RO115953B1 - Procedeu continuu pentru prepararea dimiristilperoxidicarbonatului - Google Patents
Procedeu continuu pentru prepararea dimiristilperoxidicarbonatuluiInfo
- Publication number
- RO115953B1 RO115953B1 RO99-01109A RO9901109A RO115953B1 RO 115953 B1 RO115953 B1 RO 115953B1 RO 9901109 A RO9901109 A RO 9901109A RO 115953 B1 RO115953 B1 RO 115953B1
- Authority
- RO
- Romania
- Prior art keywords
- dimirystyl
- peroxydicarbonate
- preparing
- continuous process
- reaction
- Prior art date
Links
- BEQKKZICTDFVMG-UHFFFAOYSA-N 1,2,3,4,6-pentaoxepane-5,7-dione Chemical compound O=C1OOOOC(=O)O1 BEQKKZICTDFVMG-UHFFFAOYSA-N 0.000 title abstract 2
- 238000010924 continuous production Methods 0.000 title abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 150000002978 peroxides Chemical class 0.000 abstract 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 abstract 1
- 239000012670 alkaline solution Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- FZFAMSAMCHXGEF-UHFFFAOYSA-N chloro formate Chemical compound ClOC=O FZFAMSAMCHXGEF-UHFFFAOYSA-N 0.000 abstract 1
- 238000006073 displacement reaction Methods 0.000 abstract 1
- 239000000839 emulsion Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000000977 initiatory effect Effects 0.000 abstract 1
- 239000000178 monomer Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 238000005502 peroxidation Methods 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Invenţia se referă la un procedeu continuu pentru prepararea dimiristilperoxidicarbonatului, utilizat drept iniţiator la polimerizarea monomerilor etilenici, în special a clorurii de vinil, care constă în peroxidarea cloroformiatului de miristil cu o soluţie alcalină de apă oxigenată, la o temperatură de 20...25°C, continuarea reacţiei într-un reactor cu deplasare la o temperatură de 17...20°C, definitivarea reacţiei la 8...11°C, urmată de încălzire, separarea emulsiei de peroxid, solzificarea rapidă a fazei organice şi descărcarea electrostatică a peroxidului sub formă de solzi.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO99-01109A RO115953B1 (ro) | 1999-10-18 | 1999-10-18 | Procedeu continuu pentru prepararea dimiristilperoxidicarbonatului |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO99-01109A RO115953B1 (ro) | 1999-10-18 | 1999-10-18 | Procedeu continuu pentru prepararea dimiristilperoxidicarbonatului |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RO115953B1 true RO115953B1 (ro) | 2000-08-30 |
Family
ID=64358133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO99-01109A RO115953B1 (ro) | 1999-10-18 | 1999-10-18 | Procedeu continuu pentru prepararea dimiristilperoxidicarbonatului |
Country Status (1)
| Country | Link |
|---|---|
| RO (1) | RO115953B1 (ro) |
-
1999
- 1999-10-18 RO RO99-01109A patent/RO115953B1/ro unknown
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