RU2255483C1 - Method for production of pesticide composition (variants) - Google Patents

Abstract

FIELD: agents for biological plant protection.

SUBSTANCE: claimed method includes extraction of biomass of family Mortierella or Pythium micromycete in microwave field with extractant selected from group including lower alcohols, saturated or unsaturated C₁-C₁₀-hydrocarbons optionally substituted with halogen, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixture thereof; extract separation and introducing therein non-active components to produce target product. During this process extraction pressure in extraction mixture is periodically decompressed to provide extractant boiling and elevated again up to starting pressure.

EFFECT: reduced energy consumption; intensified extraction process.

41 cl

Description

The group of inventions relates to the production technology of pesticides with immunostimulating and growth-regulating activity.

A known method of extraction of biological raw materials, which involves mixing it with a liquid extractant, heating the mixture to a temperature of 40-80 ° C, periodically evacuating with a supply of heat to maintain a temperature of 5-15 ° C above the boiling point under vacuum pressure and increasing the pressure to its original value with subsequent separation of the extract (SU 1286232 A1, 01/30/1987).

This method is not suitable for the extraction of thermolabile and easily oxidizable substances, such as polyunsaturated fatty acids. In addition, the disadvantage of this method is the high specific energy consumption due to the low efficiency of using the phase transition energy to destroy the cellular structure of the raw material, which is due to the localization of the boiling zone on the heat-supplying surface.

Closest to the proposed is a method for the production of a pesticidal composition, comprising extracting the biomass of micromycete Mortierella alpina in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen , nitrous oxide, carbon dioxide and mixtures thereof, upon condensation in the extraction mixture of vapors of the extractant, separation of the extract and the introduction of inactive components into it to obtain the target th product (RU 2075934 C1, 27.03.1997).

The disadvantage of this method is the high specific energy consumption due to the low efficiency of using the phase transition energy to destroy the cellular structure of the raw material, which is caused by a fairly uniform distribution of the condensation zones of the gas phase bubbles of the extractant throughout the extraction mixture.

The technical result of the invention is to reduce specific energy consumption.

This result is achieved in that in a method for the production of a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen , nitrous oxide, carbon dioxide and mixtures thereof, separation of the extract and the introduction of inactive components into it to obtain the target product, according to the invention, use the biomass of Pythium micromycete catenulatum, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Pythi micromycete biomass is used um coloratum, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures the boiling of the extractant, and at the same time the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Pythi micromycete biomass is used um gracile, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Pythi micromycete biomass is used um irregulare, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is dropped to a value that ensures boiling of the extractant, and at the same time the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Pythi micromycete biomass is used um ultimum, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Pythi micromycete biomass is used um insidiosum, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Sapro micromycete biomass is used legnia parasitica, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is dropped to a value that ensures boiling of the extractant, and at the same time the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting the biomass of Mortierella alpina micromycete in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives are inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, extraction processing mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella elongata, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella bainieri, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella exigua, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella minutissima, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella verticillata, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella hygrophila, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella polycephala, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella globalpina, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella indohii, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella sepedonioides, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures the boiling of the extractant, and at the same time the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella lignicola, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella humilis, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella alliaceae, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella strangulata, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella pusilla, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella gracilis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella globulifera, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella jenkinii, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella dichotoma, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella sclerotiella, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella zychae, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella marburgensis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separation of the extract and the introduction of inactive components into it to obtain the target product, according to the invention, biomass of micromycete Mo is used rtierella beljakovae, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella sarnyensis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella nigrescens, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella gemmifera, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella reticulata, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value,

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella parvispora, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella pulchella, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella gamsii, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella spinosa, the processing of the extraction mixture by the microwave field is carried out in an oscillating mode, during the exposure of the extraction mixture to the microwave field, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella nantahalensis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The same result is achieved in that in a method for producing a pesticidal composition, which involves extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, according to the invention, Morti micromycete biomass is used erella spinosa var. sterilis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.

The methods are implemented as follows.

The biomass of any of the micromycete species provided for by the process variants is mixed with a liquid extractant selected from the group consisting of lower alcohols, saturated and unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, carbon dioxide and mixtures thereof , with parameters known from traditional technologies (Kasyanov G.I. et al. Processing of plant materials with liquefied and compressed gases. - M .: AgroNIITEIPP, 1993 - 40 s .; Patokina EV, Development of methods for the separation of polyunsaturated x fatty acids from microbiological raw materials. Abstract of a dissertation by a candidate of chemical sciences - M.: MITHT, 1985 - 24 pp.). The listed extractants, as is known, make it possible to recover eicosatetraenoic and eicosapentaenoic acids, which have immunostimulating and growth-regulating activity and serve as the active principle of each target product obtained in this group of inventions. The obtained extraction mixture is treated with a microwave electromagnetic field in an oscillating mode with known parameters (Gubiev YK Scientific and practical principles of heat-technological processes of food production in the electromagnetic field of a microwave. Abstract of thesis, Doctor of Technical Sciences - M .: MTIPP, 1990 - 48 p.). The pressure in the extraction mixture in the process of exposure to it, the microwave field is reset to a value that ensures boiling of the extractant, and increase to the initial value corresponding to the pressure of the saturated vapor of the extractant at the extraction temperature, at the time of termination of the microwave field. The oscillating mode is calculated by the maximum efficiency of low-frequency pressure pulsations according to known dependencies (Lomachinsky V.A. Highly efficient technologies for processing plant materials - M .: Russian Technologies, 1996, pp. 54-56).

As is known, the microwave electromagnetic field, regardless of the type of extractant and the extracted material, leads to uneven heating of the extraction mixture and intensive extraction of polar substances from intercellular capillaries of biological raw materials. In addition, the internal contents of the cells of biological raw materials are heated, which leads to an increase in intracellular pressure and some acceleration of diffusion through cell membranes due to the pressure difference.

When depressurizing to a value that ensures boiling of the extractant, as in the proposed group of inventions, the formation of each bubble of the gas phase or the collapse of each bubble of the gas phase, as in the closest analogue, is accompanied by the creation of a shock wave in the extraction mixture that destroys the cellular structure of the biomass due to shock loads and accumulation of fatigue and thermal stresses. This leads to a constant increase with increasing speed of the contact surface of the phases and a decrease in the diffusion resistance of raw materials, regardless of the choice of extractant and type of biomass.

As is known, the action of shock waves decreases in proportion to the square of the distance from the epicenter, that is, in this case, from the place of formation or collapse of the gas phase bubble in the extraction mixture. The vapor bubbles are condensed by heat exchange with the liquid phase of the extraction mixture; therefore, in the closest analogue, it occurs in the liquid phase at a certain distance from the extracted biomass particles. When depressurizing without external heat supply, which is provided for in the first analogue, solid particles in the extraction mixture serve as vaporization centers and most gas phase bubbles form directly on the surface of biomass particles. It follows from this that the specific energy consumption of shock waves for the destruction of cell membranes of biomass and the entire extraction process, respectively, in the proposed group of inventions will always be less than in each analogue. Moreover, this difference will be the greater, the greater the value of the hydraulic module of the extraction mixture, and does not depend on the type of extracted biomass and the choice of extractant.

With the termination of the microwave field, which is not provided for in the closest analogue, convective flows appear in the extraction mixture that equalize the temperature field. As a result, the biomass is subjected to cooling, which increases the accumulation of thermal stresses in it and further reduces the specific energy consumption of shock waves and the microwave field to destroy the cell membranes of biomass. In addition, the process of updating the contact surface of the phases, intensifying the extraction, is accelerated.

The process of increasing pressure in the extraction mixture that accompanies biomass cooling accelerates the accumulation of fatigue stresses in biomass particles, which reduces the energy expenditure of shock waves on the destruction of biomass cell membranes.

Both of these processes are independent of the choice of extractant and the type of biomass used.

Thus, the specific energy consumption for the destruction of the cellular structure and extraction of biomass in the proposed group of inventions will always be less than in each analogue.

The extract obtained is separated from the meal and inactive components, for example, an antioxidant, a filler, an anti-caking agent and a wetting agent, are introduced into it, as in the closest analogue, to obtain the target product. Other things being equal, its biological effectiveness will be determined solely by the composition of the extract. Since, as shown above, substances with immunostimulating and growth-regulating activity contained in the biomass of each of the micromycete species provided for by the process variants, the extract will be included in the composition, the possibility of using the target product obtained by each method variant for the named purpose will be determined by the composition of the concomitant substances in the extracts, namely the absence in them of substances that inhibit these types of activity. The composition of the extracts is determined by the choice of micromycete biomass and in each of the options provided by this group of inventions differs from the closest analogue, with the exception of the option in which the biomass of micromycete Mortierella alpina is used. The composition of all the extracts turned out to be rather complicated for its complete identification, therefore, the biological effectiveness of all the target products was checked by comparative tests with a reference preparation obtained using the biomass of micromycete Mortierella alpina, as in the closest analogue. Skifyanka wheat and Korolek cucumbers were used as test cultures. The treatment was carried out equal in terms of the total content of eicosatetraenoic and eicosapentaenoic acids in amounts of all preparations.

Wheat treatment was carried out at the pre-sowing stage and during vegetation in the exit phase into the tube at the flow rate of the preparations according to 0.5 mg / t and 0.5 mg / ha, respectively. The relative difference compared with the closest analogue in germination was from +8.1 to -1.9%, in germination energy from +4.6 to -4.1%, in the development of phytopathogens from +4.8 to -5, 1%, yield from +8.5 to -4.2%.

The processing of cucumbers was carried out at the pre-sowing stage and during vegetation in the flowering phase at a flow rate of drugs by AI 1 g / t and 10 mg / ha, respectively. The relative difference compared with the closest analogue in germination was from +3.9 to - 3.7%, in terms of germination energy from +3.3 to -2.7%, in the development of phytopathogens from +4.5 to -6, 7%, in yield from +9.9 to -5.7%.

None of the test cultures showed a correlation between the improvement or deterioration of the processing efficiency indicators as compared with the closest analogue depending on the type of micromycete biomass.

Thus, the proposed group of inventions allows to reduce specific energy consumption.

Claims (41)

1. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Pythium catenulatum is used, the extraction art the microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 2. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the desired product, characterized in that the biomass of micromycete Pythium coloratum is used, microwave field B is carried in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 3. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that they use the biomass of micromycete Pythium gracile, processing the extraction mixture field and the microwave is carried in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 4. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Pythium irregulare is used, processing of extraction cm If the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value. 5. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of Pythium ultimum micromycete is used, processing of the extraction mixture field and the microwave is carried in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 6. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Pythium insidiosum is used, If the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to act on the extraction mixture, the pressure in it increases to the initial value. 7. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Saprolegnia parasitica is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 8. A method of producing a pesticidal composition, comprising extracting the biomass of Mortierella alpina micromycete in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide , carbon dioxide and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the extraction mixture is treated with a microwave field in liruyuschem mode during the extraction mixture influence on the field reset to a value that ensures boiling extractant microwave pressure therein, and simultaneously with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 9. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the desired product, characterized in that the biomass of micromycete Mortierella elongata is used, extraction treatment with Mesi by the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value. 10. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella bainieri is used, extraction treatment impurity microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 11. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella exigua is used, the extraction treatment with art the microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 12. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella minutissima is used, extraction treatment mixtures microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 13. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella verticillata is used, extraction treatment the first mixture by the microwave field is carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 14. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella hygrophila is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 15. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella polycephala is used, extraction treatment mixtures microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 16. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of the micromycete Mortierella globalpina is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 17. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella indohii is used, the extraction treatment with Mesi by the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value. 18. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella sepedonioides is used, extraction treatment th field of microwave mixture is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 19. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella lignicola is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 20. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella humilis is used, the extraction treatment with Mesi by the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value. 21. A method of producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella alliaceae is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 22. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella strangulata is used, extraction treatment mixtures microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 23. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella pusilla is used, the extraction treatment with Mesi by the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value. 24. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella gracilis is used, extraction treatment impurity microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 25. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella globulifera is used, extraction treatment mixtures microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 26. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella jenkinii is used, extraction treatment impurity microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 27. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella dichotoma is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 28. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the desired product, characterized in that the micromycete biomass with Mortierella sclerotiella is used, extraction treatment oh mixtures microwave field carried in oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 29. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella zychae is used, the extraction treatment with art the microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 30. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella marburgensis is used, extraction treatment the first mixture by the microwave field is carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 31. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella beljakovae is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 32. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella sarnyensis is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 33. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella nigrescens is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 34. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella gemmifera, processing extraction mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 35. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella reticulata is used, the extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 36. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella parvispora is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 37. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella pulchella is used, extraction treatment mixtures by the microwave field are carried out in an oscillating mode, during exposure of the microwave field to the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and simultaneously with the termination of the microwave field on the extraction mixture, the pressure in it increases to the initial value. 38. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella gamsii is used, the extraction treatment with art the microwave field is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 39. A method of manufacturing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella spinosa is used, the extraction treatment with Mesi by the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is released to a value that ensures the boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value. 40. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella nantahalensis is used, the extraction th field of microwave mixture is carried out in an oscillating mode, during exposure to a microwave field extraction mixture pressure therein dropping to a value that ensures boiling of the extractant, and concurrently with the termination of the microwave field in the extraction mixture pressure therein is raised to the original value. 41. A method for producing a pesticidal composition, comprising extracting micromycete biomass in a microwave field with a liquid extractant selected from the group consisting of lower alcohols, saturated or unsaturated hydrocarbons containing up to 10 carbon atoms in a molecule, their halogen derivatives, inert gases, nitrogen, nitrous oxide, dioxide carbon and mixtures thereof, separating the extract and introducing inactive components into it to obtain the target product, characterized in that the biomass of micromycete Mortierella spinosa var. sterilis, the treatment of the extraction mixture with the microwave field is carried out in an oscillating mode, during the action of the microwave field on the extraction mixture, the pressure in it is reduced to a value that ensures boiling of the extractant, and at the same time as the microwave field ceases to affect the extraction mixture, the pressure in it increases to the initial value.