RU2009123788A - METHOD FOR PRODUCING 5-AMINO-6-METHYLURACYL - Google Patents

METHOD FOR PRODUCING 5-AMINO-6-METHYLURACYL Download PDF

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Publication number
RU2009123788A
RU2009123788A RU2009123788/04A RU2009123788A RU2009123788A RU 2009123788 A RU2009123788 A RU 2009123788A RU 2009123788/04 A RU2009123788/04 A RU 2009123788/04A RU 2009123788 A RU2009123788 A RU 2009123788A RU 2009123788 A RU2009123788 A RU 2009123788A
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RU
Russia
Prior art keywords
methyluracil
amino
producing
bromo
aqueous ammonia
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RU2009123788/04A
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Russian (ru)
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RU2417991C2 (en
Inventor
Ахат Газизьянович Мустафин (RU)
Ахат Газизьянович Мустафин
Альфия Раисовна Гимадиева (RU)
Альфия Раисовна Гимадиева
Юлия Николаевна Чернышенко (RU)
Юлия Николаевна Чернышенко
Альберт Ханифович Фаттахов (RU)
Альберт Ханифович Фаттахов
Ильдус Бариевич Абдрахманов (RU)
Ильдус Бариевич Абдрахманов
Original Assignee
Учреждение Российской академии наук Институт органической химии Уфимского научного центра РАН (RU)
Учреждение Российской академии наук Институт органической химии Уфимского научного центра РАН
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Application filed by Учреждение Российской академии наук Институт органической химии Уфимского научного центра РАН (RU), Учреждение Российской академии наук Институт органической химии Уфимского научного центра РАН filed Critical Учреждение Российской академии наук Институт органической химии Уфимского научного центра РАН (RU)
Priority to RU2009123788/04A priority Critical patent/RU2417991C2/en
Publication of RU2009123788A publication Critical patent/RU2009123788A/en
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Abstract

Способ получения 5-амино-6-метилурацила, отличающийся тем, что 5-бром-6-метилурацил взаимодействует с водным аммиаком при мольном соотношении 5-бром-6-метилурацил : водный аммиак равном 1:11 при температуре 110-140°C в течение 16-20 ч с последующим охлаждением реакционной смеси и выделением целевого продукта. A method of producing 5-amino-6-methyluracil, characterized in that 5-bromo-6-methyluracil interacts with aqueous ammonia in a molar ratio of 5-bromo-6-methyluracil: aqueous ammonia equal to 1:11 at a temperature of 110-140 ° C for 16-20 hours, followed by cooling of the reaction mixture and the selection of the target product.

Claims (1)

Способ получения 5-амино-6-метилурацила, отличающийся тем, что 5-бром-6-метилурацил взаимодействует с водным аммиаком при мольном соотношении 5-бром-6-метилурацил : водный аммиак равном 1:11 при температуре 110-140°C в течение 16-20 ч с последующим охлаждением реакционной смеси и выделением целевого продукта. A method of producing 5-amino-6-methyluracil, characterized in that 5-bromo-6-methyluracil interacts with aqueous ammonia in a molar ratio of 5-bromo-6-methyluracil: aqueous ammonia equal to 1:11 at a temperature of 110-140 ° C for 16-20 hours, followed by cooling of the reaction mixture and the selection of the target product.
RU2009123788/04A 2009-06-22 2009-06-22 Method of producing 5-amino-6-methyluracil RU2417991C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2009123788/04A RU2417991C2 (en) 2009-06-22 2009-06-22 Method of producing 5-amino-6-methyluracil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2009123788/04A RU2417991C2 (en) 2009-06-22 2009-06-22 Method of producing 5-amino-6-methyluracil

Publications (2)

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RU2009123788A true RU2009123788A (en) 2010-12-27
RU2417991C2 RU2417991C2 (en) 2011-05-10

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RU2417991C2 (en) 2011-05-10

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Effective date: 20180623