PL83674B1 - - Google Patents
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- Publication number
- PL83674B1 PL83674B1 PL1972156178A PL15617872A PL83674B1 PL 83674 B1 PL83674 B1 PL 83674B1 PL 1972156178 A PL1972156178 A PL 1972156178A PL 15617872 A PL15617872 A PL 15617872A PL 83674 B1 PL83674 B1 PL 83674B1
- Authority
- PL
- Poland
- Prior art keywords
- nickel
- aluminum alloy
- pyridine
- temperature
- alkylpyridines
- Prior art date
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 34
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 13
- 229910000838 Al alloy Inorganic materials 0.000 claims description 12
- NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 claims description 12
- 229910052759 nickel Inorganic materials 0.000 claims description 11
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 10
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000012670 alkaline solution Substances 0.000 claims description 5
- 238000005530 etching Methods 0.000 claims description 5
- 150000003222 pyridines Chemical class 0.000 claims description 5
- 239000007868 Raney catalyst Substances 0.000 claims description 4
- 229910000564 Raney nickel Inorganic materials 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 description 5
- ROFVEXUMMXZLPA-UHFFFAOYSA-N Bipyridyl Chemical group N1=CC=CC=C1C1=CC=CC=N1 ROFVEXUMMXZLPA-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- PIINXYKJQGMIOZ-UHFFFAOYSA-N 1,2-dipyridin-2-ylethane-1,2-dione Chemical group C=1C=CC=NC=1C(=O)C(=O)C1=CC=CC=N1 PIINXYKJQGMIOZ-UHFFFAOYSA-N 0.000 description 1
- NRGGMCIBEHEAIL-UHFFFAOYSA-N 2-ethylpyridine Chemical compound CCC1=CC=CC=N1 NRGGMCIBEHEAIL-UHFFFAOYSA-N 0.000 description 1
- XVMSFILGAMDHEY-UHFFFAOYSA-N 6-(4-aminophenyl)sulfonylpyridin-3-amine Chemical compound C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=N1 XVMSFILGAMDHEY-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000012451 post-reaction mixture Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000004076 pyridyl group Chemical group 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/06—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom
- C07D213/22—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom containing only hydrogen and carbon atoms in addition to the ring nitrogen atom containing two or more pyridine rings directly linked together, e.g. bipyridyl
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C19/00—Alloys based on nickel or cobalt
- C22C19/007—Alloys based on nickel or cobalt with a light metal (alkali metal Li, Na, K, Rb, Cs; earth alkali metal Be, Mg, Ca, Sr, Ba, Al Ga, Ge, Ti) or B, Si, Zr, Hf, Sc, Y, lanthanides, actinides, as the next major constituent
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Pyridine Compounds (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3331071A GB1390028A (en) | 1971-07-15 | 1971-07-15 | Preparation of 2,2-bipyridyls |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL83674B1 true PL83674B1 (en:Method) | 1975-12-31 |
Family
ID=10351294
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL1972156178A PL83674B1 (en:Method) | 1971-07-15 | 1972-06-21 |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS5734261B1 (en:Method) |
| AU (1) | AU462640B2 (en:Method) |
| BE (1) | BE785802A (en:Method) |
| CA (1) | CA985688A (en:Method) |
| CS (1) | CS177827B2 (en:Method) |
| DE (1) | DE2230560C3 (en:Method) |
| FR (1) | FR2145671B1 (en:Method) |
| GB (1) | GB1390028A (en:Method) |
| HU (1) | HU168640B (en:Method) |
| IT (1) | IT956779B (en:Method) |
| PL (1) | PL83674B1 (en:Method) |
| ZA (1) | ZA724187B (en:Method) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4966972A (en) * | 1989-01-19 | 1990-10-30 | Reilly Industries, Inc. | Process and catalyst for the preparation of 2,2'-bipyridyls |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB897473A (en) * | 1960-01-18 | 1962-05-30 | Ici Australia Ltd | Method and apparatus for the manufacture of 2:2-dipyridyl |
| NL290426A (en:Method) * | 1963-01-18 |
-
0
- BE BE785802D patent/BE785802A/xx not_active IP Right Cessation
-
1971
- 1971-07-15 GB GB3331071A patent/GB1390028A/en not_active Expired
-
1972
- 1972-06-19 ZA ZA724187A patent/ZA724187B/xx unknown
- 1972-06-21 PL PL1972156178A patent/PL83674B1/pl unknown
- 1972-06-21 AU AU43686/72A patent/AU462640B2/en not_active Expired
- 1972-06-22 DE DE2230560A patent/DE2230560C3/de not_active Expired
- 1972-06-22 IT IT26051/72A patent/IT956779B/it active
- 1972-07-13 CA CA147,111A patent/CA985688A/en not_active Expired
- 1972-07-13 FR FR7225435A patent/FR2145671B1/fr not_active Expired
- 1972-07-14 HU HUIE520A patent/HU168640B/hu unknown
- 1972-07-14 JP JP7067672A patent/JPS5734261B1/ja active Pending
- 1972-07-14 CS CS5020A patent/CS177827B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CS177827B2 (en:Method) | 1977-08-31 |
| FR2145671B1 (en:Method) | 1979-10-05 |
| BE785802A (fr) | 1973-01-03 |
| DE2230560C3 (de) | 1982-03-25 |
| IT956779B (it) | 1973-10-10 |
| JPS5734261B1 (en:Method) | 1982-07-22 |
| DE2230560B2 (de) | 1981-04-30 |
| DE2230560A1 (de) | 1973-02-01 |
| HU168640B (en) | 1976-06-28 |
| AU4368672A (en) | 1974-01-03 |
| ZA724187B (en) | 1973-03-28 |
| GB1390028A (en) | 1975-04-09 |
| CA985688A (en) | 1976-03-16 |
| AU462640B2 (en) | 1975-07-03 |
| FR2145671A1 (en:Method) | 1973-02-23 |
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