RU2000115752A - N-NITROXOZAZOLIDINES-1,3 AND METHOD FOR PRODUCING THEM - Google Patents

N-NITROXOZAZOLIDINES-1,3 AND METHOD FOR PRODUCING THEM

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Publication number
RU2000115752A
RU2000115752A RU2000115752/04A RU2000115752A RU2000115752A RU 2000115752 A RU2000115752 A RU 2000115752A RU 2000115752/04 A RU2000115752/04 A RU 2000115752/04A RU 2000115752 A RU2000115752 A RU 2000115752A RU 2000115752 A RU2000115752 A RU 2000115752A
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RU
Russia
Prior art keywords
general formula
och
nitroxozazolidines
producing
nitrooxazolidines
Prior art date
Application number
RU2000115752/04A
Other languages
Russian (ru)
Other versions
RU2181719C2 (en
Inventor
Владимир Александрович Тартаковский
Александр Сергеевич Ермаков
Дмитрий Борисович Виноградов
Ольга Николаевна Варфоломеева
Анатолий Петрович Денисюк
Дмитрий Леонидович Русин
Original Assignee
Институт органической химии им. Н.Д. Зелинского РАН
Filing date
Publication date
Application filed by Институт органической химии им. Н.Д. Зелинского РАН filed Critical Институт органической химии им. Н.Д. Зелинского РАН
Priority to RU2000115752A priority Critical patent/RU2181719C2/en
Priority claimed from RU2000115752A external-priority patent/RU2181719C2/en
Publication of RU2000115752A publication Critical patent/RU2000115752A/en
Application granted granted Critical
Publication of RU2181719C2 publication Critical patent/RU2181719C2/en

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Claims (2)

1. N-Нитрооксазолидины-1,3 общей формулы I:
Figure 00000001

где R= Н, СН3, СН2OСН3, CH2Cl, CH2N3.1. N-Nitrooxazolidines-1,3 of the general formula I:
Figure 00000001

where R = H, CH 3 , CH 2 OCH 3 , CH 2 Cl, CH 2 N 3 . 2. Способ получения N-нитрооксазолидинов-1,3, общей формулы I:
Figure 00000002

где R= Н, СН3, СН2OСН3, СН2С1, СН2N3,
заключающийся в том, что β-гидроксиалкилсульфаматы общей формулы II:
Figure 00000003

где R= H, CH3, CH2OCH3, CH2Cl, CH2N3
M= K, Na
подвергают взаимодействию с формальдегидом в среде воды или смеси воды со спиртом, с последующим нитрованием продукта реакции нитрующим агентом и в случае необходимости целевой продукт общей формулы I, где R= CH2Cl переводят в соединение общей формулы I, где R= СН2N3 путем обработки азидом натрия.2. The method of obtaining N-nitrooxazolidines-1,3, General formula I:
Figure 00000002

where R = H, CH 3 , CH 2 OCH 3 , CH 2 C1, CH 2 N 3 ,
consisting in the fact that β-hydroxyalkyl sulfamates of General formula II:
Figure 00000003

where R = H, CH 3 , CH 2 OCH 3 , CH 2 Cl, CH 2 N 3
M = K, Na
subjected to interaction with formaldehyde in a medium of water or a mixture of water with alcohol, followed by nitration of the reaction product with a nitrating agent and, if necessary, the target product of General formula I, where R = CH 2 Cl is transferred to a compound of General formula I, where R = CH 2 N 3 by treatment with sodium azide.
RU2000115752A 2000-06-16 2000-06-16 N-nitrooxazolidines-1,3 and method of their synthesis RU2181719C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU2000115752A RU2181719C2 (en) 2000-06-16 2000-06-16 N-nitrooxazolidines-1,3 and method of their synthesis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2000115752A RU2181719C2 (en) 2000-06-16 2000-06-16 N-nitrooxazolidines-1,3 and method of their synthesis

Publications (2)

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RU2000115752A true RU2000115752A (en) 2002-03-10
RU2181719C2 RU2181719C2 (en) 2002-04-27

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2461548C1 (en) * 2011-03-15 2012-09-20 Российская Федерация в лице Министерства промышленности и торговли (Минпромторг России) Method of producing n-nitro-5-azidomethyloxazolidine-1,3
RU2461549C1 (en) * 2011-04-20 2012-09-20 Федеральное государственное унитарное предприятие "Государственный научно-исследовательский институт "Кристалл" (ФГУП "ГосНИИ "Кристалл") Method of producing n-nitro-5-chloromethyloxazolidine-1,3

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