RO97076B1 - Polyvinyl alcohol fibre and process for producing the same - Google Patents

Polyvinyl alcohol fibre and process for producing the same

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Publication number
RO97076B1
RO97076B1 RO129118A RO12911887A RO97076B1 RO 97076 B1 RO97076 B1 RO 97076B1 RO 129118 A RO129118 A RO 129118A RO 12911887 A RO12911887 A RO 12911887A RO 97076 B1 RO97076 B1 RO 97076B1
Authority
RO
Romania
Prior art keywords
polyvinyl alcohol
degree
water
bath
dried
Prior art date
Application number
RO129118A
Other languages
Romanian (ro)
Inventor
ANDREI SîRBU
Irina-Lucretia Agachi
Maria Velicu
Constantin Radovici
Clementina-Lucia Gheorghiu
Mariana Sinderaru
Maria Ionescu
Virgil Ciobanu
ELENA PATRîNICHE
Constantin Stanciu
Original Assignee
Institutul De Cercetari Chimice
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institutul De Cercetari Chimice filed Critical Institutul De Cercetari Chimice
Priority to RO129118A priority Critical patent/RO97076B1/en
Publication of RO97076B1 publication Critical patent/RO97076B1/en

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Abstract

Inventia se refera la o fibra din alcool polivinilic, care, în scopul largirii gamei sortimentale si asigurarii unor caracteristici apropiate de a fibrelor naturale de bumbac, este constituita din alcool polivinilic cu grad de hidroliza de peste 99%, greutate moleculara de 1700...2000 si are un grad de acetizare de 28...37%, un grad de orientare de 0,935, un indice de cristalinitate de 52...65, contractie la fierbere sub 10% si se obtine printr-un procedeu ce consta în extruderea unei solutii de 14...16% alcool polivinilic în apa distilata într-o baie de coagulare formata dintr-o solutie suprasaturata de sulfat de sodiu în apa, filamentele formate fiind etirate umed într-o baie de sulfat de sodiu la o temperatura de minimum 90 degree C, uscate, pretermofixate la temperatura de 150 degree C, etirate uscat la 170...195 degree C, termofixate cu aer cald la temperatura de 185...195 degree C, acetizate într-o baie de acetizare formata din apa, acid sulfuric, sulfat de sodiu si aldehida formica, la temperatura de 90 degree C.The invention relates to a polyvinyl alcohol fiber, which, in order to broaden the assortment range and provide characteristics close to natural cotton fibers, is made of polyvinyl alcohol with a degree of hydrolysis of over 99%, a molecular weight of 1700 ... 2000 and has an acetic degree of 28-37%, an orientation degree of 0.935, a crystallinity index of 52-65, a boiling shrinkage below 10% and is obtained by a process consisting of extrusion a solution of 14-16% polyvinyl alcohol in the distilled water in a coagulation bath formed from a supersaturated solution of sodium sulfate in water, the filaments formed being wetted in a sodium sulphate bath at a temperature of at least 90 degrees C, dried, pretermophixed at 150 degrees C, dried at 170 DEG-195 DEG C., hot-melted with warm air at 185-195 DEG C., acetylated in an acetic bath made up of water, sulfuric acid, sodium sulphate and aldehydes Formica, at a temperature of 90 ° C.

RO129118A 1987-07-20 1987-07-20 Polyvinyl alcohol fibre and process for producing the same RO97076B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RO129118A RO97076B1 (en) 1987-07-20 1987-07-20 Polyvinyl alcohol fibre and process for producing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RO129118A RO97076B1 (en) 1987-07-20 1987-07-20 Polyvinyl alcohol fibre and process for producing the same

Publications (1)

Publication Number Publication Date
RO97076B1 true RO97076B1 (en) 1989-07-03

Family

ID=40905392

Family Applications (1)

Application Number Title Priority Date Filing Date
RO129118A RO97076B1 (en) 1987-07-20 1987-07-20 Polyvinyl alcohol fibre and process for producing the same

Country Status (1)

Country Link
RO (1) RO97076B1 (en)

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