RU2006141433A - METHOD FOR PRODUCING 5- {2- [5- {2- [1,3,5-Dithiazinan-5-yl] ethyl] -4-methyl-1,3,5-thiadiazinan-3-yl] ethyl} -1, 3,5, -DITHIAZINANA - Google Patents

METHOD FOR PRODUCING 5- {2- [5- {2- [1,3,5-Dithiazinan-5-yl] ethyl] -4-methyl-1,3,5-thiadiazinan-3-yl] ethyl} -1, 3,5, -DITHIAZINANA Download PDF

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RU2006141433A
RU2006141433A RU2006141433/04A RU2006141433A RU2006141433A RU 2006141433 A RU2006141433 A RU 2006141433A RU 2006141433/04 A RU2006141433/04 A RU 2006141433/04A RU 2006141433 A RU2006141433 A RU 2006141433A RU 2006141433 A RU2006141433 A RU 2006141433A
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ethyl
dithiazinan
thiadiazinan
methyl
dithiazinana
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RU2006141433/04A
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RU2333910C1 (en
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Внира Рахимовна Ахметова (RU)
Внира Рахимовна Ахметова
Елена Борисовна Рахимова (RU)
Елена Борисовна Рахимова
Руслан Адгамович Вагапов (RU)
Руслан Адгамович Вагапов
Райхана Валлиулловна Кунакова (RU)
Райхана Валлиулловна Кунакова
Усейн Меметович Джемелев (RU)
Усейн Меметович Джемелев
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Институт нефтехимии и катализа РАН (RU)
Институт нефтехимии и катализа РАН
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Способ получения 5-{2-[5-{2-[1,3,5-дитиазинан-5-ил]этил}-4-метил-1,3,5-тиадиазинан-3-ил]этил}1,3,5-дитиазинана (1):The method of obtaining 5- {2- [5- {2- [1,3,5-dithiazinan-5-yl] ethyl} -4-methyl-1,3,5-thiadiazinan-3-yl] ethyl} 1,3 5-dithiazinan (1):
Figure 00000001
Figure 00000001
 включающий взаимодействие амина с насыщенным сероводородом водным раствором формальдегида, отличающийся тем, что в качестве амина используют метилтриэтилтетраамин при мольном соотношении амин:формальдегид:сероводород, равном 1:6:4, и реакцию проводят при температуре 20°С в течение 3 ч.comprising the interaction of an amine with an aqueous solution of formaldehyde saturated with hydrogen sulfide, characterized in that methyltriethyl tetraamine is used as an amine with an amine: formaldehyde: hydrogen sulfide molar ratio of 1: 6: 4, and the reaction is carried out at a temperature of 20 ° C for 3 hours.
RU2006141433/04A 2006-11-23 2006-11-23 Method for obtaining 5-{2-[5-{2-[1,3,5-ditiazinan-5-il]ethyl}-4-methyl-1,3,5-tiadiazinan-3-il]ethyl}-1,3,5,-ditiazinan RU2333910C1 (en)

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RU2006141433/04A RU2333910C1 (en) 2006-11-23 2006-11-23 Method for obtaining 5-{2-[5-{2-[1,3,5-ditiazinan-5-il]ethyl}-4-methyl-1,3,5-tiadiazinan-3-il]ethyl}-1,3,5,-ditiazinan

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RU2006141433/04A RU2333910C1 (en) 2006-11-23 2006-11-23 Method for obtaining 5-{2-[5-{2-[1,3,5-ditiazinan-5-il]ethyl}-4-methyl-1,3,5-tiadiazinan-3-il]ethyl}-1,3,5,-ditiazinan

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2443702C2 (en) * 2010-06-02 2012-02-27 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing mono-(di-, tetra-)methyl-1,2-bis-(1,3,5-dithiazinan-5-yl)ethanes
RU2443701C2 (en) * 2010-06-02 2012-02-27 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing 1,2-bis-(2,4,6,-trialkyl-1,3,5-dithiazinan-5-yl)ethanes

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2467006C1 (en) * 2011-06-07 2012-11-20 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of obtaining 3,3'-(1,2-phenylene)-bis-1,5,3-dithiazepinane and 3,3,-[methylene-bis-(1,4-phenylene)]-bis-1,5,3- dithiazepinane
RU2478634C2 (en) * 2011-06-16 2013-04-10 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран METHOD OF PRODUCING α,ω -BIS-(1,5,3-DITHIAZEPINAN-3-YL)ALKANES

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2443702C2 (en) * 2010-06-02 2012-02-27 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing mono-(di-, tetra-)methyl-1,2-bis-(1,3,5-dithiazinan-5-yl)ethanes
RU2443701C2 (en) * 2010-06-02 2012-02-27 Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран Method of producing 1,2-bis-(2,4,6,-trialkyl-1,3,5-dithiazinan-5-yl)ethanes

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