RU2655093C2 - Method of obtaining an integrated additive for concrete - Google Patents

Method of obtaining an integrated additive for concrete Download PDF

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Publication number
RU2655093C2
RU2655093C2 RU2016128120A RU2016128120A RU2655093C2 RU 2655093 C2 RU2655093 C2 RU 2655093C2 RU 2016128120 A RU2016128120 A RU 2016128120A RU 2016128120 A RU2016128120 A RU 2016128120A RU 2655093 C2 RU2655093 C2 RU 2655093C2
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RU
Russia
Prior art keywords
concrete
mixture
following components
mixing
obtaining
Prior art date
Application number
RU2016128120A
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Russian (ru)
Inventor
Татьяна Григорьевна Ветренко
Александр Мартынович Прищеп
Юлия Алексеевна Щепочкина
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Общество с ограниченной ответственностью "Прогресс"
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Priority to RU2016128120A priority Critical patent/RU2655093C2/en
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Publication of RU2655093C2 publication Critical patent/RU2655093C2/en

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B22/00Use of inorganic materials as active ingredients for mortars, concrete or artificial stone, e.g. accelerators, shrinkage compensating agents
    • C04B22/08Acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B22/00Use of inorganic materials as active ingredients for mortars, concrete or artificial stone, e.g. accelerators, shrinkage compensating agents
    • C04B22/08Acids or salts thereof
    • C04B22/085Acids or salts thereof containing nitrogen in the anion, e.g. nitrites
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/12Nitrogen containing compounds organic derivatives of hydrazine
    • C04B24/121Amines, polyamines
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

FIELD: construction.
SUBSTANCE: method for producing a complex additive for concrete, which involves successively dissolving in 700 ml of water the following components: soda ash 1 g, sodium metasilicate 0.8 g, sodium nitrite 2 grams, bactericide 2 ml, preparation of a mixture of the following components: triethanolamine 500 ml, diethanolamine 100 ml, synthamide-5 100 ml, kerosene 5 ml, industrial oil I-20A 2 ml, compound of the solution and mixture, and then mixing them.
EFFECT: increasing the concrete strength.
1 cl

Description

Изобретение касается способов получения комплексных добавок для цементных бетонов. The invention relates to methods for complex additives for cement concrete.

Известен способ получения добавки для бетона, предусматривающий приготовление двух растворов, одного путем смешивания суперпластификатора на основе нафталин- или меламинсульфокислоты, ЛСТ, пеногасителя и биоцида с водой, нагретой до температуры 50°С, и другого путем смешивания нитрата кальция с водой, нагретой до температуры 70-75°С, смешивание указанных растворов с введением при этом гидроксида калия [1].A known method of producing additives for concrete, providing for the preparation of two solutions, one by mixing a superplasticizer based on naphthalene or melamine sulfonic acid, LST, antifoam and biocide with water heated to a temperature of 50 ° C, and the other by mixing calcium nitrate with water heated to a temperature 70-75 ° C, mixing these solutions with the introduction of potassium hydroxide [1].

Задачей изобретения является упрощение технологии получения комплексной добавки, повышение прочности цементного бетона.The objective of the invention is to simplify the technology for complex additives, increasing the strength of cement concrete.

Технический результат достигается тем, что способ получения комплексной добавки для бетона предусматривает последовательное растворение в 700 мл воды следующих компонентов: сода кальцинированная 1 г; метасиликат натрия 0,8 г; нитрит натрия 2 г; бакцид 2 мл, приготовление смеси следующих компонентов: триэтаноламин 500 мл; диэтаноламин 110 мл; синтамид-5 100 мл; керосин 5 мл; масло индустриальное И-20А 2 мл, соединение раствора и смеси с последующим их смешиванием.The technical result is achieved by the fact that the method of obtaining a complex additive for concrete involves the sequential dissolution in 700 ml of water of the following components: soda ash 1 g; sodium metasilicate 0.8 g; sodium nitrite 2 g; 2 ml bacterium, preparation of a mixture of the following components: triethanolamine 500 ml; diethanolamine 110 ml; syntamide-5 100 ml; kerosene 5 ml; industrial oil I-20A 2 ml, the connection of the solution and the mixture, followed by mixing.

Комплексную добавку для бетона получают следующим образом.A comprehensive additive for concrete is prepared as follows.

1. В отдельную емкость наливают 700 мл воды, в которой последовательно растворяют следующие компоненты: сода кальцинированная 1 г; метасиликат натрия 0,8 г; нитрит натрия 2 г; бакцид 2 мл. Для маскировки неприятного запаха комплексной добавки в раствор дополнительно может быть введено 0,5 г ароматизатора (например, синтетического ванилина).1. Pour 700 ml of water into a separate container, in which the following components are successively dissolved: soda ash 1 g; sodium metasilicate 0.8 g; sodium nitrite 2 g; bacterium 2 ml. To mask the unpleasant odor of the complex additive, an additional 0.5 g of flavoring agent (for example, synthetic vanillin) can be added to the solution.

2. В отдельной емкости смешивают следующие компоненты: триэтаноламин 500 мл; диэтаноламин 110 мл; синтамид-5 100 мл; керосин 5 мл; масло индустриальное И-20А 2 мл.2. The following components are mixed in a separate container: triethanolamine 500 ml; diethanolamine 110 ml; syntamide-5 100 ml; kerosene 5 ml; industrial oil I-20A 2 ml.

3. Осуществляют соединение раствора и смеси с последующим их смешиванием.3. Carry out the connection of the solution and the mixture, followed by mixing.

Полученную комплексную добавку фасуют, например, в стеклянную тару, перед употреблением содержимое перемешивают. При приготовлении бетонной смеси расход добавки составляет 0,3-1% от массы цемента. Добавку вводят в бетонную смесь с частью (10-20 об.%) воды затворения за 2-5 мин до окончания перемешивания. Использование добавки позволяет обеспечить подвижность бетонных смесей (осадка конуса 2,5 см при водоцементном отношении 0,36) и повысить прочность цементного бетона на сжатие на 15-30%.The resulting complex additive is Packed, for example, in a glass container, the contents are mixed before use. When preparing a concrete mixture, the consumption of additives is 0.3-1% by weight of cement. The additive is introduced into the concrete mixture with a portion (10-20 vol.%) Of mixing water 2-5 minutes before the end of mixing. The use of additives allows to ensure the mobility of concrete mixtures (cone sediment 2.5 cm at a water-cement ratio of 0.36) and increase the compressive strength of cement concrete by 15-30%.

Источники информацииInformation sources

1. RU 2320600 С2, 2008.1. RU 2320600 C2, 2008.

Claims (1)

Способ получения комплексной добавки для бетона, предусматривающий последовательное растворение в 700 мл воды следующих компонентов: сода кальцинированная 1 г, метасиликат натрия 0,8 г, нитрит натрия 2 г, бакцид 2 мл, приготовление смеси следующих компонентов: триэтаноламин 500 мл, диэтаноламин 110 мл, синтамид-5 100 мл, керосин 5 мл, масло индустриальное И-20А 2 мл, соединение раствора и смеси с последующим их смешиванием.A method of obtaining a complex additive for concrete, which involves the sequential dissolution in 700 ml of water of the following components: soda ash 1 g, sodium metasilicate 0.8 g, sodium nitrite 2 g, bacterium 2 ml, preparation of a mixture of the following components: triethanolamine 500 ml, diethanolamine 110 ml , syntamide-5 100 ml, kerosene 5 ml, industrial oil I-20A 2 ml, the compound of the solution and mixture, followed by mixing.
RU2016128120A 2016-07-12 2016-07-12 Method of obtaining an integrated additive for concrete RU2655093C2 (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996010477A1 (en) * 1994-10-04 1996-04-11 E. Khashoggi Industries Placing filaments within extruded hydraulically settable compositions
RU2320600C2 (en) * 2006-04-27 2008-03-27 Михаил Ефимович Цельнер Additive for concrete and mortars and method of preparation of such additive
RU2467968C1 (en) * 2011-03-14 2012-11-27 Роман Ринатович Сахибгареев Complex additive for concrete, mortar and cement composites (versions) and method of producing said additive
RU2527442C1 (en) * 2012-12-26 2014-08-27 Открытое акционерное общество "Полипласт" (ОАО "Полипласт") Complex additive
RU2528330C2 (en) * 2012-12-13 2014-09-10 Открытое акционерное общество "Полипласт" (ОАО "Полипласт") Complex additive for concretes

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996010477A1 (en) * 1994-10-04 1996-04-11 E. Khashoggi Industries Placing filaments within extruded hydraulically settable compositions
RU2320600C2 (en) * 2006-04-27 2008-03-27 Михаил Ефимович Цельнер Additive for concrete and mortars and method of preparation of such additive
RU2467968C1 (en) * 2011-03-14 2012-11-27 Роман Ринатович Сахибгареев Complex additive for concrete, mortar and cement composites (versions) and method of producing said additive
RU2528330C2 (en) * 2012-12-13 2014-09-10 Открытое акционерное общество "Полипласт" (ОАО "Полипласт") Complex additive for concretes
RU2527442C1 (en) * 2012-12-26 2014-08-27 Открытое акционерное общество "Полипласт" (ОАО "Полипласт") Complex additive

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Effective date: 20180713