RU2015146297A - METHOD FOR PROCESSING WASTE OF COPPER-MELTING PRODUCTION - Google Patents

METHOD FOR PROCESSING WASTE OF COPPER-MELTING PRODUCTION Download PDF

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Publication number
RU2015146297A
RU2015146297A RU2015146297A RU2015146297A RU2015146297A RU 2015146297 A RU2015146297 A RU 2015146297A RU 2015146297 A RU2015146297 A RU 2015146297A RU 2015146297 A RU2015146297 A RU 2015146297A RU 2015146297 A RU2015146297 A RU 2015146297A
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Russia
Prior art keywords
copper
carried out
solution
stack
slag
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RU2015146297A
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Russian (ru)
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RU2629129C2 (en
Inventor
Василий Михайлович Рыбаулин
Ливерий Леонидович Семенов
Татьяна Викторовна Башлыкова
Хайрие Сюлейман Шан
Мустафа Сюлейман Шан
Original Assignee
Василий Михайлович Рыбаулин
Ливерий Леонидович Семенов
Татьяна Викторовна Башлыкова
Шан Хайрие Сулейман
Шан Мустафа Сулейман
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Application filed by Василий Михайлович Рыбаулин, Ливерий Леонидович Семенов, Татьяна Викторовна Башлыкова, Шан Хайрие Сулейман, Шан Мустафа Сулейман filed Critical Василий Михайлович Рыбаулин
Priority to RU2015146297A priority Critical patent/RU2629129C2/en
Publication of RU2015146297A publication Critical patent/RU2015146297A/en
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Publication of RU2629129C2 publication Critical patent/RU2629129C2/en

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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00Obtaining copper
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Processing Of Solid Wastes (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Claims (10)

1. Комплексный способ переработки шлаков, отличающийся тем, что лежалые шлаки медеплавильного производства с повышенными содержаниями металлов (Cu, Pb, Zn, Sn, Sb, As, Bi, Fe) направляют на механическое обогащение с получением коллективного концентрата и хвостов, поступающих на окомкование и кучное биовыщелачивание с получением продуктивного раствора с извлечением в него Cu, Zn, Fe, Sb, As и твердого остатка (кека), который идет на пирометаллургию с получением чернового свинца и вторичного шлака, продуктивный раствор биовыщелачивания поступает на цементацию меди с получением цементационной меди и раствора, направляемого на осаждение из него арсената кальция и получение железооксидного транспарентного пигмента.1. An integrated method of slag processing, characterized in that the stagnant slags of the copper smelting industry with high metal contents (Cu, Pb, Zn, Sn, Sb, As, Bi, Fe) are sent to mechanical enrichment to obtain collective concentrate and tailings for pelletizing and heap bioleaching to obtain a productive solution with extraction of Cu, Zn, Fe, Sb, As and a solid residue (cake), which goes to pyrometallurgy to produce crude lead and secondary slag, the productive bioleaching solution is supplied to cement iju copper to produce carburizing copper solution and directed to the precipitation therefrom of calcium arsenate and receiving transparent iron oxide pigment. 2. Способ по п. 1, отличающийся тем, что механическое обогащение проводится посредством винтовой сепарации.2. The method according to p. 1, characterized in that the mechanical enrichment is carried out by means of screw separation. 3. Способ по п. 1, отличающийся тем, что на механическое обогащение направляется шлак при наличии в нем металлизованных компонентов меди и свинца.3. The method according to p. 1, characterized in that slag is sent to the mechanical enrichment in the presence of metallized components of copper and lead in it. 4. Способ по п. 1, отличающийся тем, что окомкование шлака ведут с получением гранул крупностью 10-12 мм при расходе 0,3-0,5 кг/т и золы сжигания местных энергетических углей 0,6-0,8 кг/т.4. The method according to p. 1, characterized in that the pelletizing of slag is carried out to obtain granules with a grain size of 10-12 mm at a flow rate of 0.3-0.5 kg / t and ash burning local energy coal 0.6-0.8 kg / t 5. Способ по п. 1, отличающийся тем, что из окомкованного шлака формируется штабель для кучного биовыщелачивания.5. The method according to p. 1, characterized in that a stack for heap bioleaching is formed from pelletized slag. 6. Способ по п. 1, отличающийся тем, что кучное биовыщелачивание ведут орошением штабеля раствором бактериального комплекса из штаммов микроорганизмов Acidithiobacillus ferrooxidans и Acidithiobacillus thiooxidans в соотношении 1:1, культивированных на питательной среде 9К до достижения удельной концентрации биоклеток 106-107 клеток/мл в течение 10 суток, с начальными значениями рН 1,8-2,1, Eh 640-680 мВ, температурой 30-35°С.6. The method according to p. 1, characterized in that heap bioleaching is carried out by irrigation of the stack with a solution of the bacterial complex from strains of the microorganisms Acidithiobacillus ferrooxidans and Acidithiobacillus thiooxidans in a ratio of 1: 1, cultured on 9K medium to achieve a specific concentration of 10 6 -10 7 cells / ml for 10 days, with initial values of pH 1.8-2.1, Eh 640-680 mV, temperature 30-35 ° С. 7. Способ по п. 1, отличающийся тем, что удельный расход раствора бактериального комплекса составляет 0,5-2 л в час на 1 м2 поверхности штабеля (12-48 л в сутки на 1 м2).7. The method according to p. 1, characterized in that the specific consumption of the solution of the bacterial complex is 0.5-2 l per hour per 1 m 2 of the surface of the stack (12-48 l per day per 1 m 2 ). 8. Способ по п. 1, отличающийся тем, что кучное биовыщелачивание ведут орошением штабеля раствором бактериального комплекса в течение 6-12 месяцев с последующей выдержкой штабеля без орошения в течение 3 месяцев.8. The method according to p. 1, characterized in that heap bioleaching is carried out by irrigation of the stack with a solution of the bacterial complex for 6-12 months, followed by exposure of the stack without irrigation for 3 months. 9. Способ по п. 1, отличающийся тем, что пирометаллургическую переработку твердого остатка (кека) биовыщелачивания ведут без предварительной сушки в две стадии плавкой в жидкой ванне (плавка в печи Ванюкова) с получением чернового свинца.9. The method according to p. 1, characterized in that the pyrometallurgical processing of the solid residue (cake) of bioleaching is carried out without preliminary drying in two stages by melting in a liquid bath (melting in the Vanyukov furnace) to produce crude lead. 10. Способ по п. 1, отличающийся тем, что цементацию меди ведут на железную стружку.10. The method according to p. 1, characterized in that the carburizing of copper is carried out on iron chips.
RU2015146297A 2015-10-28 2015-10-28 Method of processing waste copper production RU2629129C2 (en)

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RU2629129C2 RU2629129C2 (en) 2017-08-24

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115198105A (en) * 2022-07-21 2022-10-18 江西泰和百盛实业有限公司 Method for removing tellurium in process of producing high-purity low-oxygen copper rod from scrap copper

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4254088A (en) * 1979-03-27 1981-03-03 The United States Of America As Represented By The United States Department Of Energy Salt-soda sinter process for recovering aluminum from fly ash
US4420464A (en) * 1981-10-26 1983-12-13 Rockwell International Corporation Recovery of vanadium from carbonaceous materials
GB8626085D0 (en) * 1986-10-31 1986-12-03 Rtz Technical Services Ltd Smelting complex polymetallic sulphide materials
FR2625512A1 (en) * 1988-01-06 1989-07-07 Fassi Stephane Processes for upgrading industrial waste
RU2206626C1 (en) * 2001-10-01 2003-06-20 Белый Василий Васильевич Method of processing ash-and-slag wastes
WO2004053173A1 (en) * 2002-12-06 2004-06-24 Mitsubishi Corporation METHOD FOR RECOVERING VALUABLE METAL FROM WASTE CONTAINING V, Mo AND Ni
DE102006022780A1 (en) * 2005-06-08 2006-12-21 Sms Demag Ag Process for the reduction and / or purification of a slag containing a metal
RU2350666C2 (en) * 2007-04-06 2009-03-27 Татьяна Викторовна Башлыкова Complex method for recycling of slags

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115198105A (en) * 2022-07-21 2022-10-18 江西泰和百盛实业有限公司 Method for removing tellurium in process of producing high-purity low-oxygen copper rod from scrap copper
CN115198105B (en) * 2022-07-21 2023-07-21 江西泰和百盛实业有限公司 Method for removing tellurium in process of producing high-purity low-oxygen copper rod from scrap copper

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