CN104402286B - A kind of concrete early strength agent and preparation method thereof - Google Patents

A kind of concrete early strength agent and preparation method thereof Download PDF

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Publication number
CN104402286B
CN104402286B CN201410633020.2A CN201410633020A CN104402286B CN 104402286 B CN104402286 B CN 104402286B CN 201410633020 A CN201410633020 A CN 201410633020A CN 104402286 B CN104402286 B CN 104402286B
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China
Prior art keywords
parts
raw material
early strength
strength agent
sulfate
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Expired - Fee Related
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CN201410633020.2A
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Chinese (zh)
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CN104402286A (en
Inventor
杨传长
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Guangzhou engineering Chemicals Co., Ltd.
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Anhui Chuangye Mechanical & Electrical Equipment Co Ltd
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Priority to CN201410633020.2A priority Critical patent/CN104402286B/en
Publication of CN104402286A publication Critical patent/CN104402286A/en
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Publication of CN104402286B publication Critical patent/CN104402286B/en
Expired - Fee Related legal-status Critical Current
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Abstract

A kind of concrete early strength agent and preparation method thereof, relate to industrial chemicals technical field, carried out after rational proportioning formula carries out hybrid process, preparing after drying granulation by aluminum sulfate, gypsum, sulfate, sodium carbonate, slag powders, triethanolamine, potassium hydroxide, flyash, ammonium chloride, calcium silicates and water.The invention has the beneficial effects as follows: the present invention prepares convenient and simple, environment friendly and pollution-free, raw material is easy to get, and equipment investment is few, it is simple to operation, and the concrete early strength agent using effect of preparation is good, and ability of derusting is strong, and no side effects is safe and reliable.

Description

A kind of concrete early strength agent and preparation method thereof
Technical field
The present invention relates to industrial chemicals technical field, be specifically related to a kind of concrete early strength agent and preparation side thereof Method.
Background technology
Concrete early strength agent is one of concrete admixture, and concrete early strength agent refers to improve concrete early Phase intensity, and the additive that later strength is not made significant difference.The Main Function of early strength agent is to accelerate Hydrated cementitious speed, promotes the development of early strength on coagulation;Both there is early powerful, had again certain The additive of water reducing and strength increasing function is referred to as early strength water-reducing agent, but metal-derusting present on current market produces Product are a feast for the eyes, but, what a kind of concrete early strength agent can be real plays obvious effect, But also corresponding toxicity can be there is, affect health.
Summary of the invention
The technical problem to be solved is to provide a kind of intensity high, condenses fast concrete the strongest Agent and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions:
A kind of concrete early strength agent, it is characterised in that: include the raw material composition of following weight portion,
Aluminum sulfate 5-7 part, gypsum 25-35 part, sulfate 3-5 part, sodium carbonate 6-8 part, slag powders 15-25 Part, triethanolamine 2-4 part, potassium hydroxide 5-7 part, flyash 20-30 part, ammonium chloride 4-6 part, silicic acid Calcium 7-9 part, deionized water 30-40 part;
Preferred weight part of each raw material is: 6 parts of aluminum sulfate, gypsum 30 parts, 4 parts of sulfate, sodium carbonate 7 Part, slag powders 20 parts, triethanolamine 3 parts, 6 parts of potassium hydroxide, 25 parts of flyash, ammonium chloride 5 parts, silicon Acid calcium 8 parts, deionized water 35 parts;
It is another object of the present invention to prepare the method for concrete early strength agent in the present invention, it is characterised in that: Comprise the following steps:
A, select a reactor, in the deionized water of half adds reactor in raw material, then by raw material In aluminum sulfate, sulfate, sodium carbonate, triethanolamine and potassium hydroxide be added thereto, add unlatching stirring, It is heated to 20-30 DEG C so that it is after being completely dissolved, pours out;
B, select an agitator tank, the residue deionized water in raw material is added thereto, the most again by raw material Ammonium chloride and calcium silicates, stirring is until after ammonium chloride and calcium silicates all dissolve, obtaining solution A, standby;
C, the solution poured out in material A and step a is sufficiently mixed after, stir, then by former In material, gypsum, slag powders and flyash are ground into foam, are added in agitator tank, after being then sufficiently stirred for, Carry out drying granulation, pack after filtration.
The invention has the beneficial effects as follows: the present invention prepares convenient and simple, environment friendly and pollution-free, raw material is easy to get, Equipment investment is few, it is simple to operation, and the concrete early strength agent using effect of preparation is good, and using effect is obvious, No side effects, safe and reliable.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of concrete early strength agent, the raw material including following weight portion forms,
Aluminum sulfate 5kg, gypsum 25kg, sulfate 3kg, sodium carbonate 6kg, slag powders 15kg, three ethanol Amine 2kg, potassium hydroxide 5kg, flyash 20kg, ammonium chloride 4kg, calcium silicates 7kg, deionized water 30kg;
It is another object of the present invention to prepare the method for concrete early strength agent in the present invention, comprise the following steps:
A, select a reactor, in the deionized water of half adds reactor in raw material, then by raw material In aluminum sulfate, sulfate, sodium carbonate, triethanolamine and potassium hydroxide be added thereto, add unlatching stirring, It is heated to 20-30 DEG C so that it is after being completely dissolved, pours out;
B, select an agitator tank, the residue deionized water in raw material is added thereto, the most again by raw material Ammonium chloride and calcium silicates, stirring is until after ammonium chloride and calcium silicates all dissolve, obtaining solution A, standby;
C, the solution poured out in material A and step a is sufficiently mixed after, stir, then by former In material, gypsum, slag powders and flyash are ground into foam, are added in agitator tank, after being then sufficiently stirred for, Carry out drying granulation, pack after filtration.
Embodiment 2
A kind of concrete early strength agent, the raw material including following weight portion forms: aluminum sulfate 6kg, gypsum 30kg, sulfate 4kg, sodium carbonate 7kg, slag powders 20kg, triethanolamine 3kg, potassium hydroxide 6kg, Flyash 25kg, ammonium chloride 5kg, calcium silicates 8kg, deionized water 35kg;
It is another object of the present invention to prepare the method for concrete early strength agent in the present invention, comprise the following steps:
A, select a reactor, in the deionized water of half adds reactor in raw material, then by raw material In aluminum sulfate, sulfate, sodium carbonate, triethanolamine and potassium hydroxide be added thereto, add unlatching stirring, It is heated to 20-30 DEG C so that it is after being completely dissolved, pours out;
B, select an agitator tank, the residue deionized water in raw material is added thereto, the most again by raw material Ammonium chloride and calcium silicates, stirring is until after ammonium chloride and calcium silicates all dissolve, obtaining solution A, standby;
C, the solution poured out in material A and step a is sufficiently mixed after, stir, then by former In material, gypsum, slag powders and flyash are ground into foam, are added in agitator tank, after being then sufficiently stirred for, Carry out drying granulation, pack after filtration.
The general principle of the present invention and principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (2)

1. a concrete early strength agent, it is characterised in that: include the raw material group of following weight portion Become,
Aluminum sulfate 5-7 part, gypsum 25-35 part, sulfate 3-5 part, sodium carbonate 6-8 part, ore deposit Ground-slag 15-25 part, triethanolamine 2-4 part, potassium hydroxide 5-7 part, flyash 20-30 part, chlorine Change ammonium 4-6 part, calcium silicates 7-9 part, deionized water 30-40 part;
The preparation method of described concrete early strength agent is:
A, select a reactor, in the deionized water of half adds reactor in raw material, so After the aluminum sulfate in raw material, sulfate, sodium carbonate, triethanolamine and potassium hydroxide are added it In, add unlatching stirring, be heated to 20-30 DEG C so that it is after being completely dissolved, pour out;
B, select an agitator tank, the residue deionized water in raw material is added thereto, the most again By the ammonium chloride in raw material and calcium silicates, stirring until after ammonium chloride and calcium silicates all dissolve, Obtain solution A, standby;
C, the solution poured out in solution A and step a is sufficiently mixed after, stir, Then gypsum, slag powders and flyash in raw material are ground into foam, are added in agitator tank, Then, after being sufficiently stirred for, carry out drying granulation, pack after filtration.
A kind of concrete early strength agent the most according to claim 1, it is characterised in that: each former Preferred weight part of material is: 6 parts of aluminum sulfate, gypsum 30 parts, 4 parts of sulfate, sodium carbonate 7 Part, slag powders 20 parts, triethanolamine 3 parts, 6 parts of potassium hydroxide, 25 parts of flyash, ammonium chloride 5 parts, calcium silicates 8 parts, deionized water 35 parts.
CN201410633020.2A 2014-11-11 2014-11-11 A kind of concrete early strength agent and preparation method thereof Expired - Fee Related CN104402286B (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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CN104402286A CN104402286A (en) 2015-03-11
CN104402286B true CN104402286B (en) 2016-08-24

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105152574A (en) * 2015-08-25 2015-12-16 建华建材(蚌埠)有限公司 Anti-corrosion anti-cracking early strength agent and preparation method thereof
CN105349126A (en) * 2015-12-10 2016-02-24 成都川锋化学工程有限责任公司 Oil well cement coagulation-accelerating early strength agent and preparation method thereof
CN107162541A (en) * 2017-05-27 2017-09-15 明光市泰丰新材料有限公司 The energy-saving brick and preparation method of a kind of utilization sludge of sewage treatment plant manufacture
CN108439843A (en) * 2018-05-18 2018-08-24 萧县沃德化工科技有限公司 A kind of method and its application synthesizing early strength agent with industrial waste nitric acid

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101200354B (en) * 2007-11-30 2010-06-23 苏州二建建筑集团有限公司 Concrete super instant coagulant
CN101993209A (en) * 2009-08-25 2011-03-30 聂雨淼 Cement concrete early strength agent
CN102079641A (en) * 2009-11-26 2011-06-01 沈阳工业大学 Compound early strength agent for concrete
CN102701626A (en) * 2012-06-25 2012-10-03 南通优尼科化工有限公司 Cement early strength agent
CN103936324B (en) * 2014-04-30 2015-10-21 新昌县镜岭镇康柳电子元件厂 A kind of concrete early strength agent

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Effective date of registration: 20170711

Address after: 327, room 97, 510000 science Avenue, Guangzhou, Luogang District, Guangdong

Patentee after: Guangzhou engineering Chemicals Co., Ltd.

Address before: Yu and the Anhui province Bengbu City Road 233000 No. 15 Hospital No. 1 workshop

Patentee before: ANHUI CHUANGYE MECHANICAL & ELECTRICAL EQUIPMENT CO., LTD.

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