PL97237B1 - ENAMEL PROTECTING METAL SURFACES AGAINST Abrasion - Google Patents

ENAMEL PROTECTING METAL SURFACES AGAINST Abrasion Download PDF

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Publication number
PL97237B1
PL97237B1 PL1969134793A PL13479369A PL97237B1 PL 97237 B1 PL97237 B1 PL 97237B1 PL 1969134793 A PL1969134793 A PL 1969134793A PL 13479369 A PL13479369 A PL 13479369A PL 97237 B1 PL97237 B1 PL 97237B1
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PL
Poland
Prior art keywords
weight
amount
metal surfaces
enamel
against abrasion
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Application number
PL1969134793A
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Polish (pl)
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Publication of PL97237B1 publication Critical patent/PL97237B1/en

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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/10Frit compositions, i.e. in a powdered or comminuted form containing lead
    • C03C8/12Frit compositions, i.e. in a powdered or comminuted form containing lead containing titanium or zirconium

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Compositions (AREA)

Description

Przedmiotem wynalazku jest emalia ceramiczna zabezpieczajaca powierzchnie metalu przed scie¬ raniem.Znane emalie stosowane do powlekania powierz¬ chni metalowych glównie naczyn z takim celem, i aby powierzchnie te uodpornic na korozje oraz na dzialanie róznych zwiazków chemicznych zawiera¬ ja tlenki krzemu, aluminium, sodu, potasu, litu, wapnia, tytanu i boru oraz fluor w róznych zwiaz¬ kachmetalicznych. 10 Jesli chodzi o uodpornienie powierzchni metalo¬ wych przed korozja i dzialaniem agresywnych zwiazków chemicznych te znane emalie zadanie to spelnialy nalezycie.Wada tych emalii byla mala ich odpornosc na j6 scieranie, zwlaszcza przy tarciu twardych kruszyw o te powierzchnie. Spowodowane bylo to niedosta¬ teczna przyczepnoscia do podloza metalicznego, oraz mala odpornoscia na tarcie powierzchniowe.Celem wynalazku jest opracowanie takiego skla- 20 du emalii aby byla ona pozbawiona wad znanych emalii ceramicznych, oraz w pelni zabezpieczala podloze metaliczne przed scieraniem.Istota emalii wedlug wynalazku jest wprowa¬ dzenie do typowego ukladu emalii zawierajacego 25 tlenek krzemu, tlenek glinu, tlenek litu, tlenek potasu, tlenek wapnia, tlenek boru i fluor — skla¬ du w odpowiedniej ilosci tlenków takich metali jak kobalt, nikiel, mangan, zelazo oraz tlenku chromu i tlenkutytanu. ao Emalia welug wynalazku sklada sie z SiOj w ilosci 37,0 do 49,7% wagowych, AL2O3 w ilosci 3,0 do 7,3% wagowych (Li20 + K2O -l- Na20) w ilosci 1,25 do 3,9% wagowych, B2O3 w ilosci 17,0 do 23,1% wagowych, Na20 w ilosci 11,0 do 16,5% wa¬ gowych, P2O5 w ilosci 1,9 do 2,1% wagowych, K2O w ilosci 0,8 do 3,0% wagowych, CoO w ilosci od 0,1 do 0,4% wagowych, Ni02 w ilosci 0,9 do 1,85% wa¬ gowych, MnO w ilosci od 0,4 do 1,05% wagowych, Fe20a w ilosci od 0,06 do 1,0% wagowych, CaO w ilosci do 2,5% wagowych, UO2 do 0,13% wago¬ wych, Na2 SiFtf w ilosci do 3,5% wagowych i CaF2 w ilosci od 7,0 do 11,2% wagowych.W innym wariancie wykonania emalia sklada sie z Si02 w ilosci 53,0 do 58,0% wagowych, B2O3 w ilosci 8,2 do 13,6% wagowych, Na20 w ilosci od ,0 do 15,0% wagowych, CaF2 w ilosci do 7,1% wagowych, CaO do 5,3% wagowych, AI2O3 w ilo¬ sci 2,4 do 4,1% wagowych, Ti02 w ilosci 1,9 do 7,0% wagowych, (Li02 + K20 + NazO) w ilosci do 1,4% wagowych, CoO w ilosci 1,4 do 2,2% wago¬ wych, K2O w ilosci 4,0% wagowych, Na3AlFs w ilosci do 6,0% wagowych, MmO w ilosci do 3,2% wagowych, Fe203 w ilosci do 0,7% wagowych, Cr203 w ilosci od 0,9 do 1,5% wagowych, CuO w ilosci do 0,1% wagowych, NiO w ilosci do 0,2% wagowych, BaO w ilosci do 0,9% wagowych i NaF w ilosci do 5,9% wagowych.Emalia wedlug wynalazku bardzo skutecznie za¬ bezpiecza powierzchnie metalowe przed scieraniem. 47 2373 Przyklad I. Emalia o skladzie w % wago¬ wych Si02 — 38,1%, Al2Oa — 6,0% grupa (Li20 + + Na20 + KzO) — 3,0%, B2Os — 22,0%, Na20 — 16,5%, P2O5 — 2,0%, K20 — 3,0%, CoO — 0,4%, NiO — 1,85%, MnO — 1,05%, Fe203 — 0,10%, CoO — 2,5%, Na2SiF6 — 3,5%. Emalie te naklada siq bezposrednio na powierzchnie metalowe.Emalia o skladzie w % wagowych: Si02 — 54,9%, B2Os — 13,6%, Na20 — 11,2%, CaF2 — 7,1%, CaO — 5,3%, AL2O3 — 2,4%, Ti02 — 1,9%, grupa (Na2 0+ K2O + Li20) — 1,4%, CoO — 2,2%. Emalie te stosuje sie jako emalie kryjaca.Przyklad II. Emalia o skladzie w % wago¬ wych: Si02 — 37,0%, AL2O3 — 3,0%, grupa (Li20 + K20+,Na20) — 1,25%, B2O3 — 23,4%, N20 — 16,5%, P2O5 — 2,1%, K20 — 2,6%, CoO — 0,4%, NiO — 1,8%, MnO — 0,45%, Fe203 — 0,16%, Li20 — 0,13%, CaF2 — 11,2%. Emalie ite naklada sie bezposrednio na powierzchnie metalowe.Emalia o skladzie w % wagowych: Si02 — 53,0%, B2O3 — 8,2%, Na20 — 15,0%, K20 — 4,0%, TiO — 6,5%, CoO —1,4%, Na3AlF6 — 6,0%, MnO — 3,2%, Fe203 — 0,7%, Cr203 — 0,9%, CuO — 0,1%, NiO — 0,2%, BaO — 0,9%. Emalie te stosuje sie jako emalie kryjaca.Przyklad III. Emalia o skladzie w % wago¬ wych: + K2O + Na20) — 3,9%, B203 — 17,0%, Na20 — 11,0%, P2O5 — 1,9%, K20 — 0,8%, CoO — 0,1%, NiO — 0,9%, MnO — 0,4%, CaF2 — 7,0%. Emalie te naklada sie bezposrednio na powierzchnie me¬ talowe.Emalia o skladzie w % wagowych: Si02 — 58,0%.B2Q3 — 9,5%, N20 — 10,0%, K2O — 4,0%, AL2O3 4 — 4,1%, Ti02 — 7,0%, Cr203 — 1,5%, NaF — 5,9%.Emalie te stosuje sie jako emalie kryjaca. PLThe subject of the invention is a ceramic enamel protecting metal surfaces against abrasion. Known enamels used for coating metal surfaces, mainly vessels, with the purpose of making these surfaces resistant to corrosion and the action of various chemical compounds, including silicon, aluminum, sodium oxides , potassium, lithium, calcium, titanium and boron and fluorine in various metallic compounds. As for the resistance of metal surfaces against corrosion and the action of aggressive chemical compounds, these known enamels have fulfilled this task properly. The disadvantage of these enamels was their low abrasion resistance, especially when rubbing hard aggregates against these surfaces. It was caused by insufficient adhesion to the metal substrate and low resistance to surface friction. The aim of the invention is to develop such a composition of the enamel that it would be free from the drawbacks of known ceramic enamels, and to fully protect the metal substrate against abrasion. The essence of the enamel according to the invention is is the introduction to a typical enamel system containing silicon oxide, aluminum oxide, lithium oxide, potassium oxide, calcium oxide, boron oxide and fluorine - the composition of an appropriate amount of metal oxides such as cobalt, nickel, manganese, iron and chromium oxide and titanium oxide. ao The enamel of the invention consists of SiOj in an amount of 37.0 to 49.7% by weight, AL2O3 in an amount of 3.0 to 7.3% by weight (Li20 + K2O -l- Na20) in an amount of 1.25 to 3.9 wt%, B2O3 in an amount 17.0 to 23.1 wt%, Na2O in an amount 11.0 to 16.5 wt%, P2O5 in an amount of 1.9 to 2.1 wt%, K2O in an amount 0.8 up to 3.0% by weight, CoO in an amount from 0.1 to 0.4% by weight, NiO2 in an amount of 0.9 to 1.85% by weight, MnO in an amount from 0.4 to 1.05% by weight, Fe20a in an amount from 0.06 to 1.0% by weight, CaO in an amount up to 2.5% by weight, UO2 to 0.13% by weight, Na2 SiFtf in an amount up to 3.5% by weight and CaF2 in an amount from 7 0 to 11.2 wt%. In another embodiment, the enamel consists of SiO2 in an amount of 53.0 to 58.0 wt%, B2O3 in an amount of 8.2 to 13.6 wt%, Na20 in an amount from .0 to 15.0% by weight, CaF2 up to 7.1% by weight, CaO up to 5.3% by weight, Al2O3 in the amount of 2.4 to 4.1% by weight, TiO2 in the amount of 1.9 to 7.0% by weight, (LiO2 + K20 + NazO) up to 1.4% by weight, CoO at 1.4 to 2.2% by weight, K2O at 4.0% by weight Aggregates, Na3AlFs up to 6.0% by weight, MmO up to 3.2% by weight, Fe2O3 up to 0.7% by weight, Cr203 up to 0.9 to 1.5% by weight, CuO up to 0.1% by weight, NiO up to 0.2% by weight, BaO up to 0.9% by weight and NaF up to 5.9% by weight. The enamel according to the invention protects metal surfaces very effectively against abrasion. 47 2373 Example I. Enamel with the composition in% by weight SiO2 - 38.1%, Al2Oa - 6.0% group (Li20 + + Na20 + KzO) - 3.0%, B2Os - 22.0%, Na20 - 16.5%, P2O5 - 2.0%, K20 - 3.0%, CoO - 0.4%, NiO - 1.85%, MnO - 1.05%, Fe203 - 0.10%, CoO - 2 , 5%, Na2SiF6 - 3.5%. These enamels are applied directly to metal surfaces. Emalies with the composition in% by weight: Si02 - 54.9%, B2Os - 13.6%, Na20 - 11.2%, CaF2 - 7.1%, CaO - 5.3% , AL2O3 - 2.4%, Ti02 - 1.9%, group (Na2 0+ K2O + Li20) - 1.4%, CoO - 2.2%. These enamels are used as covering enamels. Example II. Enamel with the composition in% by weight: SiO2 - 37.0%, AL2O3 - 3.0%, group (Li20 + K20 +, Na20) - 1.25%, B2O3 - 23.4%, N20 - 16.5% , P2O5 - 2.1%, K20 - 2.6%, CoO - 0.4%, NiO - 1.8%, MnO - 0.45%, Fe203 - 0.16%, Li20 - 0.13%, CaF2 - 11.2%. Ite enamels are applied directly to metal surfaces. Emalies with the composition in% by weight: Si02 - 53.0%, B2O3 - 8.2%, Na20 - 15.0%, K20 - 4.0%, TiO - 6.5% , CoO - 1.4%, Na3AlF6 - 6.0%, MnO - 3.2%, Fe2 O3 - 0.7%, Cr203 - 0.9%, CuO - 0.1%, NiO - 0.2%, BaO - 0.9%. These enamels are used as covering enamels. Example III. Enamel with the composition in% by weight: + K2O + Na20) - 3.9%, B203 - 17.0%, Na20 - 11.0%, P2O5 - 1.9%, K20 - 0.8%, CoO - 0.1%, NiO - 0.9%, MnO - 0.4%, CaF2 - 7.0%. These enamels are applied directly to metal surfaces. The following enamels are composed in% by weight: SiO2 - 58.0%, B2Q3 - 9.5%, N20 - 10.0%, K2O - 4.0%, AL2O3 4 - 4 , 1%, TiO2 - 7.0%, Cr2O3 - 1.5%, NaF - 5.9%. These enamels are used as opaque enamels. PL

Claims (1)

Zastrzezenia patentowe 5Patent claims 5 1. Emalia zabezpieczajaca powierzchnie metalu przed scieraniem, znamienna tym, ze sklada sie z Si02 w ilosci od 37,0 do 49,7% wagowych, A1203 w ilosci 3,0—7,3% wagowych, (Li20 + K2C + Na20) 10 w ilosci 1,25—3,9% wagowych, B2O3 w ilosci 17,0— 23,4% wagowych, Na20 w ilosci 11,0—16,5% wago¬ wych, PvOR w ilosci 1,9—!\1% wagowych, K20 w w ilosci 0,8—3,0% wagowych, CoO w ilosci 0,1— —0,4% wagowych, NiO w ilosci 0,9—1,85% wago- 15 wych, MnO w ilosci 0,4—1,05% wagowych, Fe203 w ilosci 0,06—1,0% wagowych, CaO w ilosci do 2,5% wagowych, LiaO w ilosci do 0,13% wago¬ wych, Na2SIF6 w ilosri do 3,5% wagowych, CaF2 w ilosci 7,0—11,2% wagowych. 20 2, Emalia zabezpieczajaca powierzchnie metalu przed scieraniem, znamienna tym, ze sklada sie 7 Si02 w ilosci 53,0—58,0% wagowych, B2Oa w ilosci 8,2—13,6% wagowych, Na20 w ilosci 10,0—15,0% wagowych, CaF2 w ilosci do 7,1% wagowych, CaO 25 w ilosci do 5,3% wagowych, AL2O3 w ilosci 2,4— —4,1% wagowych, Ti02 w ilosci 1,9—7,C% wago¬ wych, (Li20 + K20 + Na20) w ilosci do 1,4% wa¬ gowych, CoO w ilosci 1,4—2,2% wagowych, K2O w ilosci 4,0% wagowych, Na3ALF6 w ilosci do 30 6,w'Vo wagowych, MnO w ilosci do 3,2% wagowych, Fe20a w ilosci do 0,7% wagowych, Cr203 w ilosci 0,9—1,5% wagowych, CuO w ilosci do 0,1% wago¬ wych, NiO w ilosci do 0,2% wagowych, BaO w ilo¬ sci do 0,9% wagowych, NaF w ilosci do 5,9% wa- 85 gowych. Prac. Poligraf. UPPRL naklad 120+ 18 Cena 45 zl PL1. Enamel protecting metal surfaces against abrasion, characterized in that it consists of SiO2 in the amount from 37.0 to 49.7% by weight, A1203 in the amount of 3.0-7.3% by weight, (Li20 + K2C + Na20) 10 in the amount of 1.25-3.9% by weight, B2O3 in the amount of 17.0-23.4% by weight, Na2O in the amount of 11.0-16.5% by weight, PvOR in the amount of 1.9 -! 1% by weight, K20 in the amount of 0.8-3.0% by weight, CoO in the amount of 0.1-0.4% by weight, NiO in the amount of 0.9-1.85% by weight, MnO in the amount 0.4-1.05% by weight, Fe2O3 in the amount of 0.06-1.0% by weight, CaO in the amount of up to 2.5% by weight, LiaO in the amount of up to 0.13% by weight, Na2SIF6 in the amount of 3 5 wt.% CaF2 in an amount of 7.0-11.2 wt.%. 20 2, Enamel protecting metal surfaces against abrasion, characterized by 7 SiO 2 in the amount of 53.0-58.0% by weight, B2Oa in the amount of 8.2-13.6% by weight, Na20 in the amount of 10.0- 15.0% by weight, CaF2 up to 7.1% by weight, CaO 25 up to 5.3% by weight, AL2O3 in the amount of 2.4-4.1% by weight, TiO2 in the amount of 1.9-7, C% by weight, (Li20 + K20 + Na2O) up to 1.4% by weight, CoO at 1.4-2.2% by weight, K2O at 4.0% by weight, Na3ALF6 up to 30 6% by weight, MnO up to 3.2% by weight, Fe20a up to 0.7% by weight, Cr2O3 up to 0.9-1.5% by weight, CuO up to 0.1% by weight %, NiO in an amount up to 0.2% by weight, BaO in an amount up to 0.9% by weight, NaF in an amount up to 5.9% by weight. Wash. Typographer. UPPRL circulation 120+ 18 Price PLN 45 PL
PL1969134793A 1969-07-12 1969-07-12 ENAMEL PROTECTING METAL SURFACES AGAINST Abrasion PL97237B1 (en)

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