PL60440B1 - - Google Patents
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- Publication number
- PL60440B1 PL60440B1 PL121871A PL12187167A PL60440B1 PL 60440 B1 PL60440 B1 PL 60440B1 PL 121871 A PL121871 A PL 121871A PL 12187167 A PL12187167 A PL 12187167A PL 60440 B1 PL60440 B1 PL 60440B1
- Authority
- PL
- Poland
- Prior art keywords
- pyrido
- dihydro
- straight
- carbon atoms
- hal
- Prior art date
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- 125000004432 carbon atom Chemical group C* 0.000 claims 2
- 125000004985 dialkyl amino alkyl group Chemical group 0.000 claims 2
- SFRAVXBSPHJEBZ-UHFFFAOYSA-N 6,11-dihydropyrido[3,2-c][1,5]benzodiazepin-5-one Chemical class O=C1NC2=CC=CC=C2NC2=NC=CC=C12 SFRAVXBSPHJEBZ-UHFFFAOYSA-N 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims 1
- 229940049706 benzodiazepine Drugs 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- -1 dialkylaminoalkyl halide Chemical class 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
Claims (1)
- Zastrzezenie patentowe 1. Sposób wytwarzania pochodnych 5,6-dwuwodo- ro-5-keto-llH-pirydo-[2,3-b] [l,5]-benzodwuazepiny o wzorze ogólnym przedstawionym na rysunku, w którym Rt oznacza grupe alkilowa, a R2 oznacza grupe dwualkiloaminoalkilowa o lancuchu prostym lub rozgalezionym zawierajacym 2-5 atomów we¬ gla, znamienny tym, ze na 5,6-dwuwodoro-5-keto- llH-pirydo-[2,3-b] [l,5]-benzodwuazepine o wzorze ogólnym przedstawionym na rysunku, w którym Rt ma podane wyzej znaczenie, a R2 oznacza atom wodoru, dziala sie halogenkiem dwualkiloaminoal- kilowym o wzorze Hal-R2, w którym Ra oznacza grupe dwualkiloaminoalkilowa o lancuchu prostym lub rozgalezionym zawierajacym 2. -5 atomów wegla, a Hal oznacza atom chlorowca, w obecnosci czynni¬ ka kondensujacego, takiego jak amidek sodowy, w srodowisku weglowodoru aromatycznego, zwlaszcza ksylenu, w temperaturze wrzenia mieszaniny reak¬ cyjnej. 0 R2 II I H WDA-l. Zam. 4916. Naklad 230 egz. PL
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL60440B1 true PL60440B1 (pl) | 1970-04-25 |
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