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Application filed by Hilke Ciupe, Ioan Oprean, Francisc-Petru HodosanfiledCriticalHilke Ciupe
Priority to RO107620ApriorityCriticalpatent/RO84437B1/en
Publication of RO84437A2publicationCriticalpatent/RO84437A2/en
Publication of RO84437B1publicationCriticalpatent/RO84437B1/en
Organic Low-Molecular-Weight Compounds And Preparation Thereof
(AREA)
Abstract
Inventia se refera la un procedeu de preparare a acetatului de E-7-dodecen-1-01, prin reducerea cu sodiu metalic în amoniac lichid a 7-dodecin-1-olului protejat, conform caruia se supune reducerii 1-tert-butoxi-7-dodecina, 1-tert-butoxi-E-7-dodecena astfel obtinuta fiind apoi acetilata cu un amestec de clorura de acetil; acid acetic 1:10.The invention relates to a process for the preparation of E-7-dodecen-1-ol acetate by reduction with sodium metal in liquid ammonia of protected 7-dodecin-1-ol, according to which the 1-tert- 7-dodecene, 1-tert-butoxy-E-7-dodecene thus obtained is then acetylated with a mixture of acetyl chloride; acetic acid 1:10.
RO107620A1982-05-211982-05-21Process for preparing e-7-dodecene-1-ol acetate
RO84437B1
(en)