RU2139333C1 - Vodka "magistral" - Google Patents

Abstract

FIELD: liqueur and vodka industry. SUBSTANCE: invention proposes vodka containing sugar, citric acid, sodium-containing component and an aqueous-alcoholic liquid. Vodka has sodium hydrocarbonate as a sodium-containing component at the following ratio of components, kg/1 000 dal of ready product: sugar 9.8-10.2; citric acid 0.2-0.24; sodium hydrocarbonate 0.28-0.32 and also, l: an aqueous-alcoholic liquid - the rest. Obtained vodka has a soft taste, characteristic vodka aroma. Proposed vodka corresponds to vodka prepared of an alcohol of the highest purity by its physical-chemical indices. EFFECT: high quality of vodka.

Description

 The invention relates to alcoholic beverage production, in particular to vodka.

 Known vodka "Gulyaev" [1] containing granulated sugar, citric acid and sorbitol.

 However, sorbitol is a synthetic sugar substitute, and its use in vodka is not advisable.

 The closest in technical essence and the achieved result is Monarch vodka [2], which per 1000 dal of the finished product contains sugar, citric acid 0.15-0.25 kg, a component with sodium in the form of sodium bicarbonate 0.2-0, 3 kg, aspartame 0.09-0.11 kg and water-alcohol liquid. As a result of dissolution of sodium bicarbonate and citric acid, citric acid sodium is obtained, which is introduced into the sorting (aqueous-alcoholic solution).

 However, this vodka also contains a synthetic sugar substitute - aspartame. In addition, the technological process for the preparation of vodka using sodium bicarbonate requires an additional stage of the process to obtain citric acid sodium.

 The aim of the present invention is to expand the range of vodkas and improve the organoleptic properties of vodka.

This goal is achieved by the fact that vodka containing sugar, citric acid, a component with sodium and a water-alcohol liquid, according to the invention, as a component with sodium contains sodium bicarbonate in kg in the following ratio of ingredients per 1000 gave the finished product:
Sugar - 9.8 - 10.4
Citric acid - 0.2 - 0.24
Sodium bicarbonate - 0.28 - 0.34
Water-alcohol liquid - The rest
New in the invention is that vodka as a component with sodium contains sodium bicarbonate in the following ratio of ingredients, kg per 1000 gave the finished product:
Sugar - 9.8 - 10.4
Citric acid - 0.2 - 0.24
Sodium bicarbonate - 0.28-0.34
Water-alcohol liquid - The rest
Vodka "Highway" is prepared as follows.

For the preparation of special vodka, rectified ethyl alcohol of the highest purity is used, drinking water with a hardness of up to 1 mol / m ³ for natural un softened water and up to 0.2 mol / m ³ for corrected water.

 Alcohol and water that meet the requirements of the standards are set in a sorting tank at the rate of obtaining a mixture with a strength of 40%, after which the water-alcohol solution is thoroughly mixed and passed through a coal-cleaning battery with a filtering rate of up to 40 dal / h for fresh coal and up to 30 dal / h for regenerated coal.

 Then, sodium bicarbonate is dissolved in softened water, then citric acid is added with continuous stirring to obtain sodium citric acid.

 The prepared citric acid sodium, refined granulated sugar in the form of an aqueous solution, and the aqueous-alcoholic liquid are put into a vat, mixed thoroughly and the strength is checked. If you deviate from the standard, correct vodka in the same vat by adding alcohol or water, followed by mixing and checking the strength.

 Ready vodka is sent for bottling with mandatory control filtration.

 Example 1. Alcohol and water that meet the requirements of the standards are set in a sorting tank at the rate of obtaining a mixture with a strength of 40%, after which the water-alcohol liquid is mixed, then passed through a coal-cleaning battery with a filtration rate of up to 30 dal / h for regenerated coal and up to 40 dal / h for fresh coal.

 Sodium bicarbonate in an amount of 0.26 kg is dissolved in 5 l of softened water, then, with continuous stirring, citric acid in an amount of 0.18 kg is added thereto.

 Then, the resulting solution of citric acid sodium is added to the liquefied vat, 9.6 kg of sugar are added there (all components are calculated per 1000 decaliters of the finished product) and an aqueous-alcoholic liquid with thorough stirring.

 Analyzing the qualitative composition of vodka obtained in example 1, we can draw the following conclusions: vodka is a transparent liquid with a gloss, see table.

 Examples 2-5. Highway vodka is prepared analogously to example 1, only the ingredients are used in the amounts shown in the table.

Analyzing the quality of vodka compositions according to the table, it can be concluded that an increase in citric acid and sodium carbonate leads to a burning taste of vodka, and a decrease in citric acid and sodium carbonate leads to inharmonious vodka. According to the analysis of the composition of the table, the optimal composition of vodka was selected in the following ratio of ingredients, kg per 1000 gave the finished product:
Sugar - 9.8 - 10.2
Citric acid - 0.2 - 0.24
Sodium bicarbonate - 0.28 - 0.32
and also, l:
Water-alcohol liquid - The rest
The physico-chemical characteristics of the Magistral vodka correspond to vodkas prepared with high-purity alcohol.

Indicators:
Physicochemical:
Fortress,% - 40
The volume of hydrochloric acid (HCl) with = 0.1 mol / dm ³ spent on titration of 100 cm ^{3 of} vodka, cm ³ - not more than 3.5
Mass concentration of aldehydes in terms of acetic in 1 dm ^{3 of} anhydrous alcohol, mg - not more than 8
Mass concentration of fusel oil in terms of a mixture of isoamyl and isobutyl alcohols (3: 1) in 1 dm ^{3 of} anhydrous alcohol, mg - not more than 4
Mass concentration of esters in terms of ethyl acetate in 1 dm ^{3 of} anhydrous alcohol, mg - not more than 30
The volume fraction of methyl alcohol in terms of anhydrous alcohol,% - not more than 0.05
Organoleptic:
Appearance - clear liquid
Color - colorless
Taste - soft, inherent to vodka
Aroma - characteristic vodka
Thus, high-quality vodka was obtained, the taste is soft, inherent to vodka, the aroma is characteristic of vodka.

 Vodka "Magistral" refers to high-quality distillery products, has good organoleptic properties, is stable during storage, is approved and recommended for release.

 The indicated optimal composition of the ingredients for producing Magistral vodka was tested under production conditions at Sormovsky EVZ CJSC, and positive results were obtained. Based on the results of testing, the proposed vodka with this composition of ingredients was recognized by the Central Tasting Commission of the Alcohol and Liquor Industry of the Russian Federation as complying with the established regulatory requirements and current standards for such products. The hygienic certificate 19.PTS.02.910.P.34922 was received for vodka "Magistral". V.7 from 08/29/97, the Medical Center of the Office of the President of the Russian Federation.

Sources of information
1. RU, patent N 2001096, C 12 G 3/08, 1993

 2. RU, patent N 2046133, C 12 G 3/08, 1993

Claims (1)

Vodka containing sugar, citric acid, a component with sodium and a water-alcohol liquid, characterized in that as a component with sodium it contains sodium bicarbonate in the following ratio of ingredients, kg per 1000 gave the finished product:
Sugar - 9.8 - 10.2
Citric acid - 0.2 - 0.24
Sodium bicarbonate - 0.28 - 0.32
and also, l:
Water-alcohol liquid - The rest

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