RU2657418C2 - Способ определения температуры склеивания полимера - Google Patents
Способ определения температуры склеивания полимера Download PDFInfo
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- RU2657418C2 RU2657418C2 RU2015112331A RU2015112331A RU2657418C2 RU 2657418 C2 RU2657418 C2 RU 2657418C2 RU 2015112331 A RU2015112331 A RU 2015112331A RU 2015112331 A RU2015112331 A RU 2015112331A RU 2657418 C2 RU2657418 C2 RU 2657418C2
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- reactor
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- polymerization
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- JFNLZVQOOSMTJK-KNVOCYPGSA-N norbornene Chemical compound C1[C@@H]2CC[C@H]1C=C2 JFNLZVQOOSMTJK-KNVOCYPGSA-N 0.000 description 1
- 150000002848 norbornenes Chemical class 0.000 description 1
- 238000006384 oligomerization reaction Methods 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N phosphine group Chemical group P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 1
- 229920001084 poly(chloroprene) Polymers 0.000 description 1
- 229920002857 polybutadiene Polymers 0.000 description 1
- 150000004291 polyenes Chemical class 0.000 description 1
- 229920001195 polyisoprene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- PUDIUYLPXJFUGB-UHFFFAOYSA-N praseodymium atom Chemical compound [Pr] PUDIUYLPXJFUGB-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000012262 resinous product Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- VOITXYVAKOUIBA-UHFFFAOYSA-N triethylaluminium Chemical compound CC[Al](CC)CC VOITXYVAKOUIBA-UHFFFAOYSA-N 0.000 description 1
- ORYGRKHDLWYTKX-UHFFFAOYSA-N trihexylalumane Chemical compound CCCCCC[Al](CCCCCC)CCCCCC ORYGRKHDLWYTKX-UHFFFAOYSA-N 0.000 description 1
- MCULRUJILOGHCJ-UHFFFAOYSA-N triisobutylaluminium Chemical compound CC(C)C[Al](CC(C)C)CC(C)C MCULRUJILOGHCJ-UHFFFAOYSA-N 0.000 description 1
- JLTRXTDYQLMHGR-UHFFFAOYSA-N trimethylaluminium Chemical compound C[Al](C)C JLTRXTDYQLMHGR-UHFFFAOYSA-N 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- HEPBQSXQJMTVFI-UHFFFAOYSA-N zinc;butane Chemical compound [Zn+2].CCC[CH2-].CCC[CH2-] HEPBQSXQJMTVFI-UHFFFAOYSA-N 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/14—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by using rotary bodies, e.g. vane
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N19/00—Investigating materials by mechanical methods
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
- G01N3/22—Investigating strength properties of solid materials by application of mechanical stress by applying steady torsional forces
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/44—Resins; Plastics; Rubber; Leather
- G01N33/442—Resins; Plastics
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2430/00—Assays, e.g. immunoassays or enzyme assays, involving synthetic organic compounds as analytes
- G01N2430/60—Synthetic polymers other than synthetic polypeptides as analytes
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Immunology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Adhesives Or Adhesive Processes (AREA)
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| US201261698286P | 2012-09-07 | 2012-09-07 | |
| US61/698,286 | 2012-09-07 | ||
| PCT/US2013/058002 WO2014039522A1 (en) | 2012-09-07 | 2013-09-04 | A method for determining a stickiness temperature of a resin |
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| RU2015112331A RU2015112331A (ru) | 2016-10-27 |
| RU2657418C2 true RU2657418C2 (ru) | 2018-06-13 |
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| IN (1) | IN2015DN01316A (https=) |
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| WO (1) | WO2014039522A1 (https=) |
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| US20140202204A1 (en) * | 2013-01-22 | 2014-07-24 | Air Liquide Large Industries U.S. Lp | Reactor liquid cooldown method |
| BR112017010747B1 (pt) * | 2014-11-25 | 2021-11-16 | Univation Technologies, Llc | Métodos de controle de índice de fusão de poliolefina |
| CN107018663A (zh) * | 2014-11-25 | 2017-08-04 | 尤尼威蒂恩技术有限责任公司 | 用诱导冷凝剂的组成改变聚烯烃生产速率的方法 |
| WO2017102958A1 (en) | 2015-12-17 | 2017-06-22 | Total Research & Technology Feluy | Process for determining one or more operating conditions of an olefin polymerization reactor |
| WO2020190511A1 (en) | 2019-03-21 | 2020-09-24 | Exxonmobil Chemical Patents Inc. | Methods for improving production in gas phase polymerization |
| US12202917B2 (en) | 2019-03-21 | 2025-01-21 | Exxonmobil Chemical Patents Inc. | Methods for improving gas phase polymerization |
| CN112414898B (zh) * | 2020-11-10 | 2021-12-21 | 中国农业科学院农产品加工研究所 | 复合粉体混合均匀度的评价方法 |
| CN116413382A (zh) * | 2021-12-29 | 2023-07-11 | 中国石油天然气股份有限公司 | 一种乙烯聚合评价试验装置的评价方法 |
| US20250206859A1 (en) | 2022-03-31 | 2025-06-26 | Exxonmobil Chemical Patents Inc. | Linear low density polyethylenes, polymerizations thereof, and films thereof |
| CN119768442A (zh) | 2022-08-22 | 2025-04-04 | 埃克森美孚化学专利公司 | 聚乙烯组合物和由其制备的膜 |
| CN119855843A (zh) | 2022-09-07 | 2025-04-18 | 埃克森美孚化学专利公司 | 聚乙烯及其制品 |
| WO2025250307A1 (en) | 2024-05-30 | 2025-12-04 | ExxonMobil Technology and Engineering Company | Methods for improving gas phase polymerization |
| WO2026024387A1 (en) | 2024-07-22 | 2026-01-29 | ExxonMobil Technology and Engineering Company | Polyethylene sealing layer resins |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008030294A1 (en) * | 2006-09-07 | 2008-03-13 | Univation Technologies, Llc | Methods for on-line determination of degree of resin stickiness using a model for depression of melt initiation temperature |
| US7683140B2 (en) * | 2004-05-20 | 2010-03-23 | Univation Technologies, Llc | Method for determining temperature value indicative of resin stickiness from data generated by polymerization reaction monitoring |
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| US4588790A (en) | 1982-03-24 | 1986-05-13 | Union Carbide Corporation | Method for fluidized bed polymerization |
| US4543399A (en) | 1982-03-24 | 1985-09-24 | Union Carbide Corporation | Fluidized bed reaction systems |
| NZ235032A (en) | 1989-08-31 | 1993-04-28 | Dow Chemical Co | Constrained geometry complexes of titanium, zirconium or hafnium comprising a substituted cyclopentadiene ligand; use as olefin polymerisation catalyst component |
| US5026798A (en) | 1989-09-13 | 1991-06-25 | Exxon Chemical Patents Inc. | Process for producing crystalline poly-α-olefins with a monocyclopentadienyl transition metal catalyst system |
| US5436304A (en) | 1992-03-19 | 1995-07-25 | Exxon Chemical Patents Inc. | Process for polymerizing monomers in fluidized beds |
| US5352749A (en) | 1992-03-19 | 1994-10-04 | Exxon Chemical Patents, Inc. | Process for polymerizing monomers in fluidized beds |
| JP3077940B2 (ja) | 1993-04-26 | 2000-08-21 | エクソン・ケミカル・パテンツ・インク | 流動層重合法のための安定な操作条件を決定する方法 |
| US5342907A (en) * | 1993-06-28 | 1994-08-30 | Union Carbide Chemicals & Plastics Technology Corporation | Ethylene/propylene copolymer rubbers |
| US5747406A (en) | 1997-01-10 | 1998-05-05 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for the production of olefin polymers |
| US6242545B1 (en) | 1997-12-08 | 2001-06-05 | Univation Technologies | Polymerization catalyst systems comprising substituted hafinocenes |
| US6069213A (en) | 1997-12-16 | 2000-05-30 | Union Carbide Chemicals & Plastics Technology Corporation | Mixed catalyst system |
| US6894131B2 (en) | 1998-08-21 | 2005-05-17 | Univation Technologies, Llc | Polymerization process using a metallocene catalyst system |
| JP2001255251A (ja) * | 2000-03-13 | 2001-09-21 | Sumitomo Bakelite Co Ltd | フェノール樹脂成形材料の流動性評価方法 |
| US7226789B2 (en) | 2001-12-17 | 2007-06-05 | Unication Technolofies, Llc | Method of applying non-linear dynamics to control a gas-phase polyethylene reactor operability |
| ATE503779T1 (de) * | 2001-12-20 | 2011-04-15 | Union Carbide Chem Plastic | Polyolefinherstellungsverfahren in einem fliessbettreaktor unter turbulenten bedingungen und unter kondensation des rückfuhrstroms |
| US6846884B2 (en) | 2002-09-27 | 2005-01-25 | Union Carbide Chemicals & Plastics Technology Corporation | Control of resin properties |
| CA2501528A1 (en) | 2002-10-15 | 2004-04-15 | Exxonmobil Chemical Patents Inc. | On-line measurement and control of polymer properties by raman spectroscopy |
| US7244795B2 (en) | 2003-12-08 | 2007-07-17 | Univation Technologies, Llc | Polymerization process using metallocene catalyst systems |
| US7410926B2 (en) | 2003-12-30 | 2008-08-12 | Univation Technologies, Llc | Polymerization process using a supported, treated catalyst system |
| AU2005245921B2 (en) | 2004-05-20 | 2007-11-15 | Univation Technologies, Llc | Gas olefin polymerization process |
| US7459510B2 (en) | 2004-06-21 | 2008-12-02 | Exxonmobil Chemical Patents Inc. | Polymerization process |
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| CN2852109Y (zh) * | 2005-12-29 | 2006-12-27 | 华东理工大学 | 高温高压旋转粘度计 |
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| US7683140B2 (en) * | 2004-05-20 | 2010-03-23 | Univation Technologies, Llc | Method for determining temperature value indicative of resin stickiness from data generated by polymerization reaction monitoring |
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Also Published As
| Publication number | Publication date |
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| RU2015112331A (ru) | 2016-10-27 |
| EP2893342B1 (en) | 2022-04-27 |
| EP3968020B1 (en) | 2024-07-24 |
| EP2893342A1 (en) | 2015-07-15 |
| US20180326386A1 (en) | 2018-11-15 |
| CN104603615A (zh) | 2015-05-06 |
| BR112015004883B1 (pt) | 2021-11-09 |
| EP3968020A1 (en) | 2022-03-16 |
| CN108106968A (zh) | 2018-06-01 |
| ES2987855T3 (es) | 2024-11-18 |
| WO2014039522A1 (en) | 2014-03-13 |
| IN2015DN01316A (https=) | 2015-07-03 |
| BR112015004883A2 (pt) | 2017-07-04 |
| US10029226B2 (en) | 2018-07-24 |
| US20150209751A1 (en) | 2015-07-30 |
| CN108106968B (zh) | 2020-09-25 |
| ES2914610T3 (es) | 2022-06-14 |
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