14A RU 94002793 A RU94002793 A RU 94002793A RU 94002793 A RU94002793 A RU 94002793A
Authority
RU
Russia
Prior art keywords
water
dihydroquercitrol
extraction
acetone
wood
Prior art date
Application number
RU94002793/14A
Other languages
Russian (ru)
Other versions
RU2038094C1 (en
Inventor
Н.А. Тюкавкина
В.В. Наумов
Ю.А. Колесник
И.А. Руленко
В.Е. Ручкин
Т.Ф. Гаврилова
О.В. Наумов
Original Assignee
Товарищество с ограниченной ответственностью "Инкор"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Товарищество с ограниченной ответственностью "Инкор" filed Critical Товарищество с ограниченной ответственностью "Инкор"
Priority to RU94002793A priority Critical patent/RU2038094C1/en
Application granted granted Critical
Publication of RU2038094C1 publication Critical patent/RU2038094C1/en
Publication of RU94002793A publication Critical patent/RU94002793A/en

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  • Extraction Or Liquid Replacement (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Unknown Constitution (AREA)

Abstract

FIELD: medicine; methods for extraction of dihydroquercitrol from larch wood. SUBSTANCE: method for extraction of dihydroquercitrol includes extraction of the product from crushed larch wood washed with water at ambient temperature by means of mixture of water and acetone in mass ratio of 1:4. Acetone is driven off from the extract and sediments of dihydroquercitrol precipitated from the extract aqueous part is separated by centrifuging and recrystallized from hot water. The offered method allows exclusion of the process with application of polyamide sorbent, and, consequently, sorption stage, desorption and sorbent regeneration; selective extraction of dihydroquercitrol with water-acetone mixture without heating from crushed wood preliminarily washed with water that results in increase of finished product yield with its high purity. EFFECT: simplified process for extraction of dihydroquercitrol and increased yield of finished product with preservation of high degree of purity.

Claims (1)

Изобретение относится к медицине и касается способа выделения дигидрокверцетина (ДКВ) из древесины лиственницы. Целью изобретения является упрощение процесса выделения ДКВ и повышение выхода целевого продукта при сохранении высокой степени чистоты. Это достигается тем, что промытую водой измельченную древесину лиственницы экстрагируют при обычной температуре смесью воды и ацетона 1:4 вес.ч. От экстракта отгоняют ацетон, а выпавший из водной части экстракта осадок ДКВ отделяют центрифугированием и перекристаллизовывают из горячей воды. Применение данного способа выделения ДКВ из древесины лиственницы позволяет исключить из технологического процесса применение полиамидного сорбента и следовательно стадии сорбции, десорбции и регенерации сорбента, избирательно экстрагировать ДКВ водно-ацетоновой смесью без нагревания из предварительно промытой водой измельченной древесины, что приводит к повышению выхода целевого продукта при сохранении степени чистоты продукта.The invention relates to medicine and relates to a method for the isolation of dihydroquercetin (DHQ) from larch wood. The aim of the invention is to simplify the process of separation of DHQ and increase the yield of the target product while maintaining a high degree of purity. This is achieved by the fact that water-washed crushed larch wood is extracted at normal temperature with a mixture of water and acetone 1: 4 parts by weight Acetone is distilled off from the extract, and the DKW precipitate that has precipitated from the aqueous portion of the extract is separated by centrifugation and recrystallized from hot water. The use of this method for the isolation of DHQ from larch wood eliminates the use of a polyamide sorbent from the technological process and, therefore, the stage of sorption, desorption and regeneration of the sorbent, selectively extracts DHQ with an aqueous-acetone mixture without heating chopped wood from pre-washed water, which leads to an increase in the yield of the target product when maintaining the degree of purity of the product.
RU94002793A 1994-02-08 1994-02-08 Method for producing dihydroquercetin RU2038094C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU94002793A RU2038094C1 (en) 1994-02-08 1994-02-08 Method for producing dihydroquercetin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU94002793A RU2038094C1 (en) 1994-02-08 1994-02-08 Method for producing dihydroquercetin

Publications (2)

Publication Number Publication Date
RU2038094C1 RU2038094C1 (en) 1995-06-27
RU94002793A true RU94002793A (en) 1996-07-10

Family

ID=20151804

Family Applications (1)

Application Number Title Priority Date Filing Date
RU94002793A RU2038094C1 (en) 1994-02-08 1994-02-08 Method for producing dihydroquercetin

Country Status (1)

Country Link
RU (1) RU2038094C1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2135510C1 (en) * 1998-12-21 1999-08-27 Общество с ограниченной ответственностью "ПлУГ" Method and installation for processing larch wood
LT6013B (en) 2012-05-18 2014-03-25 Uab "Rokiå Kio Pragiedruliai" Process for preparing dihydroquercetin of a particularly high degree of purity

Also Published As

Publication number Publication date
RU2038094C1 (en) 1995-06-27

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